Tetrahedron Asymmetry p. 1053 - 1062 (1991)
Update date:2022-08-11
Topics:
McIntosh, John M.
Cassidy, Kenneth C.
Dissolving metal reduction of known enone 5 affords predominantly the racemic form of the title ketone (3) whereas catalytic reduction gives the meso isomer 6.Neither ketone 3 nor alcohol 4 could be satisfactorily resolved.Asymmetric synthesis of (-)-3 and (+)-4 (ee=91percent) was effected from ketone (+)-13.
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