Tetrahedron p. 3241 - 3250 (1988)
Update date:2022-08-04
Topics:
Tanaka, Kiyoshi
Chen, Xing
Yoneda, Fumio
5-Arylidene-1,3-dimethylbarbituric acid derivatives, such as 1a and 1b, effectively oxidized both alkane- and benzenethiols to disulfides under neutral condition with concomitant formation of the dihydro compounds (2a) and (2b).Thiol adduct of the dihydro compound was prepared as a stable compound and successfully applied to the synthesis of unsymmetrical disulfide under mild condition in excellent yield.Mechanistic consideration for the oxidation was also described briefly.
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Doi:10.1055/s-0029-1216844
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