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Factory direct supply best price CAS:951-77-9 Deoxycytidine monohydrate
Cas No: 951-77-9
USD $ 21.0-21.0 / Gram 10 Gram 1000 Kilogram/Month Hebei Huanchang Metallurgical Materials Co., Ltd. Contact Supplier
2'-Deoxycytidine
Cas No: 951-77-9
USD $ 32.0-50.0 / Kilogram 1 Kilogram 30 Metric Ton/Month XINXIANG AURORA BIOTECHNOLOGY CO., LTD. Contact Supplier
SAGECHEM/ 2'-Deoxycytidine /Manufacturer in China/SAGECHEM
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2'-Deoxycytidine monohydrate Manufacturer/High quality/Best price/In stock
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USD $ 3.0-3.0 / Kilogram 1 Kilogram 1-100 Metric Ton/Month Dayang Chem (Hangzhou) Co.,Ltd. Contact Supplier
High quality 2'-Deoxycytidine supplier in China
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No Data No Data Metric Ton/Day Simagchem Corporation Contact Supplier
High purity 951-77-9 2′-Deoxycytidine
Cas No: 951-77-9
USD $ 100.0-500.0 / Gram 1 Gram 99999 Gram/Year Hangzhou Dingyan Chem Co., Ltd Contact Supplier
Factory supply high quality 2-Deoxycytidine monohydrate Cas 951-77-9 with best price
Cas No: 951-77-9
USD $ 821.0-896.0 / Kilogram 1 Kilogram 4 Metric Ton/Year Wuhan Fortuna Chemical Co.,Ltd Contact Supplier
High Quality 99% 2'-deoxycytidine 951-77-9 GMP Manufacturer
Cas No: 951-77-9
USD $ 0.1-0.1 / Gram 1 Gram 100 Metric Ton/Year Xi'an Xszo Chem Co., Ltd. Contact Supplier
2'-Deoxycytidine monohydrate
Cas No: 951-77-9
No Data 1 Kilogram 10 Metric Ton/Month Henan Allgreen Chemical Co.,Ltd Contact Supplier
2'-Deoxycytidine
Cas No: 951-77-9
No Data 10 Milligram Amadis Chemical Co., Ltd. Contact Supplier

951-77-9 Usage

Chemical Properties

White crystalline powder

Uses

A deoxyribonucleoside

Uses

2?-Deoxycytidine (deoxyC) is one of the deoxynucleosides which after phosphorylation to dCTP is used to synthesis DNA via various DNA polymerases or reverse transcriptases. 2?-Deoxycytidine (deoxyC) is the substrate for deoxycytidine deaminase (EC 3.5.4.14) which converts it into 2?-deoxyuridine. 2?-Deoxycytidine is phosphorylated to the nucleotide dCMP by the enzyme deoxycytidine kinase (DCK).

Definition

ChEBI: A pyrimidine 2'-deoxyribonucleoside having cytosine as the nucleobase.

General Description

2′-Deoxycytidine (deoxyC) is one of the deoxynucleosides containing cytosine as the nucleobase. It is found in the blood, feces, and urine.

Biochem/physiol Actions

2′-Deoxycytidine (deoxyC) forms dCTP upon phosphorylation which is used to synthesis DNA via various DNA polymerases or reverse transcriptases. DeoxyC is the substrate for deoxycytidine deaminase (EC 3.5.4.14) which converts it into 2′-deoxyuridine. DeoxyC is phosphorylated to the nucleotide dCMP by the enzyme deoxycytidine kinase (DCK). DeoxyC serves as a potential head and neck cancer marker.

Safety Profile

Experimental reproductive effects. Mutation data reported. When heated to decomposition it emits toxic fumes of NOx.

Purification Methods

Purify 2'-deoxycytidine by recrystallisation from MeOH/Et2O or EtOH and dry it in air. [NMR: Miles J Am Chem Soc 85 1007 1963, UV: Fox & Shugar Biochim Biophys Acta 9 369 1952.] The hydrochloride crystallises from H2O/EtOH and has m 174o(dec, 169-173o). [Walker & Butler Can J Chem 34 1168 1956.] The picrate has m 208o(dec). [Fox et al. J Am Chem Soc 83 4066 1961, Beilstein 25 III/IV 3662.]

951-77-9 Well-known Company Product Price

Brand (Code)Product description CAS number Packaging Price Detail
TCI America (D3583)  2'-Deoxycytidine  >98.0%(HPLC)(T) 951-77-9 1g 240.00CNY Detail
TCI America (D3583)  2'-Deoxycytidine  >98.0%(HPLC)(T) 951-77-9 5g 890.00CNY Detail

951-77-9SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 12, 2017

Revision Date: Aug 12, 2017

1.Identification

1.1 GHS Product identifier

Product name 2'-deoxycytidine

1.2 Other means of identification

Product number -
Other names 2'-Deoxycytidine monohydrate

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only.
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:951-77-9 SDS

951-77-9Synthetic route

4-N-picolyl-2'-deoxycytidine
78983-36-5

4-N-picolyl-2'-deoxycytidine

2'-Deoxycytidine
951-77-9

2'-Deoxycytidine

Conditions
ConditionsYield
With ammonia In water at 20℃; for 0.5h;100%
2'-deoxycytidine monohydrochloride
3992-42-5

2'-deoxycytidine monohydrochloride

2'-Deoxycytidine
951-77-9

2'-Deoxycytidine

Conditions
ConditionsYield
With Amberlite A-26 (OH- form) In water for 0.5h; Ambient temperature;99%
Multi-step reaction with 4 steps
1: pyridine
2: pyridine / 20 °C
3: 237 mg / water / methanol / 0.5 h
4: acetic acid / dioxane; H2O / 0.67 h / 20 °C / UV-irradiation
View Scheme
Multi-step reaction with 4 steps
1: pyridine
2: pyridine / 20 °C
3: 325 mg / water / methanol / 0.5 h
4: acetic acid / dioxane; H2O / 0.33 h / 20 °C / UV-irradiation
View Scheme
With triethylamine In methanol pH=7;
4-O-(2,4,6-Trimethylphenyl)-2'-deoxyuridine
130197-82-9

4-O-(2,4,6-Trimethylphenyl)-2'-deoxyuridine

A

2'-deoxyuridine
951-78-0

2'-deoxyuridine

B

2'-Deoxycytidine
951-77-9

2'-Deoxycytidine

Conditions
ConditionsYield
With ammonium hydroxide at 65℃; for 2h;A n/a
B 98%
4-methylamino-1-(β-D-2-deoxyribofuranosyl)pyrimidin-2(1H)-one
22882-02-6

4-methylamino-1-(β-D-2-deoxyribofuranosyl)pyrimidin-2(1H)-one

2'-Deoxycytidine
951-77-9

2'-Deoxycytidine

Conditions
ConditionsYield
With manganese(IV) oxide; C17H20N4O9P(1-)*Na(1+); oxygen In water; acetonitrile at 20℃; under 760.051 Torr; for 7h; Irradiation; chemoselective reaction;95%
3',5'-di-O-acetyl-2'-deoxycytidine
65919-98-4

3',5'-di-O-acetyl-2'-deoxycytidine

2'-Deoxycytidine
951-77-9

2'-Deoxycytidine

Conditions
ConditionsYield
With ammonia at 25℃;93%
With ammonia In methanol at 25℃; for 24h; Yield given;
N4-5'-O-di(triphenylmethyl)-2'-deoxycytidine

N4-5'-O-di(triphenylmethyl)-2'-deoxycytidine

2'-Deoxycytidine
951-77-9

2'-Deoxycytidine

Conditions
ConditionsYield
With ammonium cerium(IV) nitrate; silica gel In dichloromethane at 25℃; for 2h; detritylation;90%
C23H30BN3O8

C23H30BN3O8

2'-Deoxycytidine
951-77-9

2'-Deoxycytidine

Conditions
ConditionsYield
With dihydrogen peroxide In aq. phosphate buffer; dimethyl sulfoxide at 20℃; for 0.333333h; pH=7.2;88%
6-(2-Deoxy-β-D-ribosyl)tetrazolo<1,5-c>pyrimidine-5(6H)-one
108584-99-2

6-(2-Deoxy-β-D-ribosyl)tetrazolo<1,5-c>pyrimidine-5(6H)-one

2'-Deoxycytidine
951-77-9

2'-Deoxycytidine

Conditions
ConditionsYield
With hydrogen; palladium on activated charcoal In methanol for 50h;86%
2'-deoxy-4-N-acetylcytidine
380887-00-3

2'-deoxy-4-N-acetylcytidine

ammonia
7664-41-7

ammonia

2'-Deoxycytidine
951-77-9

2'-Deoxycytidine

Conditions
ConditionsYield
In methanol84.6%
N4-benzoyl-2'-deoxycytidine
4836-13-9

N4-benzoyl-2'-deoxycytidine

2'-Deoxycytidine
951-77-9

2'-Deoxycytidine

Conditions
ConditionsYield
With ethylenediamine at 40℃; for 20h;67%
With ethylenediamine; phenol at 40℃; for 20h; debenzoylation;67%
With sodium hydroxide In methanol; water for 0.0333333h; microwave irradiation;
5-Iodo-2'-deoxycytidine
611-53-0

5-Iodo-2'-deoxycytidine

diphenyldisulfane
882-33-7

diphenyldisulfane

A

5-phenylsulfanyl-2'-deoxycytidine

5-phenylsulfanyl-2'-deoxycytidine

B

2'-Deoxycytidine
951-77-9

2'-Deoxycytidine

Conditions
ConditionsYield
With [2,2]bipyridinyl; copper In N,N-dimethyl-formamide at 110℃; for 6h; Inert atmosphere; Sealed tube;A 58%
B n/a
2-deoxy–α-D-ribose 1-phosphate
17039-17-7

2-deoxy–α-D-ribose 1-phosphate

Cytosine
71-30-7

Cytosine

2'-Deoxycytidine
951-77-9

2'-Deoxycytidine

Conditions
ConditionsYield
With purine nucleoside phosphorylase at 50℃; for 20h; pH=8; aq. buffer; Enzymatic reaction;57.5%

A

α-2'-deoxycytidine
4449-40-5

α-2'-deoxycytidine

B

2'-Deoxycytidine
951-77-9

2'-Deoxycytidine

Conditions
ConditionsYield
With ammonia In methanolA 54%
B 46%
1-(3,5-O-dibenzoyl-2-deoxy-β-D-erythro-pentofuranosyl)-4-methoxy-2-pyrimidone
303041-54-5

1-(3,5-O-dibenzoyl-2-deoxy-β-D-erythro-pentofuranosyl)-4-methoxy-2-pyrimidone

2'-Deoxycytidine
951-77-9

2'-Deoxycytidine

Conditions
ConditionsYield
With ammonia In methanol at 100℃; Substitution; deacylation;50%
Cytosine
71-30-7

Cytosine

thymidine
50-89-5

thymidine

2'-Deoxycytidine
951-77-9

2'-Deoxycytidine

Conditions
ConditionsYield
With nucleoside deoxyribosyltransferase-II; sodium citrate at 40℃; for 20h; pH=6.4; Enzymatic reaction;49.8%
With sodium hydroxide; 1-(3-sulfonatopropyl)piperidine In water at 40℃; Enzymatic reaction;
5-(chloromercuri)-2'-deoxycytidine
65523-09-3

5-(chloromercuri)-2'-deoxycytidine

N,N'-Bis(trifluoroacetyl)cystamine
118042-46-9

N,N'-Bis(trifluoroacetyl)cystamine

A

5-<3-(Trifluoroacetamido)-1-thiapropyl>-2'-deoxycytidine
135638-74-3

5-<3-(Trifluoroacetamido)-1-thiapropyl>-2'-deoxycytidine

B

2'-Deoxycytidine
951-77-9

2'-Deoxycytidine

Conditions
ConditionsYield
With lithium tetrachloropalladate(II) In methanol Ambient temperature;A 5%
B n/a
N4-acetyl-O3',O5'-bis-(4-chloro-benzoyl)-2'-deoxy-cytidine
101320-23-4

N4-acetyl-O3',O5'-bis-(4-chloro-benzoyl)-2'-deoxy-cytidine

2'-Deoxycytidine
951-77-9

2'-Deoxycytidine

Conditions
ConditionsYield
With ammonia
3',5'-di-O-benzoyl-2'-deoxycytidine
20963-97-7

3',5'-di-O-benzoyl-2'-deoxycytidine

2'-Deoxycytidine
951-77-9

2'-Deoxycytidine

Conditions
ConditionsYield
With ammonium hydroxide
C53H73N21O37P6

C53H73N21O37P6

A

Phosphoric acid (2R,3S,5R)-5-(2-amino-6-hydroxy-purin-9-yl)-3-hydroxy-tetrahydro-furan-2-ylmethyl ester (S)-2,3-dihydroxy-1-(2-hydroxy-ethyl)-propyl ester
104779-62-6, 104870-73-7

Phosphoric acid (2R,3S,5R)-5-(2-amino-6-hydroxy-purin-9-yl)-3-hydroxy-tetrahydro-furan-2-ylmethyl ester (S)-2,3-dihydroxy-1-(2-hydroxy-ethyl)-propyl ester

B

2'-deoxyguanosine
961-07-9

2'-deoxyguanosine

C

2'-Deoxycytidine
951-77-9

2'-Deoxycytidine

Conditions
ConditionsYield
1.) P1 nuclease, NaOAc (pH 5.5), ZnCl2, 37 deg C, 1.5 h, 2.) alkaline phosphatase, Tris-HCl (pH 7.5), 37 deg C, 30 min; Yield given. Multistep reaction;
C53H73N21O36(18)OP6

C53H73N21O36(18)OP6

A

Cytosine
71-30-7

Cytosine

B

C15H24N5O9(18)OP

C15H24N5O9(18)OP

C

2'-deoxyguanosine
961-07-9

2'-deoxyguanosine

D

2'-Deoxycytidine
951-77-9

2'-Deoxycytidine

Conditions
ConditionsYield
1.) P1 nuclease, NaOAc (pH 5.5), ZnCl2, 37 deg C, 1.5 h, 2.) alkaline phosphatase, Tris-HCl (pH 7.5), 37 deg C, 30 min; Yield given. Multistep reaction;
C53H71(2)H2N21O37P6

C53H71(2)H2N21O37P6

A

C15H22(2)H2N5O10P

C15H22(2)H2N5O10P

B

2'-deoxyguanosine
961-07-9

2'-deoxyguanosine

C

2'-Deoxycytidine
951-77-9

2'-Deoxycytidine

Conditions
ConditionsYield
1.) P1 nuclease, NaOAc (pH 5.5), ZnCl2, 37 deg C, 1.5 h, 2.) alkaline phosphatase, Tris-HCl (pH 7.5), 37 deg C, 30 min; Multistep reaction;
2'-Deoxyguanosine
961-07-9

2'-Deoxyguanosine

2'-deoxycytidine deprotonated radical cation

2'-deoxycytidine deprotonated radical cation

A

2'-deoxyguanosine deprotonated radical cation

2'-deoxyguanosine deprotonated radical cation

B

2'-Deoxycytidine
951-77-9

2'-Deoxycytidine

Conditions
ConditionsYield
at 20℃; Rate constant; pH = 7.0;
N-Fmoc-dC
87424-19-9

N-Fmoc-dC

2'-Deoxycytidine
951-77-9

2'-Deoxycytidine

Conditions
ConditionsYield
With ammonium hydroxide In pyridine at 20℃; for 0.5h;
N4-isobutyryll-2'-deoxycytidine
110522-75-3

N4-isobutyryll-2'-deoxycytidine

A

4-methylamino-1-(β-D-2-deoxyribofuranosyl)pyrimidin-2(1H)-one
22882-02-6

4-methylamino-1-(β-D-2-deoxyribofuranosyl)pyrimidin-2(1H)-one

B

2'-Deoxycytidine
951-77-9

2'-Deoxycytidine

Conditions
ConditionsYield
With ammonia; methylamine In water at 65℃; for 1h; Product distribution; deprotection reagent;A 0.7 % Chromat.
B n/a
1-(2-Deoxy-3,5-di-O-acetyl-β-D-ribosyl)-4-chloropyrimidin-2(1H)-one
108584-97-0

1-(2-Deoxy-3,5-di-O-acetyl-β-D-ribosyl)-4-chloropyrimidin-2(1H)-one

2'-Deoxycytidine
951-77-9

2'-Deoxycytidine

Conditions
ConditionsYield
With ammonia at 50℃; for 8h; Product distribution;
C33H46N11O22P3

C33H46N11O22P3

A

2'-Deoxyguanosine
961-07-9

2'-Deoxyguanosine

B

Phosphoric acid (2R,3S,5R)-5-(4-amino-2-oxo-2H-pyrimidin-1-yl)-2-hydroxymethyl-tetrahydro-furan-3-yl ester (2R,3S)-2,3,5-trihydroxy-pentyl ester
139924-17-7

Phosphoric acid (2R,3S,5R)-5-(4-amino-2-oxo-2H-pyrimidin-1-yl)-2-hydroxymethyl-tetrahydro-furan-3-yl ester (2R,3S)-2,3,5-trihydroxy-pentyl ester

C

2'-Deoxycytidine
951-77-9

2'-Deoxycytidine

Conditions
ConditionsYield
With sodium tetrahydroborate 2) snake venom phosphodiesterase, A. P.; Yield given. Multistep reaction;
C33H46N11O22P3

C33H46N11O22P3

A

2'-Deoxyguanosine
961-07-9

2'-Deoxyguanosine

B

Phosphoric acid (2R,3S,5R)-5-(4-amino-2-oxo-2H-pyrimidin-1-yl)-2-hydroxymethyl-tetrahydro-furan-3-yl ester (2R,3S)-2,3,5-trihydroxy-pentyl ester
139924-17-7

Phosphoric acid (2R,3S,5R)-5-(4-amino-2-oxo-2H-pyrimidin-1-yl)-2-hydroxymethyl-tetrahydro-furan-3-yl ester (2R,3S)-2,3,5-trihydroxy-pentyl ester

C

2'-Deoxycytidine
951-77-9

2'-Deoxycytidine

Conditions
ConditionsYield
With sodium tetrahydroborate 2) snake venom phosphodiesterase, A. P.; Yield given. Multistep reaction;
C39H49N9O25P3(3-)

C39H49N9O25P3(3-)

A

2'-Deoxycytidine
951-77-9

2'-Deoxycytidine

B

thymidine
50-89-5

thymidine

Conditions
ConditionsYield
With alkaline phosphatase; snake venom phosphodiesterase enzymatic hydrolysis of various tetranucleosides;
C53H75N13O32P4
115173-87-0

C53H75N13O32P4

A

putrescinylthymidine
90289-35-3

putrescinylthymidine

B

2'-Deoxycytidine
951-77-9

2'-Deoxycytidine

C

thymidine
50-89-5

thymidine

Conditions
ConditionsYield
nuclease S1; VPDase (with APase) Product distribution; multistep reaction;
C53H75N13O32P4

C53H75N13O32P4

A

putrescinylthymidine
90289-35-3

putrescinylthymidine

B

2'-Deoxycytidine
951-77-9

2'-Deoxycytidine

C

thymidine
50-89-5

thymidine

Conditions
ConditionsYield
nuclease S1; VPDase (with APase) Product distribution; multistep reaction;
1,3-Dichloro-1,1,3,3-tetraisopropyldisiloxane
69304-37-6

1,3-Dichloro-1,1,3,3-tetraisopropyldisiloxane

2'-Deoxycytidine
951-77-9

2'-Deoxycytidine

2'-deoxy-3',5'-di-O-1,1,3,3-(tetraisopropyldisiloxane-1,3-diyl)cytidine
102434-71-9

2'-deoxy-3',5'-di-O-1,1,3,3-(tetraisopropyldisiloxane-1,3-diyl)cytidine

Conditions
ConditionsYield
With pyridine at 20℃;99.9%
With pyridine Ambient temperature;97%
With pyridine at 20℃; for 4h; Inert atmosphere;55%
2'-Deoxycytidine
951-77-9

2'-Deoxycytidine

2'-deoxyuridine
951-78-0

2'-deoxyuridine

Conditions
ConditionsYield
With cytidine deaminase enzyme In aq. phosphate buffer at 37℃; for 0.0833333h; pH=7; Enzymatic reaction;99%
With acetic acid; sodium nitrite
With sodium hydroxide at 90.1℃; Rate constant; Mechanism; various reagent concentration, decomposition to nonchromophoric products;
tert-butyldimethylsilyl chloride
18162-48-6

tert-butyldimethylsilyl chloride

benzoic acid anhydride
93-97-0

benzoic acid anhydride

2'-Deoxycytidine
951-77-9

2'-Deoxycytidine

N4-benzoyl-O3',O5'-bis(tert-butyldimethylsilyl)-2'-deoxycytidine
51549-38-3

N4-benzoyl-O3',O5'-bis(tert-butyldimethylsilyl)-2'-deoxycytidine

Conditions
ConditionsYield
Stage #1: tert-butyldimethylsilyl chloride; 2'-Deoxycytidine With 1H-imidazole In N,N-dimethyl-formamide at 20℃; for 4h;
Stage #2: benzoic acid anhydride In N,N-dimethyl-formamide at 160℃; for 0.25h; microwave irradiation; Further stages.;
99%
acetic anhydride
108-24-7

acetic anhydride

2'-Deoxycytidine
951-77-9

2'-Deoxycytidine

N4-acetyl-2'-deoxycytidine
32909-05-0

N4-acetyl-2'-deoxycytidine

Conditions
ConditionsYield
In N,N-dimethyl-formamide98%
In methanol for 3h; Heating;
benzoic acid anhydride
93-97-0

benzoic acid anhydride

2'-Deoxycytidine
951-77-9

2'-Deoxycytidine

N4-benzoyl-1-(3',5'-di-O-benzoyl-2'-deoxy-β-D-ribofuranosyl)-cytosine
31501-22-1

N4-benzoyl-1-(3',5'-di-O-benzoyl-2'-deoxy-β-D-ribofuranosyl)-cytosine

Conditions
ConditionsYield
With dmap; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide for 0.0177778h; microwave irradiation;98%
o-nitroiodobenzene
609-73-4

o-nitroiodobenzene

2'-Deoxycytidine
951-77-9

2'-Deoxycytidine

N6-2-nitrobenzen-1-yl-2'-deoxycytidine

N6-2-nitrobenzen-1-yl-2'-deoxycytidine

Conditions
ConditionsYield
With tetraethylammonium fluoride; 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene; tris(dibenzylideneacetone)dipalladium (0) In dimethyl sulfoxide at 20℃;98%
propionic acid anhydride
123-62-6

propionic acid anhydride

2'-Deoxycytidine
951-77-9

2'-Deoxycytidine

N4-propionyl-2'-deoxycytydine
199593-07-2

N4-propionyl-2'-deoxycytydine

Conditions
ConditionsYield
In N,N-dimethyl-formamide96%
ammonium hydroxide
1336-21-6

ammonium hydroxide

benzoyl chloride
98-88-4

benzoyl chloride

2'-Deoxycytidine
951-77-9

2'-Deoxycytidine

N4-benzoyl-2'-deoxycytidine
4836-13-9

N4-benzoyl-2'-deoxycytidine

Conditions
ConditionsYield
Stage #1: 2'-Deoxycytidine With pyridine; chloro-trimethyl-silane
Stage #2: benzoyl chloride With pyridine
Stage #3: ammonium hydroxide
96%
2-Methylpropionic anhydride
97-72-3

2-Methylpropionic anhydride

2'-Deoxycytidine
951-77-9

2'-Deoxycytidine

N4-isobutyryll-2'-deoxycytidine
110522-75-3

N4-isobutyryll-2'-deoxycytidine

Conditions
ConditionsYield
In N,N-dimethyl-formamide95%
71%
tert-butyldimethylsilyl chloride
18162-48-6

tert-butyldimethylsilyl chloride

2'-Deoxycytidine
951-77-9

2'-Deoxycytidine

2'-deoxy-3',5'-bis-O-(tert-butyldimethylsilyl)cytidine
51549-29-2

2'-deoxy-3',5'-bis-O-(tert-butyldimethylsilyl)cytidine

Conditions
ConditionsYield
With pyridine at 20℃; for 48h;95%
With 1H-imidazole In N,N-dimethyl-formamide at 20℃; for 14h;95%
With 1H-imidazole In N,N-dimethyl-formamide at 20℃; for 10h; Inert atmosphere;88%
N2-(2-oxoethyl)guanine

N2-(2-oxoethyl)guanine

2'-Deoxycytidine
951-77-9

2'-Deoxycytidine

N2-(2-oxoethyl)deoxyguanosine

N2-(2-oxoethyl)deoxyguanosine

Conditions
ConditionsYield
With trans-N-deoxyribosylase from Lactobacillus helveticus In water at 37℃; for 15h; deoxyribosylation; Enzymatic reaction;95%
2'-Deoxycytidine
951-77-9

2'-Deoxycytidine

4,4',4''-trimethoxytrityl chloride
49757-42-8

4,4',4''-trimethoxytrityl chloride

N4-(4,4',4
845306-87-8

N4-(4,4',4"-trimethoxytrityl)-2'-deoxycytidine

Conditions
ConditionsYield
With chloro-trimethyl-silane In pyridine at 20℃; for 16h;95%
Stage #1: 2'-Deoxycytidine With pyridine; chloro-trimethyl-silane at 20℃; for 2h;
Stage #2: 4,4',4''-trimethoxytrityl chloride With pyridine at 20℃; for 16h;
95%
Stage #1: 2'-Deoxycytidine With pyridine; chloro-trimethyl-silane at 20℃; for 2h;
Stage #2: 4,4',4''-trimethoxytrityl chloride With pyridine at 20℃; for 16h;
Stage #3: With ammonia In water
benzoyl chloride
98-88-4

benzoyl chloride

2'-Deoxycytidine
951-77-9

2'-Deoxycytidine

C16H18N2O6

C16H18N2O6

Conditions
ConditionsYield
With pyridine; chloro-trimethyl-silane at 0℃; Inert atmosphere;95%
butanoic acid anhydride
106-31-0

butanoic acid anhydride

2'-Deoxycytidine
951-77-9

2'-Deoxycytidine

Butyric acid (2R,3S,5R)-5-(4-butyrylamino-2-oxo-2H-pyrimidin-1-yl)-3-hydroxy-tetrahydro-furan-2-ylmethyl ester
145355-76-6

Butyric acid (2R,3S,5R)-5-(4-butyrylamino-2-oxo-2H-pyrimidin-1-yl)-3-hydroxy-tetrahydro-furan-2-ylmethyl ester

Conditions
ConditionsYield
In tetrahydrofuran at 60℃; for 6h; Candida antarctica lipase (SP435);94%
2,2-dimethoxy-1-methylpyrrolidine
39650-82-3

2,2-dimethoxy-1-methylpyrrolidine

2'-Deoxycytidine
951-77-9

2'-Deoxycytidine

4-N-(N-methylpyrrolidin-2-ylidene)-2’-deoxycytidine
98533-08-5

4-N-(N-methylpyrrolidin-2-ylidene)-2’-deoxycytidine

Conditions
ConditionsYield
In methanol for 1h;94%
In methanol at 20℃; for 3h; Inert atmosphere;85%
N,N-diisopropylformamide dimethyl acetal
19449-28-6

N,N-diisopropylformamide dimethyl acetal

2'-Deoxycytidine
951-77-9

2'-Deoxycytidine

N4-<(diisopropylamino)methylene>-2'-deoxycytidine

N4-<(diisopropylamino)methylene>-2'-deoxycytidine

Conditions
ConditionsYield
In N,N-dimethyl-formamide for 8h; Ambient temperature;93%
phenyl isocyanate
103-71-9

phenyl isocyanate

2'-Deoxycytidine
951-77-9

2'-Deoxycytidine

2'-deoxy-N4-[(phenylamino)carbonyl]cytidine
219582-35-1

2'-deoxy-N4-[(phenylamino)carbonyl]cytidine

Conditions
ConditionsYield
With triethylamine In N,N-dimethyl-formamide at 20℃; for 0.5h;92%
1-(p-nitrophenylethoxycarbonyl)-benzotriazole
88091-66-1

1-(p-nitrophenylethoxycarbonyl)-benzotriazole

2'-Deoxycytidine
951-77-9

2'-Deoxycytidine

2'-deoxy-N4-{[2-(4-nitrophenyl)ethoxy]carbonyl}cytidine
88091-67-2

2'-deoxy-N4-{[2-(4-nitrophenyl)ethoxy]carbonyl}cytidine

Conditions
ConditionsYield
In N,N-dimethyl-formamide at 60℃; for 15h;91%
In N,N-dimethyl-formamide at 60℃;90%
tert-butyldimethylsilyl chloride
18162-48-6

tert-butyldimethylsilyl chloride

2'-Deoxycytidine
951-77-9

2'-Deoxycytidine

β-D-5'-O-tert-butyldimethylsilyl-2'-deoxycytidine
51549-27-0

β-D-5'-O-tert-butyldimethylsilyl-2'-deoxycytidine

Conditions
ConditionsYield
With 1H-imidazole In N,N-dimethyl-formamide at 20℃;91%
2'-Deoxycytidine
951-77-9

2'-Deoxycytidine

5-bromo-2'-deoxycytidine
1022-79-3

5-bromo-2'-deoxycytidine

Conditions
ConditionsYield
With N-Bromosuccinimide; acetic acid at 20℃; for 0.333333h;90%
With 1-(2-methoxyethyl)-3-methylimidazolium trifluoroacetate; N-Bromosuccinimide at 25℃; for 0.5h;85%
With bromine In pyridine; tetrachloromethane at 22℃; for 12h;72%
n-hexanoic anhydride
2051-49-2

n-hexanoic anhydride

2'-Deoxycytidine
951-77-9

2'-Deoxycytidine

Hexanoic acid (2R,3S,5R)-5-(4-hexanoylamino-2-oxo-2H-pyrimidin-1-yl)-3-hydroxy-tetrahydro-furan-2-ylmethyl ester
145355-77-7

Hexanoic acid (2R,3S,5R)-5-(4-hexanoylamino-2-oxo-2H-pyrimidin-1-yl)-3-hydroxy-tetrahydro-furan-2-ylmethyl ester

Conditions
ConditionsYield
In tetrahydrofuran at 60℃; for 12h; Candida antarctica lipase (SP435);90%
N,N-dibutylformamide dimethyl acetal
19449-30-0

N,N-dibutylformamide dimethyl acetal

2'-Deoxycytidine
951-77-9

2'-Deoxycytidine

4-N-((di-n-butylamino)methylene)-2'-deoxycytidine
98533-10-9

4-N-((di-n-butylamino)methylene)-2'-deoxycytidine

Conditions
ConditionsYield
In methanol for 2h;90%
pentafluorophenyl benzoate
1548-84-1

pentafluorophenyl benzoate

2'-Deoxycytidine
951-77-9

2'-Deoxycytidine

N4-benzoyl-2'-deoxycytidine
4836-13-9

N4-benzoyl-2'-deoxycytidine

Conditions
ConditionsYield
In pyridine at 80℃; for 5h;90%
di-tert-butylsilyl bis(trifluoromethanesulfonate)
85272-31-7

di-tert-butylsilyl bis(trifluoromethanesulfonate)

2'-Deoxycytidine
951-77-9

2'-Deoxycytidine

3',5'-O-(Di-tert-butylsilanediyl)deoxycytidine
97219-08-4

3',5'-O-(Di-tert-butylsilanediyl)deoxycytidine

Conditions
ConditionsYield
90%
N,N-dimethyl-formamide dimethyl acetal
4637-24-5

N,N-dimethyl-formamide dimethyl acetal

2'-Deoxycytidine
951-77-9

2'-Deoxycytidine

N4-<(dimethylamino)methylene>-2'-deoxycytidine
17331-11-2

N4-<(dimethylamino)methylene>-2'-deoxycytidine

Conditions
ConditionsYield
In N,N-dimethyl-formamide for 8h; Ambient temperature;90%
In methanol Ambient temperature; Yield given;
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