Journal fur Praktische Chemie - Chemiker-Zeitung p. 37 - 40 (1992)
Update date:2022-08-22
Topics:
Ye, Siyu
Beck, F.
Norcamphor (1) was anodically oxidized at Pb/PbO2 anodes in 1 M*H2SO4, MeCN/H2O (V/V = 1/1). 3-Oxocyclopentaneacetic acid (3) and oxabicyclo<3.3.0>octan-3-one (4) were obtained with material yields up to 76percent and 42percent, respectively.The effects of electrode materials, current densities and concentrations were studied.A possible anodic oxidation mechanism was proposed.
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