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18) Multiple attempts to monitor the reaction at 145 °C using the
3
̈
internal olefin cyclohexene were unsuccessful. Attempts to alter the
̈
reaction conditions by scale or by vessel resulted in inconsistent and
̈
10
poor yields (ca. <10%). Attempts to use d -o-xylenes and monitor the
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reaction at 140 °C by H NMR spectroscopy resulted in poor yields
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