Chemistry Letters p. 646 - 647 (2001)
Update date:2022-08-16
Topics:
Kitamura, Masanori
Shen, Baojian
Liu, Yanjun
Zheng, Hegen
Takahashi, Tamotsu
Aromatization of highly alkyl-substituted dihydroanthracene was performed with the n-BuLi/TMEDA/MeI. Treatment of 1,2,3,4,5,6,7,8-octapropyl-9, 10-dihydroanthracene with 2.2 equiv of n-BuLi, TMEDA at 50 °C in hexane for 3 h, followed by 1.1 equiv of MeI at room temperature for 1 h gave the corresponding anthracene in 98% yield.
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