Synthesis of Allenyl- and Alkynyl-stannanes by Reduction of Allenyl- and Alkynyl-chlorostannanes

DOI: 10.1039/c39950000699

Source and publish data:

Journal of the Chemical Society. Chemical communications p. 699 - 700 (1995)

Update date:2022-08-04

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Authors:

Lassalle, Laurent

Janati, Tajdine

Guillemin, Jean-Claude

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Article abstract of DOI:10.1039/c39950000699

Allenyl- 1a, b and alkynyl-stannanes 2a-c are synthesized by reaction of the corresponding allenyl- and alkynyl-tributylstannanes with tin tetrachloride or dichlorodimethylstannane followed by a chemoselective reduction of the formed chlorostannanes with tributylstannane in the presence of duroquinone or galvinoxyl, a radical inhibitor.

Full text of DOI:10.1039/c39950000699

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