Synthesis of L-[4,5,5,5-D4]isoleucine: Determination of approximate rotamer population about the Cβ-Cγ bond

DOI: 10.1002/jlcr.439

Source and publish data:

Journal of labelled compounds and radiopharmaceuticals p. 141 - 147 (2001)

Update date:2022-08-05

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Authors:

Oba Oba

Miyakawa

Shionoya

Nishiyama

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Article abstract of DOI:10.1002/jlcr.439

An asymmetric synthesis of regio- and stereoselectively deuteriumlabelled L-isoleucine was examined. An unsaturated γ-lactam readily available from L-pyroglutamic acid was stereoselectively methylated by the Gilman reagent and subsequent oxidation of the

Full text of DOI:10.1002/jlcr.439

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