Tetrahedron Letters p. 5649 - 5652 (1996)
Update date:2022-08-03
Topics:
Crimmins, Michael T.
Rafferty, Stephen W.
Lewis acid-promoted triethylsilane reduction of 6,6-spiroketal alcohols produces cis-2,6-disubstituted tetrahydropyrans with excellent regioselectivity and stereocontrol. An appended alcohol allows bidentate coordination of the Lewis acid to selectively activate one C-O bond of the anomeric center toward reductive cleavage.
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Doi:10.1039/b718462j
(2008)Doi:10.1016/0022-328X(96)06383-8
(1996)Doi:10.1002/hlca.19680510715
(1968)Doi:10.1016/0957-4166(96)00381-3
(1996)Doi:10.1080/00397919708004803
(1997)Doi:10.1002/cber.19961291014
(1996)