Phosphorus, Sulfur and Silicon and the Related Elements p. 1865 - 1870 (2003)
Update date:2022-08-17
Topics:
Lakouraj
Tajbakhsh
Khojasteh
Mild and efficient method for deprotection of silyl ethers to alcohols is described using Caro's acid supported on silica gel. Reactions are carried out in dichloromethane at room temperature and their parent hydroxy compounds obtained in good to excellent yields. Using this procedure, tetrahydropyranyl ethers (THP) remain intact during desilylation reaction.
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