Tetrahedron Letters p. 681 - 684 (1984)
Update date:2022-07-30
Topics:
Cruickshank, Kenneth A.
Jiricny, Josef
Reese, Colin B.
Uracil and thymine react with benzoyl chloride in acetonitrile-pyridine solution at room temperature to give first their 1-N-benzoyl (2b and 3b) and then their 1-N,3-N-dibenzoyl derivatives (4a and 4b, respectively); the latter compounds are converted into the corresponding 3-N-benzoyl derivatives (5a and 6a) under mild conditions of basic hydrolysis.
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