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Product FOB Price Min.Order Supply Ability Supplier
Butyldiglycol 112-34-5
Cas No: 112-34-5
USD $ 200.0-200.0 / Gram 1 Gram 100 Metric Ton/Month Henan Tianfu Chemical Co., Ltd. Contact Supplier
High quality 2-(2-Butoxyethoxy)Ethanol supplier in China
Cas No: 112-34-5
No Data 1 Metric Ton 30 Metric Ton/Month Simagchem Corporation Contact Supplier
High purity 112-34-5 Diethylene Glycol Butyl ether
Cas No: 112-34-5
USD $ 100.0-500.0 / Gram 1 Gram 99999 Gram/Year Hangzhou Dingyan Chem Co., Ltd Contact Supplier
2-(2-Butoxyethoxy)ethanol
Cas No: 112-34-5
USD $ 1.0-3.0 / Kilogram 1 Kilogram 10 Kilogram/Day Hebei yanxi chemical co.,LTD. Contact Supplier
Diethylene Glycol Monobutyl Ether (DEB)
Cas No: 112-34-5
USD $ 1.0-1.0 / Metric Ton 1 Metric Ton 5000 Metric Ton/Year Hefei TNJ chemical industry co.,ltd Contact Supplier
Factory price Cosmetic BUTOXYDIGLYCOL 112-34-5 Manufacturer
Cas No: 112-34-5
USD $ 0.1-0.1 / Gram 1 Gram 100 Metric Ton/Year Xi'an Xszo Chem Co., Ltd. Contact Supplier
Butyldiglycol
Cas No: 112-34-5
No Data 100 Gram 20 Metric Ton/Month Henan Allgreen Chemical Co.,Ltd Contact Supplier
Factory Supply 2-(2-butoxyethoxy)ethanol
Cas No: 112-34-5
No Data 1 1 Ality Chemical Corporation Contact Supplier
trihexadecyl(methyl)ammonium chloride
Cas No: 112-34-5
No Data 10 Milligram Amadis Chemical Co., Ltd. Contact Supplier
Butyldiglycol Manufacturer/High quality/Best price/In stock
Cas No: 112-34-5
USD $ 3.0-3.0 / Kilogram 1 Kilogram 1-100 Metric Ton/Month Dayang Chem (Hangzhou) Co.,Ltd. Contact Supplier

112-34-5 Usage

Reactivity Profile

Butyldiglycol is a ether-alcohol derivative. The ether being relatively unreactive. Flammable and/or toxic gases are generated by the combination of alcohols with alkali metals, nitrides, and strong reducing agents. They react with oxoacids and carboxylic acids to form esters plus water. Oxidizing agents convert alcohols to aldehydes or ketones. Alcohols exhibit both weak acid and weak base behavior. They may initiate the polymerization of isocyanates and epoxides.

General Description

Colorless liquid with a mild pleasant odor. Mixes with water.

Uses

Solvent.

Chemical Properties

Diethylene glycol monobutyl ether is a colorless, high-boiling liquid with a mild odour. It is miscible in proportions with water, alcohol (methanol), ketones (acetone), ethers (ethyl ether), aromatic hydrocarbons (benzene), paraffinic hydrocarbons (n-heptane), and halogenated hydrocarbons (carbon tetrachloride). As it is an ether-alcohol type compound it possesses solvent action for many substances such as oils, dyes, gums, and natural and synthetic resins. It is used as a high-boiling solvent in nitrocellulose lacquers and other synthetic coatings, baking lacquers, flash-dry printing inks, and dye bath.

Safety Profile

Moderately toxic by ingestion and intraperitoneal routes. Mddly toxic by skin contact. A severe eye irritant. Combustible when exposed to heat or flame; can react with oxidizing materials. To fight fire, use alcohol foam, CO2, or dry chemical. When heated to decomposition it emits acrid smoke and irritating fumes. See also GLYCOL ETHERS.

Chemical Reactivity

Reactivity with Water No reaction; Reactivity with Common Materials: No reaction; Stability During Transport: Stable; Neutralizing Agents for Acids and Caustics: Not pertinent; Polymerization: Not pertinent; Inhibitor of Polymerization: Not pertinent.

Contact allergens

This organic solvent belongs to the carbitols group and is included in waterbased liquids such as paints, surface cleaners, polishes, and disinfectants. It is considered to be an exceptional allergen.

Uses

Diethylene glycol monobutyl ether (DGBE)is used as a solvent for cellulose ester,lacquers, varnishes, and dyes; as a primarycomponent of the aqueous film-forming foam that is used by the U.S. Navy in shipboardfirefighting systems (Hobson et al. 1987).

Health Hazard

DGBE showed low toxicity in test species.Toxic symptoms are similar to those ofother glycol ethers containing two etherealoxygen atoms. The routes of entry into thebody are ingestion and absorption throughthe skin. Hobson and coworkers (1987)investigated the subchronic oral toxicity ofDGBE in rats. The toxic effects observedwere lowering of food consumption, elevatedliver and spleen weights, lowered redblood cell counts and lymphocyte counts,and a dose-related decrease in corpuscularhemoglobin concentration. The high dosescaused pulmonary congestion. No renaldamage was reported.LD50 value, oral (guinea pigs): 2000 mg/kgDGBE is an eye irritant. There is no reporton teratogenicity of this compound.

Purification Methods

Dry the ether with anhydrous K2CO3 or CaSO4, filter and fractionally distil it. Peroxides can be removed by refluxing with stannous chloride or a mixture of FeSO4 and KHSO4 (or, less completely, by filtration under slight pressure through a column of activated alumina). [Beilstein 1 IV 2394.]

Waste Disposal

DGBE is mixed with a combustible solventand burned in a chemical incinerator. Smallamounts may be disposed down the drainwith large amounts of water.

Health Hazard

Inhalation for brief periods has no significant effect. Contact with liquid causes moderate irritation of eyes and corneal injury. Prolonged contact with skin causes only minor irritation.

Fire Hazard

Butyldiglycol is combustible.

Air & Water Reactions

Oxidizes readily in air to form unstable peroxides that may explode spontaneously [Bretherick, 1979 p.151-154, 164]. Water soluble.
InChI:InChI=1/C8H18O.C4H10O3/c1-3-5-7-9-8-6-4-2;5-1-3-7-4-2-6/h3-8H2,1-2H3;5-6H,1-4H2

112-34-5 Well-known Company Product Price

Brand (Code)Product description CAS number Packaging Price Detail
Alfa Aesar (A16068)  Diethylene glycol mono-n-butyl ether, 99%    112-34-5 1000ml 408.0CNY Detail
Alfa Aesar (A16068)  Diethylene glycol mono-n-butyl ether, 99%    112-34-5 5000ml 972.0CNY Detail
Sigma-Aldrich (03351)  Diethyleneglycolmonobutylether  for surfactant analysis, ≥99.0% 112-34-5 03351-1L 1,764.36CNY Detail

112-34-5SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 10, 2017

Revision Date: Aug 10, 2017

1.Identification

1.1 GHS Product identifier

Product name Butyldiglycol

1.2 Other means of identification

Product number -
Other names 2-(2-butoxyethoxy)ethanol

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only. Solvents
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:112-34-5 SDS

112-34-5Synthetic route

oxirane
75-21-8

oxirane

butan-1-ol
71-36-3

butan-1-ol

A

2-Butoxyethanol
111-76-2

2-Butoxyethanol

B

Diethylene glycol monobutyl ether
112-34-5

Diethylene glycol monobutyl ether

Conditions
ConditionsYield
With potassium aluminum sulfate at 170℃; for 24h; Reagent/catalyst; Autoclave;A 93.1%
B 6.63%
n-Butyl chloride
109-69-3

n-Butyl chloride

diethylene glycol
111-46-6

diethylene glycol

Diethylene glycol monobutyl ether
112-34-5

Diethylene glycol monobutyl ether

Conditions
ConditionsYield
With sodium hydroxide; water at 100℃; for 24h;70%
oxirane
75-21-8

oxirane

butan-1-ol
71-36-3

butan-1-ol

Diethylene glycol monobutyl ether
112-34-5

Diethylene glycol monobutyl ether

Conditions
ConditionsYield
With boron trifluoride diethyl etherate at 50℃;
butan-1-ol
71-36-3

butan-1-ol

diethylene glycol
111-46-6

diethylene glycol

Diethylene glycol monobutyl ether
112-34-5

Diethylene glycol monobutyl ether

Conditions
ConditionsYield
sulfuric acid In toluene Heating;
1-bromo-butane
109-65-9

1-bromo-butane

sodium diethylene glycolate

sodium diethylene glycolate

Diethylene glycol monobutyl ether
112-34-5

Diethylene glycol monobutyl ether

Conditions
ConditionsYield
With diethylene glycol
oxirane
75-21-8

oxirane

butan-1-ol
71-36-3

butan-1-ol

A

2-Butoxyethanol
111-76-2

2-Butoxyethanol

B

Diethylene glycol monobutyl ether
112-34-5

Diethylene glycol monobutyl ether

C

triethyleneglycol monobutyl ether
143-22-6

triethyleneglycol monobutyl ether

Conditions
ConditionsYield
2,4,6-trimethyl-pyridine at 160℃; under 2311.54 - 3345.86 Torr; for 2.5h; Product distribution / selectivity; Inert atmosphere;
sodium butanolate at 140℃; under 7500.75 Torr; for 5h; Product distribution / selectivity;A 20.16 %Chromat.
B 9.07 %Chromat.
C 6.10 %Chromat.
catalyst of invention (Sb2O3, copper acetate, hydrogen peroxide; calcined) at 140℃; under 30003 Torr; for 24 - 120h; Product distribution / selectivity;A 76 - 77 %Chromat.
B 13 - 14 %Chromat.
C 9 %Chromat.
pyrene
129-00-0

pyrene

A

phthalic anhydride
85-44-9

phthalic anhydride

B

xanth-9-one
90-47-1

xanth-9-one

C

pentadecane
629-62-9

pentadecane

D

n-docosane
629-97-0

n-docosane

E

n-hexacosane
630-01-3

n-hexacosane

F

tetradecane
629-59-4

tetradecane

G

Hexadecane
544-76-3

Hexadecane

H

Diethylene glycol monobutyl ether
112-34-5

Diethylene glycol monobutyl ether

I

n-butyl isobutyrate
97-87-0

n-butyl isobutyrate

J

heneicosane
629-94-7

heneicosane

K

n-tricosane
638-67-5

n-tricosane

L

tetracosane
646-31-1

tetracosane

M

n-pentacosane
629-99-2

n-pentacosane

N

cyclopenta[def]phenanthrene
203-63-4

cyclopenta[def]phenanthrene

O

1,2-benzenedicarboxylic acid diisooctyl ether

1,2-benzenedicarboxylic acid diisooctyl ether

P

2,6-di-tert-butyl-4-methyl-phenol
128-37-0

2,6-di-tert-butyl-4-methyl-phenol

Q

Diethyl phthalate
84-66-2

Diethyl phthalate

R

Phthalic acid dibutyl ester
84-74-2

Phthalic acid dibutyl ester

S

4H-Cyclopenta[def]phenanthrene
203-64-5

4H-Cyclopenta[def]phenanthrene

T

benzyl n-butyl phthalate
85-68-7

benzyl n-butyl phthalate

U

1,1'-Biphenyl-2,2',6,6'-tetracarboxaldehyde
4371-26-0

1,1'-Biphenyl-2,2',6,6'-tetracarboxaldehyde

V

4,5-phenanthrene-8,9-dicarbaldehyde
16162-34-8

4,5-phenanthrene-8,9-dicarbaldehyde

W

1-hexadecylcarboxylic acid
57-10-3

1-hexadecylcarboxylic acid

X

6-propyltridecane

6-propyltridecane

Conditions
ConditionsYield
With oxygen; ozone In water for 0.25 - 2h;
Tetraethylene glycol
112-60-7

Tetraethylene glycol

ethylene glycol
107-21-1

ethylene glycol

butyraldehyde
123-72-8

butyraldehyde

diethylene glycol
111-46-6

diethylene glycol

2,2'-[1,2-ethanediylbis(oxy)]bisethanol
112-27-6

2,2'-[1,2-ethanediylbis(oxy)]bisethanol

A

2-propyl-1,3-dioxolane
3390-13-4

2-propyl-1,3-dioxolane

B

2-Butoxyethanol
111-76-2

2-Butoxyethanol

C

Diethylene glycol monobutyl ether
112-34-5

Diethylene glycol monobutyl ether

D

triethyleneglycol monobutyl ether
143-22-6

triethyleneglycol monobutyl ether

E

tetraethylene glycol monobutyl ether
1559-34-8

tetraethylene glycol monobutyl ether

F

butan-1-ol
71-36-3

butan-1-ol

Conditions
ConditionsYield
With hydrogen; palladium 10% on activated carbon at 180℃; under 51716.2 Torr; for 2h;
butyraldehyde
123-72-8

butyraldehyde

diethylene glycol
111-46-6

diethylene glycol

Diethylene glycol monobutyl ether
112-34-5

Diethylene glycol monobutyl ether

Conditions
ConditionsYield
With hydrogen; palladium 10% on activated carbon at 200℃; under 51716.2 Torr; for 2h; Inert atmosphere;94.5 %Chromat.
With palladium 10% on activated carbon; hydrogen at 200℃; under 51755.2 Torr; for 2h;94.5 %Chromat.
Diethylene glycol monobutyl ether
112-34-5

Diethylene glycol monobutyl ether

p-toluenesulfonyl chloride
98-59-9

p-toluenesulfonyl chloride

diethylene glycol monobutyl ether tosylate
50964-16-4

diethylene glycol monobutyl ether tosylate

Conditions
ConditionsYield
Stage #1: Diethylene glycol monobutyl ether; p-toluenesulfonyl chloride With dmap In dichloromethane at 20℃;
Stage #2: With triethylamine In dichloromethane at 20℃;
100%
With sodium hydroxide In tetrahydrofuran; water at 0℃; for 2h;85%
With pyridine In dichloromethane at 20℃; for 3h;57%
With pyridine
Diethylene glycol monobutyl ether
112-34-5

Diethylene glycol monobutyl ether

2-hexyldecanoic acid
25354-97-6

2-hexyldecanoic acid

2-(2-butoxyethoxy)ethyl 2-hexyldecanoate

2-(2-butoxyethoxy)ethyl 2-hexyldecanoate

Conditions
ConditionsYield
With p-toluenesulfonic acid monohydrate99%
With p-toluenesulfonic acid monohydrate99%
Diethylene glycol monobutyl ether
112-34-5

Diethylene glycol monobutyl ether

Methyl decanoate
110-42-9

Methyl decanoate

1-Decanol
112-30-1

1-Decanol

Conditions
ConditionsYield
With sodium borohydrid In 5,5-dimethyl-1,3-cyclohexadiene98%
Diethylene glycol monobutyl ether
112-34-5

Diethylene glycol monobutyl ether

2-Bromoacetyl bromide
598-21-0

2-Bromoacetyl bromide

2-(2-butoxyethoxy)ethyl 2-bromoacetate
56521-78-9

2-(2-butoxyethoxy)ethyl 2-bromoacetate

Conditions
ConditionsYield
With sodium carbonate In dichloromethane at -5 - 20℃; for 12h; Green chemistry;98%
With triethylamine In dichloromethane at -78℃; Inert atmosphere;72%
Diethylene glycol monobutyl ether
112-34-5

Diethylene glycol monobutyl ether

acrylonitrile
107-13-1

acrylonitrile

3-[2-(2-butoxyethoxy)ethoxy]propanenitrile
35633-48-8

3-[2-(2-butoxyethoxy)ethoxy]propanenitrile

Conditions
ConditionsYield
With sodium methylate for 1.16667h;97%
Adipic acid
124-04-9

Adipic acid

2-(2-methoxyethoxy)ethyl alcohol
111-77-3

2-(2-methoxyethoxy)ethyl alcohol

Diethylene glycol monobutyl ether
112-34-5

Diethylene glycol monobutyl ether

methyldiglycol butyldiglycol adipate

methyldiglycol butyldiglycol adipate

Conditions
ConditionsYield
toluene-4-sulfonic acid In toluene at 118 - 145℃; for 6.5h; Heating / reflux;96.9%
Diethylene glycol monobutyl ether
112-34-5

Diethylene glycol monobutyl ether

paracetaldehyde
123-63-7

paracetaldehyde

2-butoxyethyl 2-ethoxyethyl ether
3895-17-8

2-butoxyethyl 2-ethoxyethyl ether

Conditions
ConditionsYield
With hydrogen; palladium on activated charcoal at 160℃; under 760 Torr; for 18h; Etherification;96%
With hydrogen; palladium on activated charcoal at 160℃; for 10h; atmospheric pressure;96%
Diethylene glycol monobutyl ether
112-34-5

Diethylene glycol monobutyl ether

1-[2-(2-chloroethoxy)-ethoxy]butane
1120-23-6

1-[2-(2-chloroethoxy)-ethoxy]butane

Conditions
ConditionsYield
With pyridine; thionyl chloride In chloroform for 10h; Reflux;95%
With pyridine; thionyl chloride
Diethylene glycol monobutyl ether
112-34-5

Diethylene glycol monobutyl ether

Octanal
124-13-0

Octanal

2-butoxyethyl 2-(octoxy)ethyl ether
101433-27-6

2-butoxyethyl 2-(octoxy)ethyl ether

Conditions
ConditionsYield
With hydrogen; palladium on activated charcoal at 160℃; under 760 Torr; for 18h; Etherification;95%
With hydrogen; palladium on activated charcoal at 160℃; for 10h; atmospheric pressure;95%
Diethylene glycol monobutyl ether
112-34-5

Diethylene glycol monobutyl ether

Acetic formic anhydride
2258-42-6

Acetic formic anhydride

2-(2-butoxyethoxy)ethyl formate

2-(2-butoxyethoxy)ethyl formate

Conditions
ConditionsYield
With pyridine 1.) 0 deg C, 5 h, 2.) rt, 12 h;90%
Diethylene glycol monobutyl ether
112-34-5

Diethylene glycol monobutyl ether

C38H74N6O10

C38H74N6O10

Conditions
ConditionsYield
Stage #1: Diethylene glycol monobutyl ether; Hexamethylene diisocyanate; dibutyltin dilaurate In hexane at 20 - 45℃;
Stage #2: trans-1,2-Diaminocyclohexane In hexane at 15 - 20℃; for 0.5h;
88.8%
Diethylene glycol monobutyl ether
112-34-5

Diethylene glycol monobutyl ether

1,3-Diiodobenzene
626-00-6

1,3-Diiodobenzene

1,3-Bis-[2-(2-butoxy-ethoxy)-ethoxy]-benzene
71784-21-9

1,3-Bis-[2-(2-butoxy-ethoxy)-ethoxy]-benzene

Conditions
ConditionsYield
With copper(l) iodide; 1,10-Phenanthroline; caesium carbonate In 5,5-dimethyl-1,3-cyclohexadiene for 20h; Reflux; Inert atmosphere;86%
formaldehyd
50-00-0

formaldehyd

Diethylene glycol monobutyl ether
112-34-5

Diethylene glycol monobutyl ether

rccc-2,8,14,20-tetrakis-(iso-butyl)-resorcin[4]arene
118600-20-7, 134731-86-5

rccc-2,8,14,20-tetrakis-(iso-butyl)-resorcin[4]arene

C80H128O20

C80H128O20

Conditions
ConditionsYield
With iminodiacetic acid In acetonitrile81%
Diethylene glycol monobutyl ether
112-34-5

Diethylene glycol monobutyl ether

vanadium(V) oxychloride
7727-18-6

vanadium(V) oxychloride

dichloro(2-(2-butoxyethoxy)ethanolate)oxovanadium(V)

dichloro(2-(2-butoxyethoxy)ethanolate)oxovanadium(V)

Conditions
ConditionsYield
In pentane byproducts: HCl; N2, equimol., V compd. added dropwise to a soln. of alcohol, stirred for2 h, heated on water bath; decanted, concd., stored at 0°C, ppt. collected, dried (vac.); elem. anal.;80%
Diethylene glycol monobutyl ether
112-34-5

Diethylene glycol monobutyl ether

1-Iodonaphthalene
90-14-2

1-Iodonaphthalene

1-(2-(2-butoxyethoxy)ethoxy)naphthalene

1-(2-(2-butoxyethoxy)ethoxy)naphthalene

Conditions
ConditionsYield
With copper(l) iodide; 1,10-Phenanthroline; caesium carbonate In 5,5-dimethyl-1,3-cyclohexadiene at 145℃; for 26h; Inert atmosphere;79%
With copper(l) iodide; 1,10-Phenanthroline; caesium carbonate In 5,5-dimethyl-1,3-cyclohexadiene at 145℃; for 26h; Inert atmosphere;79%
Diethylene glycol monobutyl ether
112-34-5

Diethylene glycol monobutyl ether

2-Phenylpropanal
34713-70-7

2-Phenylpropanal

(E/Z)-(1-(2-(2-butoxyethoxy)ethoxy)prop-1-en-2-yl)benzene

(E/Z)-(1-(2-(2-butoxyethoxy)ethoxy)prop-1-en-2-yl)benzene

Conditions
ConditionsYield
With methanesulfonic acid; methanesulfonic acid sodium salt In toluene for 15h; Inert atmosphere; Reflux; Dean-Stark;79%
Diethylene glycol monobutyl ether
112-34-5

Diethylene glycol monobutyl ether

[2-(2-chloro-2-oxoethoxy)phenoxy]acetyl chloride
31250-16-5

[2-(2-chloro-2-oxoethoxy)phenoxy]acetyl chloride

Dibutoxyethoxyethyl 1,2-phenylenedioxydiacetate

Dibutoxyethoxyethyl 1,2-phenylenedioxydiacetate

Conditions
ConditionsYield
In tetrachloromethane Ambient temperature;76%
5-(chloromethyl)-6-propyl-1,3-benzodioxole
1938-32-5

5-(chloromethyl)-6-propyl-1,3-benzodioxole

Diethylene glycol monobutyl ether
112-34-5

Diethylene glycol monobutyl ether

Piperonyl butoxide
51-03-6

Piperonyl butoxide

Conditions
ConditionsYield
Stage #1: Diethylene glycol monobutyl ether With sodium hydroxide In water Reflux;
Stage #2: 5-(chloromethyl)-6-propyl-1,3-benzodioxole In water for 5h; Reflux;
75%
With sodium hydroxide at 30℃; for 5h;230 g
Diethylene glycol monobutyl ether
112-34-5

Diethylene glycol monobutyl ether

1,2-Diiodobenzene
615-42-9

1,2-Diiodobenzene

1,2-bis(2-(2-(butyloxy)ethoxy)ethoxy)benzene
71784-20-8

1,2-bis(2-(2-(butyloxy)ethoxy)ethoxy)benzene

Conditions
ConditionsYield
With copper(l) iodide; 1,10-Phenanthroline; caesium carbonate In 5,5-dimethyl-1,3-cyclohexadiene for 40h; Reflux; Inert atmosphere;75%
With copper(l) iodide; 1,10-Phenanthroline; caesium carbonate In 5,5-dimethyl-1,3-cyclohexadiene at 140℃; for 24h; Inert atmosphere;4 g
2,3-Dichloro-1,4-naphthoquinone
117-80-6

2,3-Dichloro-1,4-naphthoquinone

Diethylene glycol monobutyl ether
112-34-5

Diethylene glycol monobutyl ether

C26H38O8

C26H38O8

Conditions
ConditionsYield
With NAH In tetrahydrofuran at 80℃; Inert atmosphere;71%
Diethylene glycol monobutyl ether
112-34-5

Diethylene glycol monobutyl ether

2-(2-methoxyphenoxy)acetyl chloride
40926-73-6

2-(2-methoxyphenoxy)acetyl chloride

Butoxyethoxyethyl o-methoxyphenoxyacetate

Butoxyethoxyethyl o-methoxyphenoxyacetate

Conditions
ConditionsYield
In chloroform for 12h; Heating;69.01%
Diethylene glycol monobutyl ether
112-34-5

Diethylene glycol monobutyl ether

3-{[(4-bromobutyl)oxy]methyl}-3-methyloxetane
103781-33-5

3-{[(4-bromobutyl)oxy]methyl}-3-methyloxetane

3-(2,7,10,13-tetraoxaheptadecyl)-3-methyloxetane

3-(2,7,10,13-tetraoxaheptadecyl)-3-methyloxetane

Conditions
ConditionsYield
With sodium hydroxide; tetrabutylammomium bromide In hexane for 5h; Heating;68%
2-iodoacetyl chloride
38020-81-4

2-iodoacetyl chloride

Diethylene glycol monobutyl ether
112-34-5

Diethylene glycol monobutyl ether

2-(2-butoxyethoxy)ethyl-2-iodoacetate
56521-91-6

2-(2-butoxyethoxy)ethyl-2-iodoacetate

Conditions
ConditionsYield
With sodium carbonate In dichloromethane at -5 - 20℃; for 12h; Green chemistry;68%
Diethylene glycol monobutyl ether
112-34-5

Diethylene glycol monobutyl ether

2-(2-nitrophenoxy)acetyl chloride
20142-87-4

2-(2-nitrophenoxy)acetyl chloride

Butoxyethoxyethyl o-nitrophenoxyacetate

Butoxyethoxyethyl o-nitrophenoxyacetate

Conditions
ConditionsYield
In chloroform for 12h; Heating;66.89%
2,2,4,4,6,6-hexachloro-1,3,5-triaza-2,4,6-triphosphorine
940-71-6

2,2,4,4,6,6-hexachloro-1,3,5-triaza-2,4,6-triphosphorine

Diethylene glycol monobutyl ether
112-34-5

Diethylene glycol monobutyl ether

A

C24H51Cl3N3O9P3
1245625-50-6

C24H51Cl3N3O9P3

B

C24H51Cl3N3O9P3
1245625-47-1

C24H51Cl3N3O9P3

C

C24H51Cl3N3O9P3
1245625-36-8

C24H51Cl3N3O9P3

Conditions
ConditionsYield
With sodium hydride In tetrahydrofuran at -60 - 20℃; for 3.5h; Inert atmosphere;A 20%
B 16%
C 64%
Diethylene glycol monobutyl ether
112-34-5

Diethylene glycol monobutyl ether

A

C24H51Cl3N3O9P3
1245625-50-6

C24H51Cl3N3O9P3

B

C24H51Cl3N3O9P3
1245625-47-1

C24H51Cl3N3O9P3

C

C24H51Cl3N3O9P3
1245625-36-8

C24H51Cl3N3O9P3

Conditions
ConditionsYield
With 2,2,4,4,6,6-hexachloro-1,3,5-triaza-2,4,6-triphosphorine; sodium hydride In tetrahydrofuran at -60 - 20℃; for 3.5h; Inert atmosphere;A 20%
B 16%
C 64%
With 2,2,4,4,6,6-hexachloro-1,3,5-triaza-2,4,6-triphosphorine; sodium hydride In tetrahydrofuran at -60 - 20℃; for 3.5h; Inert atmosphere;A 20%
B 16%
C 64%
Diethylene glycol monobutyl ether
112-34-5

Diethylene glycol monobutyl ether

(5,10,15,20-tetraphenylporphinato)dichlorophosphorus(V) chloride

(5,10,15,20-tetraphenylporphinato)dichlorophosphorus(V) chloride

di(3,6-dioxadecyloxo)tetraphenylporphyrinatophosphorus(V) chloride

di(3,6-dioxadecyloxo)tetraphenylporphyrinatophosphorus(V) chloride

Conditions
ConditionsYield
With pyridine In acetonitrile for 24h; Reflux;60%
With pyridine In acetonitrile for 24h; Reflux;
Diethylene glycol monobutyl ether
112-34-5

Diethylene glycol monobutyl ether

2-methyl-2-octyldodecanoic acid

2-methyl-2-octyldodecanoic acid

C29H58O4

C29H58O4

Conditions
ConditionsYield
With toluene-4-sulfonic acid In toluene for 18h; Dean-Stark; Reflux;60%

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