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506-68-3

Basic Information
CAS No.: 506-68-3
Name: Cyanogen bromide
Article Data: 107
Molecular Structure:
Molecular Structure of 506-68-3 (Cyanogen bromide)
Formula: CBrN
Molecular Weight: 105.922
Synonyms: Cyanogenbromide (8CI);Bromine cyanide;Bromine cyanide (BrCN);Bromine monocyanide;Bromocyan;Bromocyanide;Bromocyanide (BrCN);Bromocyanogen;Campilit;Cyanobromide;Cyanogen bromide (BrCN);Cyanogen monobromide;NSC 89684;
EINECS: 208-051-2
Density: 2.052 g/cm3
Melting Point: 50-53 °C(lit.)
Boiling Point: 61.5 °C at 760 mmHg
Flash Point: 61.4°C
Solubility: decomposed slowly by cold H2O [HAW93]
Appearance: white crystalline solid
Hazard Symbols: VeryT+,DangerousN,FlammableF,CorrosiveC
Risk Codes: 26/27/28-34-50/53-40-11-36/37
Safety: 53-28-36/37/39-45-60-61-26-16-7/9
Transport Information: UN 3390 6.1/PG 1
PSA: 23.79000
LogP: 0.86238
Synthetic route
302-04-5

Thiocyanate

hypobromite

A

506-68-3

bromocyane

B

10097-32-2

bromide

C

14808-79-8

Sulfate

Conditions
ConditionsYield
With sodium hydroxide; sodium perchlorate In water Kinetics; Rapid addn. of thermostated aq. NaOBr soln. to aq. NaClO4 soln. contg. SCN(1-) and NaOH, 293-313 K; Monitored by iodometric estimation of unreacted OBr(1-), react. mechanism discussed.;A 94%
B n/a
C 95%
302-04-5

Thiocyanate

CH3C6H4SO2NBr(1-)

A

506-68-3

bromocyane

B

10097-32-2

bromide

C

14808-79-8

Sulfate

D

70-55-3

toluene-4-sulfonamide

Conditions
ConditionsYield
With sodium hydroxide; sodium perchlorate In water Kinetics; Rapid addn. of thermostated aq. bromamine-T soln. to aq. NaClO4 soln. contg. SCN(1-) and NaOH, 303 K; Monitored by iodometric estimation of unreacted bromamin-T, react. mechanism discussed.;A 94%
B n/a
C 95%
D n/a
333-20-0

potassium thioacyanate

41085-71-6

bromamine T

A

506-68-3

bromocyane

B

10097-32-2

bromide

C

14808-79-8

Sulfate

D

70-55-3

toluene-4-sulfonamide

Conditions
ConditionsYield
With sodium hydroxide; sodium perchlorate In water Kinetics; Rapid addn. of thermostated aq. bromamine-T soln. to aq. NaClO4 soln. contg. SCN(1-) and NaOH, 303 K; Monitored by iodometric estimation of unreacted bromamin-T, react. mechanism discussed.;A 94%
B n/a
C 95%
D n/a

sodium hypobromide

333-20-0

potassium thioacyanate

A

506-68-3

bromocyane

B

10097-32-2

bromide

C

14808-79-8

Sulfate

Conditions
ConditionsYield
With sodium hydroxide; sodium perchlorate In water Kinetics; Rapid addn. of thermostated aq. NaOBr soln. to aq. NaClO4 soln. contg. SCN(1-) and NaOH, 293-313 K; Monitored by iodometric estimation of unreacted OBr(1-), react. mechanism discussed.;A 94%
B n/a
C 95%
128-08-5

N-Bromosuccinimide

1600-27-7

mercury(II) diacetate

333-20-0

potassium thioacyanate

A

123-56-8

Succinimide

B

506-68-3

bromocyane

C

10097-32-2

bromide

D

14808-79-8

Sulfate

E

hydrogen cation

Conditions
ConditionsYield
With sodium hydroxide In methanol; water Kinetics; oxidation of SCN(1-) by NBS in aq. methanol in presence of mercuric acetate and NaOH at 303 K; gravimetric and iodometric methods;A n/a
B 94%
C n/a
D 94%
E n/a
With perchloric acid In methanol; water Kinetics; oxidation of SCN(1-) by NBS in aq. methanol in presence of mercuric acetate and HClO4 at 273 K; gravimetric and iodometric methods;A n/a
B 94%
C n/a
D 94%
E n/a

ammonium bromide

74-90-8

hydrogen cyanide

506-68-3

bromocyane

Conditions
ConditionsYield
In water Electrolysis; potential: 3.2 V;current density:929 A/dm2; molar ratio: 1-1;89%
773837-37-9

sodium cyanide

506-68-3

bromocyane

Conditions
ConditionsYield
With bromine In water89%
Stage #1: sodium cyanide With hydrogenchloride In water at 0 - 5℃; for 0.166667h;
Stage #2: With bromine In water at 0 - 5℃; for 1.3h; pH=< 7; Time;
With bromine In water at -5 - 5℃;
With bromine In methanol at 1℃; for 0h; Inert atmosphere;

potassium cyanide

506-68-3

bromocyane

Conditions
ConditionsYield
With bromine; potassium bromide In water at 0 - 5℃; for 0.0866667h; Flow reactor;72%
289-82-7

2H-1,2-oxazine

1415915-00-2

(S)-3-amino-2,2,4-trifluoro-3-(2-fluoro-phenyl)-butan-1-ol

A

506-68-3

bromocyane

B

1415915-01-3

(S)-5,5-difluoro-4-fluoromethyl-4-(2-fluoro-phenyl)-5,6-dihydro-4H-[1,3]oxazin-2-ylamine

Conditions
ConditionsYield
A n/a
B 41%
2973-00-4

dibromo-dinitro-methane

151-50-8

potassium cyanide

506-68-3

bromocyane

Conditions
ConditionsYield
With ethanol
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Chemistry

IUPAC Name:Carbononitridic bromide
Molecular Formula:CBrN
Formula Weight:105.92g/mol
Storage temp.:0-6°C
Density:1.443 g/mL at 25 °C
Melting Point:50-53 °C(lit.)
Boiling Point:61-62 °C(lit.)
Index of Refraction:1.467
Flash point:61.4°C
Vapor Pressure:100 mm Hg ( 22.6 °C)
EINECS:208-051-2
Molar Refractivity:14.32cm
Molar Volume:51.6cm3 
Polarizability:5.67 10-24cm3
Surface Tension:43.2dyne/cm  
Enthalpy of Vaporization:30.39kJ/mol 
Stability: Stable. Reacts violently with water and with mineral and organic acids
Synonyms of Cyanogen bromide (506-68-3) :(CN)Br;BrCN;Bromine cyanide(BrCN);Bromine monocyanide;brominecyanide(brcn);Bromocyanide(BrCN);Bromocyanogen;Bromure de cyanogen
Product Categories of Cyanogen bromide (506-68-3):Inorganics;C1 to C5;Cyanides/Nitriles;Nitrogen Compounds
Structure of Cyanogen bromide (506-68-3):

 

Uses

It can be used as microbicides and military poison,and also can be used in the preparation of cyanide and organic synthesis.

Toxicity Data With Reference

1.    

ihl-hmn LCLo:92 ppm/10M

    NTIS**    National Technical Information Service. (Springfield, VA 22161) (Formerly U.S. Clearinghouse for Scientific and Technical Information) PB214-270 .
2.    

ihl-mus LCLo:500 mg/m3/10M

    NDRC**    National Defense Research Committee, Office of Scientific Research and Development, Progress Report No. 9-4-1-9 ,1943.

Hazard Codes  T+,N,F,C
Risk Statements  26/27/28-34-50/53-40-11-36/37 
26/27/28:  Very Toxic by inhalation, in contact with skin and if swallowed
34:  Causes burns 
50/53:  Very Toxic to aquatic organisms, may cause long-term adverse effects in the aquatic environment
40:  Limited evidence of a carcinogenic effect 
11:  Highly Flammable
36/37:  Irritating to eyes and respiratory system 
Safety Statements  53-28-36/37/39-45-60-61-26-16-7/9
53:  Avoid exposure - obtain special instruction before use
28:  After contact with skin, wash immediately with plenty of ... (to be specified by the manufacturer)
36/37/39:  Wear suitable protective clothing, gloves and eye/face protection
45:  In case of accident or if you feel unwell, seek medical advice immediately (show label where possible) 
60:  This material and/or its container must be disposed of as hazardous waste 
61:  Avoid release to the environment. Refer to special instructions safety data sheet
26:  In case of contact with eyes, rinse immediately with plenty of water and seek medical advice 
16:  Keep away from sources of ignition - No smoking   
7/9:  Keep container tightly closed and in a well-ventilated place 

Consensus Reports

Cyanide and its compounds are on the Community Right-To-Know List. EPA Extremely Hazardous Substances List. Reported in EPA TSCA Inventory.

Safety Profile

A human and experimental poison by inhalation. Corrosive. When heated to decomposition it emits very toxic fumes of CN and Br. Possibly unstable. See also other cyanogen entries; CYANIDE; and BROMIDES.

Standards and Recommendations

DOT Classification:  6.1; Label: Poison, Corrosive

Specification

Cyanogen bromide is a colorless to white crystalline solid with a penetrating odor. Cyanogen bromide is slightly soluble in water. Cyanogen bromide is gradually decomposed by water and very rapidly by acids to give off hydrogen bromide, a flammable and poisonous gas. Contamination with many materials can cause rapid decomposition of the material. Cyanogen bromide is toxic by inhalation of its vapors or by the hydrogen cyanide from decomposition or by ingestion. Toxic oxides of nitrogen are produced in fire involving Cyanogen bromide. Cyanogen bromide is used in gold extraction, to make other chemicals, and as a fumigant.