Synthesis, purification and spectral analysis of mononitrocyclopentapyrenes

DOI: 10.1002/recl.19871061205

Source and publish data:

Recueil des Travaux Chimiques des Pays-Bas p. 628 - 640 (1987)

Update date:2022-08-02

Topics:

Authors:

Braken-van Leersum, A. M. van den

Spijker, N. M.

Lugtenburg, J.

Cornelisse, J.

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Article abstract of DOI:10.1002/recl.19871061205

The synthesis ,purification and characterization of seven isomeric nitrocyclopentapyrenes (nitroCPPs) are described.Nitration of partially hydrogenated CPPs affords mixtures of nitroderivatives, which, after separation, are aromatized with DDQ.The resulting nitroCPPS are characterized by their 1H NMR, 13C NMR, UV-vis, IR and mass spectra.The interaction between the nitro group and the aromatic system of CPP is discussed.

Full text of DOI:10.1002/recl.19871061205

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