Tetrahedron Letters p. 6143 - 6146 (1993)
Update date:2022-07-30
Topics: Rearrangement squalestatins
Chan, Chuen
Inglis, Graham Ga
Procopiou, Panayiotis A.
Ross, Barry C.
Srikantha, Anton Rp
Watson, Nigel S.
3-Decarboxy squalestatins 3 and 4 were synthesised via photolysis of t-butyl peroxyester 7. Lactol 10 was isolated unexpectedly from both HCl-dioxan cleavage of 8, a by-product of the photolysis, and attempted Barton decarboxylation of 6. In TFA under anh
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