Russian Journal of Physical Chemistry p. 807 - 811 (2015)
Update date:2022-08-11
Topics:
Mondieig
Negrier
Leger
Lakhrissi
El Assyry
Lakhrissi
Essassi
Benali
Boucetta
The synthesis and the crystal structure of the N-isopropenylbenzimidazolone (C10H10N2O) are presented. The synthesis was performed by Meth-Cohen method by reaction of o-phenylenediamine with ethyl acetoacetate in refluxed xylene. The single crystal structure was determined at room temperature by means of X-rays diffraction. The crystal system is monoclinic, with space group C2/c and eight molecules per unit cell. The unit cell dimensions are: a = 15.978(1) ?, b = 6.100(2) ?, c = 18.222(2) ?, β = 90.16(1)° and V = 1776.0(6) ?3.
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(1943)