Inorganica Chimica Acta p. 237 - 241 (1998)
Update date:2022-09-26
Topics:
Wendt, Ola F.
Scodinu, Alessandra
Elding, Lars I.
Crystals of cis-[PtCl2(SbPh3)2] (1) are monoclinic, space group P21/a with a=20.5708(12), b=10.1942(4), c=33.3984(15) A, β=94.394(4)° and Z= 8. Substitution of chloride for iodide yields trans-[Ptl2(SbPh3)2] (2), the crystals of which are monoclinic, space group P21/c with a=18.108(4), b=10.102(2), c=19.115(5) A, β=95.241(16)° and Z=4. The average Pt-Cl distance in 1 is 2.338(12) A, implying a trans influence of triphenyl stibine comparable with that of triphenyl phosphine, as opposed to what has been reported earlier. IR and Raman data for 1 and 2 are reported and discussed.
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