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592-41-6

Basic Information
CAS No.: 592-41-6
Name: 1-Hexene
Molecular Structure:
Molecular Structure of 592-41-6 (1-Hexene)
Formula: C6H12
Molecular Weight: 84.16
Synonyms: 1-n-Hexene;Dialen 6;Hexene;Linealene 6;NSC 74121;
EINECS: 209-753-1
Density: 0.686 g/cm3
Melting Point: -140 °C
Boiling Point: 62.81 °C at 760 mmHg
Flash Point: -9.444 °C
Solubility: 0.005 g/100 mL
Appearance: colourless liquid
Hazard Symbols: FlammableF,HarmfulXn,DangerousN
Risk Codes: 11-65-67-51/53
Safety: 9-16-23-29-62-57-33
Transport Information:
PSA: 0.00000
LogP: 2.36260
Synthetic route
74-85-1

ethene

592-41-6

1-hexene

Conditions
ConditionsYield
With trimethylamine-N-oxide; [N(4-C6H4Br)3][B(C6F5)4]; triethylaluminum; [Cr(CO)4(2-C6H4(MeO))2PN(Me)P(2-C6H4(MeO))2] In toluene at 60℃; under 30002.4 Torr; for 1h;100%
In chlorobenzene at 45℃; under 36201.3 Torr; for 4h; Product distribution / selectivity;99%
In chlorobenzene at 60℃; under 36201.3 Torr; for 4h; Product distribution / selectivity;99%
1436-34-6

1,2-Epoxyhexane

592-41-6

1-hexene

Conditions
ConditionsYield
With triphenylphosphine at 200℃; for 6h;100%
With carbon monoxide; C29H32IrN5O; bis(trifluoromethane)sulfonimide lithium In benzene-d6 at 80℃; under 7500.75 Torr; for 24h; Catalytic behavior; Reagent/catalyst; Solvent; Temperature; Time; Schlenk technique; chemoselective reaction;98%
With zirconium(IV) chloride; sodium iodide In acetonitrile for 0.0166667h; Heating;88%
624-20-4

1,2-dibromohexane

592-41-6

1-hexene

Conditions
ConditionsYield
With 1,2-bis(diphenylphosphino)ethane nickel(II) chloride; ethylmagnesium bromide In tetrahydrofuran at 0℃;100%
With sodium tetrahydroborate; nickel dichloride In tetrahydrofuran at 20℃; for 1h;80%
With tetramethylammonium perchlorate In N,N-dimethyl-formamide Electrolysis;
16643-09-7

trimethylstannyl sodium

2695-47-8

6-Bromo-1-hexene

A

592-41-6

1-hexene

B

(CH3)3Sn((CH2)4CH)

C

73017-75-1

(CH3)3Sn(CH2C5H9)

Conditions
ConditionsYield
With tert-butylamine In tetrahydrofuran react. at 0°C under Ar;A 0%
B 100%
C 0%
With DPCH In tetrahydrofuran react. at 0°C under Ar;A <1
B 98%
C 0%
In tetrahydrofuran react. at 0°C under Ar;A 0%
B 98%
C 0%
In tetrahydrofuran; benzene react. at 0°C under Ar;A <1
B 85%
C 10%
With DCPH In tetrahydrofuran; benzene react. at 0°C under Ar;A 15%
B 79%
C 1.5%
693-02-7

hex-1-yne

592-41-6

1-hexene

Conditions
ConditionsYield
With hydrogen; N,N′-bis(salicylidene)-ethylenediamino‑palladium In pyridine for 0.35h;98%
With hydrogen In methanol at 20℃; under 760.051 Torr; for 4.5h; Green chemistry;94%
With hydrogen In methanol under 760.051 Torr; for 5.5h;93%
1631-73-8

trimethylstannane

2695-47-8

6-Bromo-1-hexene

4111-54-0

lithium diisopropyl amide

A

592-41-6

1-hexene

B

96-37-7

methyl-cyclopentane

C

661-69-8

hexamethyldistannane

Conditions
ConditionsYield
In diethyl ether; cyclohexane to 6-bromo-1-hexene (1.04 mmol) and 2 equiv. of Me3SnH in Et2O at 0°C added LDA (1.04 mmol, in cyclohexane) under Ar, react. time 20 min, quenched with water; analyzed by GLPC;A 77%
B 16%
C 97%
In diethyl ether; cyclohexane to 6-bromo-1-hexene (1.04 mmol) and 1 equiv. of Me3SnH in Et2O at 0°C added LDA (1.04 mmol, in cyclohexane) under Ar, react. time 20 min, quenched with water; analyzed by GLPC;A 41%
B 18%
C 86%
In hexane; cyclohexane to 6-bromo-1-hexene (1.04 mmol) and 2 equiv. of Me3SnH in hexane at 0°C added LDA (1.04 mmol, in cyclohexane) under Ar, react. time 20 min, quenched with water; analyzed by GLPC;A 76%
B 18%
C 27%
In hexane; cyclohexane to 6-bromo-1-hexene (1.04 mmol) and 1 equiv. of Me3SnH in hexane at 0°C added LDA (1.04 mmol, in cyclohexane) under Ar, react. time 20 min, quenched with water; analyzed by GLPC;A 45%
B 32%
C 48%
74-85-1

ethene

A

592-41-6

1-hexene

B

polyethylene

polyethylene

Conditions
ConditionsYield
In chlorobenzene at 60℃; for 4h; Product distribution / selectivity; Autoclave;A 96%
B n/a
In chlorobenzene at 60℃; under 36201.3 Torr; for 4h; Product distribution / selectivity;A 91%
B n/a
methylaluminoxane; tantalum pentachloride In chlorobenzene at 45℃; under 36201.3 Torr; for 4h; Product distribution / selectivity;A 84%
B n/a
In chlorobenzene at 45℃; under 36201.3 Torr; for 4h; Product distribution / selectivity;A 84%
B n/a
In chlorobenzene at 45℃; under 36201.3 Torr; for 4h; Product distribution / selectivity;A 26%
B n/a
2695-47-8

6-Bromo-1-hexene

A

592-41-6

1-hexene

B

96-37-7

methyl-cyclopentane

C

110-82-7

cyclohexane

Conditions
ConditionsYield
With tris-(trimethylsilyl)silane; 2,2'-azobis(isobutyronitrile) at 70℃;A 4.1%
B 93%
C 2%
With tri-n-butyl-tin hydride; 2,2'-azobis(isobutyronitrile) at 70℃;A 15%
B 83%
C 1.2%
With 9-borabicyclo[3.3.1]nonane dimer; tribenzyltin hydride In toluene at 0℃; Product distribution; variation of reagent;A 29%
B 68%
C 3%
74-85-1

ethene

A

592-41-6

1-hexene

B

872-05-9

1-Decene

Conditions
ConditionsYield
Cl(1-)*NPr4(1+) at 50℃; under 22502.3 Torr; for 1h;A 91.7%
B 5.5%
modified methylalumoxane; C28H24Cl2FeN2S In n-heptane at 30 - 52℃; under 21446.5 Torr; for 0.5h; Product distribution / selectivity;
With [η5-(3-SiMe3)C5H3CMe2-3,5-Me2C6H3]Ti(TEA) In toluene at 20℃; under 7500.75 Torr; for 0.25h; Pressure; Reagent/catalyst; Temperature; Inert atmosphere;
693-02-7

hex-1-yne

A

592-41-6

1-hexene

B

110-54-3

hexane

Conditions
ConditionsYield
With hydrogen; copper-palladium; silica gel In ethanol at 25℃; under 760 Torr; Kinetics;A 91%
B n/a
With hydrogen; platinum In ethanol at 30℃; under 15200 Torr; Product distribution; 80 atm;A 41.7%
B 57.3%
With hydrogen; Ni(C17H35COO)2; triethylaluminum In toluene at 40℃; Kinetics; Object of study: selectivity;
74-85-1

ethene

A

592-41-6

1-hexene

B

111-66-0

oct-1-ene

Conditions
ConditionsYield
With CrCl2(tetrahydrofuran)2; N,N'-bis(diphenylphosphino)-N,N'-dimethylpropane-1,3-diamine In methyl cyclohexane at 80℃; under 30003 Torr; for 0.5h; Inert atmosphere;A 9%
B 91%
bis(2-(decylthio)ethyl)amine; chromium chloride In toluene at 90℃; under 33753.4 Torr; for 0.502778 - 0.527778h; Product distribution / selectivity;A 90.85%
B 0.5%
chromium(III)2-ethylhexanoate; trimethylaluminum; N-[bis(2-methoxyphenyl)phosphino]-P,P-bis(2-methoxyphenyl)-N-methylphosphinous amide In methyl cyclohexane; toluene at 60℃; under 36003.6 - 37503.8 Torr; for 0.175h; Product distribution / selectivity;A 89.7%
B 8.5%
74-85-1

ethene

A

106-98-9

1-butylene

B

592-41-6

1-hexene

Conditions
ConditionsYield
[Ph2PC6H4C(OB(C6F5)3)O-κ2P,O](η3-CH2CMeCH2) In toluene at 0℃; under 2280.15 Torr; for 1h; Product distribution; Further Variations:; Temperatures; Pressures; oligomerization;A 90%
B 6%
With tetraphenyl phosphonium chloride; chromium at 80℃; under 37503.8 Torr; for 1h; Product distribution / selectivity;A 7.5%
B 88.3%
With [6,6'-diphenyl-[2,2']-bipyridinyl]NiBr2; triethyl aluminum sesquichloride In toluene Catalytic behavior; Reagent/catalyst; Inert atmosphere; Schlenk technique;A 88%
B 9%
52056-08-3

di-n-hexyl diselenide

A

592-41-6

1-hexene

B

112-40-3

dodecane

Conditions
ConditionsYield
at 600℃; under 20 Torr; for 0.0333333h;A 90%
B 7%
64851-26-9

1-(Dichloroamino)-n-hexane

A

592-41-6

1-hexene

B

628-73-9

hexanenitrile

Conditions
ConditionsYield
A 7%
B 88%
20449-21-2

2-(but-3-en-1-yl)-2-methyl-1,3-dioxolane

19689-19-1

5-decene

A

592-41-6

1-hexene

B

2-Methyl-2-((E)-oct-3-enyl)-[1,3]dioxolane

Conditions
ConditionsYield
aluminum oxide; tetramethylstannane; rhenium(VII) oxide In chlorobenzene at 25℃; for 3h; Yields of byproduct given;A n/a
B 87%
626-93-7

n-hexan-2-ol

592-41-6

1-hexene

Conditions
ConditionsYield
With hydrogen bromide; tetrabutyl phosphonium bromide at 200℃; for 0.25h; Menshutkin Reaction; Inert atmosphere;86%
82963-28-8

{bis(triphenylphosphine)nitrogen}{cis-HW(CO)4P(OMe)3}

2695-47-8

6-Bromo-1-hexene

A

592-41-6

1-hexene

B

100504-27-6

BrW(CO)4P(OCH3)3(1-)

Conditions
ConditionsYield
In tetrahydrofuranA 85%
B n/a
1629-60-3

1-hexene-3-one

592-41-6

1-hexene

Conditions
ConditionsYield
With n-butylsilane; tris(pentafluorophenyl)borate In dichloromethane84%
74-85-1

ethene

A

homopolymer of ethylene

homopolymer of ethylene

B

592-41-6

1-hexene

Conditions
ConditionsYield
methylaluminoxane; C33H29Cl3CrNP2 at 24 - 30℃; under 2250.23 - 22502.3 Torr; for 1 - 2h; Product distribution / selectivity;A 3%
B 83%
methylaluminoxane; C23H24Cl3CrNPS at 24 - 30℃; under 22502.3 Torr; for 1h; Product distribution / selectivity;A 18%
B 82%
[CrCl2Me(tetrahydrofuran)3]; C27H26N2; polyamethylaluminoxane-IP; trimethylaluminum In toluene at 50℃; under 7757.43 Torr; for 1h; Product distribution / selectivity;
112-17-4

n-decyl acetate

A

592-41-6

1-hexene

B

872-05-9

1-Decene

D

2511-92-4

1-Butyl-2-methylcyclopropane

E

41977-37-1

1-Methyl-2-pentylcyclopropane

F

142-29-0

cyclopentene

Conditions
ConditionsYield
at 495℃; for 0.00727778h; Rate constant; Product distribution; various temp., also in toluene, also with 14C-labelled ester;A 1.03%
B 81.3%
C 1.91%
D 1.2%
E 0.497%
F 0.45%
74-85-1

ethene

A

homopolymer of ethylene

homopolymer of ethylene

B

592-41-6

1-hexene

C

111-66-0

oct-1-ene

Conditions
ConditionsYield
methylaluminoxane; C64H58Cl6Cr2N2O2P4 In dodecane; toluene at 25℃; under 3040.2 Torr; for 1.5h; Product distribution / selectivity;A 80%
B n/a
C n/a
methylaluminoxane, aged; C54H54Cl6Cr2N2P4 In dodecane; toluene at 25℃; under 3040.2 Torr; for 1.5h; Product distribution / selectivity;A 50%
B n/a
C n/a
methylaluminoxane; C64H58Cl6Cr2N2O2P4 In toluene at 25℃; under 3040.2 Torr; for 1.5h; Product distribution / selectivity;A 20%
B n/a
C n/a
1436-34-6

1,2-Epoxyhexane

68-12-2, 33513-42-7

N,N-dimethyl-formamide

A

592-41-6

1-hexene

B

39741-97-4

formic acid 1-bromomethylpentyl ester

Conditions
ConditionsYield
With bromine; triphenylphosphine at 0℃; for 0.583333h;A n/a
B 78%
1631-73-8

trimethylstannane

2695-47-8

6-Bromo-1-hexene

A

592-41-6

1-hexene

B

96-37-7

methyl-cyclopentane

C

1527-99-7

n-butyltrimethyltin

Conditions
ConditionsYield
With n-butyllithium In octane TMTH (1.00 mmol) and 6-bromo-1-hexene (1.08 mmol) in octane cooled to 0°C under Ar, n-BuLi (1.00 mmol, in octane) added via syringe, stirred for 15 min, quenched with water; analyzed by GC;A 56%
B 30%
C 78%
95903-96-1

triethylbenzylammonium ethanolate

638-45-9

1-Iodohexane

A

592-41-6

1-hexene

B

5756-43-4

ethyl n-hexyl ether

Conditions
ConditionsYield
at 20 - 25℃; for 1h; Product distribution; other halogenoalkanes, other alkoxides and alcoholates; var. reaction conditions;A 4.8%
B 75%
at 20 - 25℃; for 1h;A 4.8%
B 75%
638-45-9

1-Iodohexane

A

592-41-6

1-hexene

B

5756-43-4

ethyl n-hexyl ether

Conditions
ConditionsYield
With triethylbenzylammonium ethanolate at 20 - 25℃; for 1h;A 4.8%
B 75%
629-03-8

1 ,6-dibromohexane

A

592-41-6

1-hexene

B

110-54-3

hexane

C

592-42-7

1,5-Hexadien

D

111-27-3

hexan-1-ol

Conditions
ConditionsYield
With tetramethylammonium perchlorate In 2,2,2-trifluoroethanol; N,N-dimethyl-formamide Electrolysis;A 4%
B 75%
C 5%
D 18%
629-03-8

1 ,6-dibromohexane

592-41-6

1-hexene

Conditions
ConditionsYield
With magnesium at 600℃;72%
1631-73-8

trimethylstannane

2695-47-8

6-Bromo-1-hexene

A

592-41-6

1-hexene

B

96-37-7

methyl-cyclopentane

Conditions
ConditionsYield
In diethyl ether Irradiation (UV/VIS); photoinduced react. of 6-bromo-1-hexene (1.04 mmol) with 2 equiv. of Me3SnH in Et2O under Ar; analyzed by GLPC;A 71%
B 20%
In hexane Irradiation (UV/VIS); photoinduced react. of 6-bromo-1-hexene (1.04 mmol) with 1 equiv. of Me3SnH in hexane under Ar; analyzed by GLPC;A 51%
B 46%
In diethyl ether Irradiation (UV/VIS); photoinduced react. of 6-bromo-1-hexene (1.04 mmol) with 1 equiv. of Me3SnH in Et2O under Ar; analyzed by GLPC;A 51%
B 45%
37555-23-0

2-trifluoromethylsulfonyloxy-1-hexene

124-38-9

carbon dioxide

A

592-41-6

1-hexene

B

4380-88-5

2-butylacrylic acid

Conditions
ConditionsYield
With bis-triphenylphosphine-palladium(II) chloride; tetrabutylammonium tetrafluoroborate In N,N-dimethyl-formamide at 20℃; under 760 Torr; electrolyses, carbon cathode, Mg anode, E=-2.2 V;A 8%
B 70%
With nBuNBF4; bis-triphenylphosphine-palladium(II) chloride In N,N-dimethyl-formamide at 20℃; electrochemical reaction;A 8%
B 70%
2695-47-8

6-Bromo-1-hexene

A

592-41-6

1-hexene

B

5876-87-9

1,11-dodecadiene

C

96-37-7

methyl-cyclopentane

Conditions
ConditionsYield
With potassium In ammonia; tert-butyl alcohol Product distribution; Mechanism; Heating;A 63.6%
B 20.7%
C 0.7%
With potassium In ammonia; tert-butyl alcohol Heating;A 63.6%
B 20.7%
C 0.7%
75-54-7

Dichloromethylsilane

592-41-6

1-hexene

14799-94-1

n-hexylmethyldichlorosilane

Conditions
ConditionsYield
at 90℃; for 5h; Inert atmosphere;100%
at 90℃; for 5h; Inert atmosphere;100%
Stage #1: 1-hexene With diethylenetriaminepentaacetic acid (DTPA)-functionalized silica supported Pt at 60℃; for 0.5h;
Stage #2: Dichloromethylsilane at 60℃; for 4h; Catalytic behavior; Temperature; Reagent/catalyst;
99.6%
592-41-6

1-hexene

1436-34-6

1,2-Epoxyhexane

Conditions
ConditionsYield
With C20H24CoN2O6(1+)*NO3(1-)*H2O; oxygen; isobutyraldehyde In acetonitrile at 60℃; under 760.051 Torr; for 8h; Time; chemoselective reaction;100%
With dihydrogen peroxide; (Bu4N)3K[γ-SiW10O36(PhPO)2] In water at 65℃; for 2h; microwave irradiation;99%
With tert.-butylhydroperoxide In acetonitrile at 65 - 68℃; for 24h;99%
592-41-6

1-hexene

624-20-4

1,2-dibromohexane

Conditions
ConditionsYield
With bromine In chloroform at 0℃; for 0.166667h;100%
With bromine In chloroform at 0 - 5℃;93%
With propane 3-bromo-1-(triphenylphosphonium) tribromide In dichloromethane at 20℃; for 0.5h;92%
592-41-6

1-hexene

6920-22-5

Hexane-1,2-diol

Conditions
ConditionsYield
With poly{[CuBa(pyridine-2,5-dicarboxylate)2(H2O)5]*H2O}; dihydrogen peroxide In acetonitrile at 60℃; for 6h; Catalytic behavior; Reagent/catalyst;100%
With N-methyl-2-indolinone; fluorous OsO4 In water; acetone; tert-butyl alcohol at 20℃; for 36h;97%
With N-methyl-2-indolinone; polysulfone microencapsulated OsO4 In water; acetone; acetonitrile at 20℃; for 0.416667h;96%
592-41-6

1-hexene

110-54-3

hexane

Conditions
ConditionsYield
With hydrogen; In tetrahydrofuran at 90℃; under 5250.4 Torr; for 0.166667h; Product distribution; other olefins, other catalysts; var. temp., solv., press., and time;100%
With hydrogen; (iPrPDI)Fe(N2)2 at 20℃; under 3040 Torr; for 19h;100%
With Wilkinson's catalyst; hydrogen In dichloromethane-d2 at 45℃; under 3000.3 Torr; for 6h; Concentration; Reagent/catalyst; Solvent; Temperature; Time; Sealed tube; Inert atmosphere;100%
592-41-6

1-hexene

591-78-6

n-hexan-2-one

Conditions
ConditionsYield
With water; palladium dichloride In N,N-dimethyl-formamide under 1300 Torr; for 5h; Rate constant; Mechanism; oxidation of different olefines by Wacker process; variation of solvent: formamide, tensioactive and cotensioactive component in microemulsions; reaction time;100%
With water; palladium dichloride In various solvent(s) under 1300 Torr; for 0.833333h; closed reactor, in microemulsion with formamide;100%
With Pd(II)(15-crown-5-phen)Cl2; dinitrogen monoxide In N,N-dimethyl acetamide; water at 150℃; under 2250.23 Torr; for 18h;99%
592-41-6

1-hexene

928-65-4

hexyltrichlorosilane

Conditions
ConditionsYield
With trichlorosilane at 90℃; for 5h; Inert atmosphere;100%
With trichlorosilane at 90℃; for 5h; Inert atmosphere;100%
With trichlorosilane; nickel In tetrahydrofuran at 20 - 25℃;94%
592-41-6

1-hexene

592-43-8

2-hexene

Conditions
ConditionsYield
With C10H19B11Cl11PPd In dichloromethane-d2 at 25℃; for 0.0833333h; Inert atmosphere;100%
With aluminum (III) chloride; [(2,6-iPrC6H3NC(Me)C(Me)N-2,6-iPrC6H3)Pd(CH3)(Cl)]; acetonitrile In dichloromethane at 25℃; for 18h; Reagent/catalyst; Darkness; Inert atmosphere;81%
With platinum on activated charcoal; carbon dioxide at 300 - 305℃;
617-86-7

triethylsilane

592-41-6

1-hexene

13810-04-3

n-hexyltriethylsilane

Conditions
ConditionsYield
at 90℃; for 5h; Inert atmosphere;100%
at 90℃; for 5h; Inert atmosphere;100%
With C26H31F5NZn(1+)*C24BF20(1-) In dichloromethane-d2 at 20℃; for 28h; Reagent/catalyst; Inert atmosphere; Glovebox;100%
592-41-6

1-hexene

1066-35-9

dimethylmonochlorosilane

3634-59-1

dimethylhexylsilyl chloride

Conditions
ConditionsYield
at 90℃; for 5h; Inert atmosphere;100%
With platinum on carbon nanotubes In neat (no solvent) at 20℃; for 24h;97%
dihydrogen hexachloroplatinate In diethyl ether for 15h; Heating;80%
592-41-6

1-hexene

2487-90-3

trimethoxysilane

3069-19-0

n-hexyltrimethoxysilane

Conditions
ConditionsYield
at 90℃; for 5h; Inert atmosphere;100%
at 90℃; for 5h; Inert atmosphere;100%
With dichlorobis-(ethylene)-μ,μ'-dichloroplatinum(II)
592-41-6

1-hexene

998-30-1

Triethoxysilane

18166-37-5

hexyltriethoxysilane

Conditions
ConditionsYield
at 90℃; for 5h; Inert atmosphere;100%
at 90℃; for 5h; Inert atmosphere;100%
With platinum on carbon nanotubes In neat (no solvent) at 20℃; for 24h;98%
592-41-6

1-hexene

938-24-9

indantrione

145046-47-5

2-((E)-Hex-2-enyl)-2-hydroxy-indan-1,3-dione

Conditions
ConditionsYield
In chloroform at 80℃; for 4h;100%
592-41-6

1-hexene

13412-55-0

triphenylmethylacetonitrile oxide

123622-72-0

5-butyl-3-(triphenylmethyl)-2-isoxazoline

Conditions
ConditionsYield
In benzene at 85℃; for 48h;100%
592-41-6

1-hexene

824-79-3

sodium 4-methylbenzenesulfinate

71963-96-7

2-iodo-1-tosylhexane

Conditions
ConditionsYield
With iodine In water; ethyl acetate at 20℃; for 1.33333h; iodosulfonization;100%
With iodine In water; ethyl acetate for 2h; Ambient temperature;
592-41-6

1-hexene

114341-77-4

α-bromopropionyl 2-oxazolidinone amide

4-bromo-2-methyloctanoyl 2-oxazolidinone amide

Conditions
ConditionsYield
With triethyl borane; scandium tris(trifluoromethanesulfonate) In hexane; 1,2-dichloro-ethane at 25℃; for 1h;100%
592-41-6

1-hexene

141353-28-8

3-bromoacetyl-1,3-oxazolidin-2-one

224804-26-6

4-bromooctanoyl 2-oxazolidinone amide

Conditions
ConditionsYield
With triethyl borane; ytterbium(III) triflate In hexane; 1,2-dichloro-ethane at 25℃; for 1h;100%
With air; triethyl borane In 2,2,2-trifluoroethanol at 25℃; for 1.5h;90%
With triethyl borane; oxygen; ytterbium(III) triflate In hexane; 1,2-dichloro-ethane at 20℃; for 0.5h;83%
592-41-6

1-hexene

114341-80-9

(S)-4-Benzyl-3-((R)-2-bromo-propionyl)-oxazolidin-2-one

4-bromo-2-methyloctanoyl (5(S)-benzyl-2-oxazolidone) amide

Conditions
ConditionsYield
With triethyl borane; scandium tris(trifluoromethanesulfonate) In hexane; 1,2-dichloro-ethane at 25℃; for 1h;100%
592-41-6

1-hexene

280-64-8

9-bora-bicyclo[3.3.1]nonane

42371-64-2

9-hexyl-9-borabicyclo[3.3.1]nonane

Conditions
ConditionsYield
In tetrahydrofuran at 60℃; for 12h; Schlenk technique; Inert atmosphere;100%
In tetrahydrofuran at 25℃; for 24h; Schlenk technique; Inert atmosphere;100%
In tetrahydrofuran at 20℃; for 2h;87%
592-41-6

1-hexene

56252-56-3

diisobutyl(2,6-di-tert-butyl-4- methylphenoxy)aluminum

106751-52-4

C6H13Al(OC6H2(CH3)(C(CH3)3)2(CH2CH(CH3)2))

Conditions
ConditionsYield
With catalyst: ZrCl2(C5H5)2/AlH(CH2CH(CH3)2)2 In xylene react. of the Al compd. with the olefin (mol ratio 1:3) in dry xylene at 140°C for 5-7 h;100%
With catalyst: ZrCl4/AlH(CH2CH(CH3)2)2 In toluene react. of the Al compd. with the olefin (mol ratio 1:3) in toluene for 10 h;78%
With catalyst: (C5H5)2ZrCl2-iBu2AlH In xylene byproducts: isobutene; addn. of Cp2ZrCl2 to phenoxide at 20°C, mixt. stirred 0.5h, addn. of i-Bu2AlH, refluxed and addn. of olefin, reaction time 5 h at 140°C; isobutene condensed in a trap cooled to -78°C;
With catalyst: (C5H5)2ZrCl2-iBu2AlH In toluene byproducts: isobutene; addn. of Cp2ZrCl2 to phenoxide at 20°C, mixt. stirred 0.5h, addn. of i-Bu2AlH, refluxed and addn. of olefin, reaction time 10h at 140°C; isobutene condensed in a trap cooled to -78°C;
With catalyst: ZrCl4/AlH(CH2CH(CH3)2)2 In xylene react. of the Al compd. with the olefin (mol ratio 1:3) in dry xylene at 140°C for 5-7 h;<50
592-41-6

1-hexene

892-20-6

triphenylstannane

103047-76-3

n-hexyltriphenylstannane

Conditions
ConditionsYield
Irradiation (UV/VIS); UV-irradiation at 25-50 °C for 18 h;;100%
Irradiation (UV/VIS); UV-irradiation at 25-50 °C for 18 h;;100%
592-41-6

1-hexene

1145706-23-5

[Re(Br)(H)(NO)(PiPr3)2]

1260114-02-0

[Re(Br)(H)(NO)(Pi-Pr3)2(η2-CH2=CHBu)]

Conditions
ConditionsYield
In benzene-d6 (N2, Schlenk) complex and 1-hexane were mixed in C6D6; evapd. in vac. for 24 h; elem. anal.;100%
With BH3*THF or B(C6F5)3 or B(C2H5)3 or B(C6H5)3 (Ar) the complex and boron Lewis acid (B(C6F5)3 or BH3*THF or B(C2H5)3 or B(C6H5)3) were mixed in 1-hexane; detected by NMR spectra;
592-41-6

1-hexene

1873-88-7

1,1,1,3,5,5,5-heptamethyltrisiloxan

1873-90-1

3-n-hexyl-1,1,1,3,5,5,5-heptamethyltrisiloxane

Conditions
ConditionsYield
With 1,3-bis(tert-buthylethynyl)-1,1,3,3-tetramethyldisiloxane platinum (0) at 50℃; for 16h; Time; Reagent/catalyst;100%
With C27H55NOPtSi5 In benzene-d6; toluene at 50℃; for 5h; Reagent/catalyst; Concentration; Schlenk technique; Inert atmosphere;95%
With C24H33N2ORh In tetrahydrofuran at 20℃; for 24h; Time; Inert atmosphere; Glovebox; regioselective reaction;86%
67-56-1

methanol

592-41-6

1-hexene

1514956-43-4

2-methoxyhexyltellurium tribromide

Conditions
ConditionsYield
With tellurium(IV) tetrabromide for 8h; Heating; regioselective reaction;100%
592-41-6

1-hexene

1333-74-0

hydrogen

110-54-3

hexane

Conditions
ConditionsYield
With C61H98ClN3P2Ru In dichloromethane-d2 at 50℃; under 3040.2 Torr; for 4h; Reagent/catalyst; Time;100%
With triethylsilane; ReH(NO)2(P(CH(CH3)2)3)2; tris(pentafluorophenyl)borate at 100℃; under 30003 Torr; for 1h; Catalytic behavior; Autoclave;
With triethylsilane; [ReH(NO)2(P(C6H11)3)2]; tris(pentafluorophenyl)borate at 100℃; under 30003 Torr; for 1h; Catalytic behavior; Autoclave;
1295-35-8

bis(1,5-cyclooctadiene)nickel (0)

592-41-6

1-hexene

4141-59-7

1,2-bis(di-tert-butyl)phosphinoethane

[(dtbpe)Ni(1-hexene)]

Conditions
ConditionsYield
In tetrahydrofuran-d8 at 60℃; for 24h; Inert atmosphere;100%
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Consensus Reports

Reported in EPA TSCA Inventory.

Standards and Recommendations

ACGIH TLV: TWA 50 ppm

Specification

The 1-Hexene is an organic compound with the formula C6H12. The IUPAC name of this chemical is hex-1-ene. With the CAS registry number 592-41-6, it is also named as Hexene. The product's categories are Industrial/Fine Chemicals; 1-Olefins (GC Standard); Analytical Chemistry; Standard Materials for GC; HA-HTGasoline, Diesel & Petroleum; Alpha Sort; E-LAlphabetic; H; Olefins; Substance Classes; Volatiles/ Semivolatiles; Acyclic; Alkenes; Organic Building Blocks. Besides, it is colourless liquid, which should be stored in a closed cool and dry place.

The primary use of 1-hexene is as a comonomer in production of polyethene. Another significant use of 1-hexene is the production of linear aldehyde via hydroformylation ( oxo synthesis ) for later production of the short-chain fatty acid heptanoic acid.

Physical properties about 1-Hexene are: (1)ACD/LogP: 3.36; (2)ACD/LogD (pH 5.5): 3.356; (3)ACD/LogD (pH 7.4): 3.356; (4)ACD/BCF (pH 5.5): 209.093; (5)ACD/BCF (pH 7.4): 209.093; (6)ACD/KOC (pH 5.5): 1594.066; (7)ACD/KOC (pH 7.4): 1594.066; (8)#Freely Rotating Bonds: 3; (9)Index of Refraction: 1.397; (10)Molar Refractivity: 29.571 cm3; (11)Molar Volume: 122.67 cm3; (12)Polarizability: 11.723×10-24cm3; (13)Surface Tension: 20.139 dyne/cm; (14)Density: 0.686 g/cm3; (15)Enthalpy of Vaporization: 29.24 kJ/mol; (16)Boiling Point: 62.81 °C at 760 mmHg; (17)Vapour Pressure: 188.145 mmHg at 25°C.

Preparation: this chemical can be prepared by ethene. This reaction will need reagent methylaluminoxane, catalyst tridentate PNP Cr(III) complex. The reaction time is 30 min with reaction temperature of 80 °C. The yield is about 100%.



Uses of 1-Hexene: it can be used to produce hex-1-en-3-one at temperature of 55 °C. It will need reagent HgSO4 and diluted H2SO4.

When you are using this chemical, please be cautious about it as the following:
It is highly flammable and toxic to aquatic organisms, may cause long-term adverse effects in the aquatic environment. If swallowed, do not induce vomiting: seek medical advice immediately and show this container or label. Please keep container in a well-ventilated place and keep away from sources of ignition - No smoking. Take precautionary measures against static discharges. In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. Besides, this chemical may cause lung damage if swallowed. It is vapours may cause drowsiness and dizziness. When you are using it, do not empty into drains and do not breathe gas/fumes/vapour/spray (appropriate wording to be specified by the manufacturer). In case of contact with eyes, rinse immediately with plenty of water and seek medical advice.

You can still convert the following datas into molecular structure:
(1)SMILES: CCCCC=C
(2)InChI: InChI=1/C6H12/c1-3-5-6-4-2/h3H,1,4-6H2,2H3
(3)InChIKey: LIKMAJRDDDTEIG-UHFFFAOYAY
(4)Std. InChI: InChI=1S/C6H12/c1-3-5-6-4-2/h3H,1,4-6H2,2H3
(5)Std. InChIKey: LIKMAJRDDDTEIG-UHFFFAOYSA-N

The toxicity data is as follows:

Organism Test Type Route Reported Dose (Normalized Dose) Effect Source
rabbit LD skin > 10gm/kg (10000mg/kg) SKIN AND APPENDAGES (SKIN): HAIR: OTHER National Technical Information Service. Vol. OTS0535205,
rat LC50 inhalation 32000ppm/4H (32000ppm) BEHAVIORAL: GENERAL ANESTHETIC

BEHAVIORAL: SOMNOLENCE (GENERAL DEPRESSED ACTIVITY)

LUNGS, THORAX, OR RESPIRATION: OTHER CHANGES
National Technical Information Service. Vol. OTS0535205,
rat LD oral > 10gm/kg (10000mg/kg)   National Technical Information Service. Vol. OTS0535205,