Journal of Fluorine Chemistry p. 637 - 648 (1982)
Update date:2022-08-30
Topics:
Dolbier, William R.
Burkholder, Conrad R.
Piedrahita, Carlos A.
Improved syntheses of 1-fluoropropadiene and 1,1-difluoropropadiene are presented as is the synthesis of a third reactive allene, 1,1-difluoro-3-methyl-1,2-butadiene.Gram quantities of these highly reactive fluorinated allenes may be prepared conveniently in high yield and purity.All three are reactive dienophiles and cycloadd regiospecifically using their non-fluorine-substituted double bonds.
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