Journal of the Chemical Society, Dalton Transactions p. 451 - 456 (1987)
Update date:2022-08-06
Topics:
Elrington, Margaret
Greenwood, Norman N.
Kennedy, John D.
Thornton-Pett, Mark
Reaction of Na2a 10percent yield of the lemon-yellow air-stable covalent complex <(PMe2Ph)3RuB12H12>, characterized by elemental analysis and multielement nuclear magnetic single- and multiple-resonance spectroscopy.Reaction of a = 2 246.3(2), b = 1 189.2(2), c = 1 972.5(2) pm, β = 111.04(1) deg, Z = 4, an space group P21/n.The compounds may formally be regarded either as ruthenium(II) complexes of closo-dodecaboranyl ligands which bind in a trihapto tridentate mode to the octahedral metal centres via three two-electron three-centre B-H-Ru bridge bonds, or as 13-vertex pileo 2n-electron metallaborane cluster species which have capped closed deltahedral cluster geometries.
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