Reaction vial made out of sintered silicon carbide (CAS 409-21-2) (SiC) for performing microwave chemistry under single-mode conditions
Sintered silicon carbide: A new ceramic vessel material for microwave chemistry in single-mode reactors
Figure 1
For the experiments described in this work, a 10 mL reaction vial made out of sintered SiC of the exact same geometry as a standard micro-wave-transparent Pyrex process vial was used (Figure 1). As with the standard Pyrex vial, the SiC vessel can be fitted with a thermoplastic snap cap and PTFE-coated silicone septa to allow microwave processing up to 300℃ and 30 bar pressure (Figure 1).
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