Tetrahedron p. 7243 - 7250 (1999)
Update date:2022-08-17
Topics:
Billard, Thierry
Greiner, Alfred
Langlois, Bernard R.
The solution of sodium trifluoromethanesulfinate (sodium 'triflinate' and phosphoryl chloride (2/1), in AcOEt, behaves like an equivalent of the CF3S(O)+ cation. It can be used in situ to prepare trifluoromethanesulfinates (CF3S(O)OR) or trifluoromethanesulfinamides (CF3S(O)NHR) at room temperature from alcohols or amines, respectively.
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