Angewandte Chemie - International Edition p. 7607 - 7610 (2011)
Update date:2022-08-03
Topics:
Ghereg, Dumitru
Ladeira, Sonia
Saffon, Nathalie
Escudie, Jean
Gornitzka, Heinz
A highly reactive phosphagermacarbene (PGeHC) was synthesized by [3+2] cycloaddition between phosphagermaallene Tip(tBu)GeiCiPMes* (Tip= 2,4,6-triisopropylphenyl; Mes=2,4,6-tris-tert-butylphenyl) and diphenylketene. It forms complexes with [{Rh(CO)2Cl}2] and Me3P, and undergoes a Wittig-type reaction with diphenylketene (see scheme). Copyright
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