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Calcium nitrate tetrahydrate
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13477-34-4 Usage

Chemical Properties

White colourless deliquescent crystals

Definition

ChEBI: A hydrate that is the tetrahydrate form of cadmium nitrate.

Uses

Used in the preparation of calcium standard solutions.

Purification Methods

Crystallise the nitrate four times from water (0.4mL/g) by cooling in a CaCl2-ice freezing mixture. The tetrahydrate is dried over conc H2SO4 and stored over P2O5, to give the anhydrous salt. It is deliquescent. After 3 recrystallisations of ACS grade salt, it had Co, Fe, Mg, Sr and Zn at 0.2, 1. 0, 0.02, 10 and 0.02 ppm resp. [Bassett & Taylor J Chem Soc 105 1926 1914.]
InChI:InChI=1/Ca.NO3.4H2O/c;2-1(3)4;;;;/h;;4*1H2/q+2;-1;;;;

13477-34-4 Well-known Company Product Price

Brand (Code)Product description CAS number Packaging Price Detail
Sigma (C2786)  Calciumnitratetetrahydrate  suitable for cell culture, suitable for plant cell culture 13477-34-4 C2786-1KG 1,275.30CNY Detail
Sigma (C2786)  Calciumnitratetetrahydrate  suitable for cell culture, suitable for plant cell culture 13477-34-4 C2786-500G 742.95CNY Detail
Sigma-Aldrich (C4955)  Calciumnitratetetrahydrate  BioXtra, ≥99.0% 13477-34-4 C4955-1KG 2,108.34CNY Detail
Sigma-Aldrich (C4955)  Calciumnitratetetrahydrate  BioXtra, ≥99.0% 13477-34-4 C4955-500G 1,219.14CNY Detail
Sigma-Aldrich (C1396)  Calciumnitratetetrahydrate  ≥99.0% 13477-34-4 C1396-1KG 1,240.20CNY Detail
Sigma-Aldrich (C1396)  Calciumnitratetetrahydrate  ≥99.0% 13477-34-4 C1396-500G 758.16CNY Detail
Sigma-Aldrich (31218)  Calciumnitratetetrahydrate  puriss. p.a., ACS reagent, 99-103% 13477-34-4 31218-5KG 4,055.22CNY Detail
Sigma-Aldrich (31218)  Calciumnitratetetrahydrate  puriss. p.a., ACS reagent, 99-103% 13477-34-4 31218-1KG 1,407.51CNY Detail
Sigma-Aldrich (31218)  Calciumnitratetetrahydrate  puriss. p.a., ACS reagent, 99-103% 13477-34-4 31218-250G 334.62CNY Detail
Sigma-Aldrich (237124)  Calciumnitratetetrahydrate  ACS reagent, 99% 13477-34-4 237124-2.5KG 2,884.05CNY Detail
Sigma-Aldrich (237124)  Calciumnitratetetrahydrate  ACS reagent, 99% 13477-34-4 237124-500G 703.17CNY Detail
Alfa Aesar (30482)  Calcium nitrate tetrahydrate, 99.98% (metals basis)    13477-34-4 500g 5015.0CNY Detail

13477-34-4SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 12, 2017

Revision Date: Aug 12, 2017

1.Identification

1.1 GHS Product identifier

Product name calcium nitrate tetrahydrate

1.2 Other means of identification

Product number -
Other names Calcium nitrate tetrahydrate

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only.
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:13477-34-4 SDS

13477-34-4Synthetic route

soda lime

soda lime

calcium cyanamide
156-62-7

calcium cyanamide

calcium(II) nitrate
13477-34-4

calcium(II) nitrate

Conditions
ConditionsYield
With air; copper(II) oxide; copper(II) carbonate; nickel(II) carbonate In neat (no solvent) storage of thin layer of mixt. of lime nitrogen, soda lime and CuO on air for few days; addn. of catalyst, heating in dry stream of air at 400°C, until oxidn. of C is complete; heating up to 3 h at 450°C; acceleration by min. of H2O vapor;;38%
nitrogen(II) oxide
10102-43-9

nitrogen(II) oxide

A

calcium nitrite

calcium nitrite

B

nitrogen
7727-37-9

nitrogen

C

calcium(II) nitrate
13477-34-4

calcium(II) nitrate

D

dinitrogen monoxide
10024-97-2

dinitrogen monoxide

Conditions
ConditionsYield
With calcium oxide 400°C, 21 h;A 0.9%
B n/a
C <1
D n/a
With CaO 400°C, 21 h;A 0.9%
B n/a
C <1
D n/a
dolomite

dolomite

nitric acid
7697-37-2

nitric acid

calcium oxide

calcium oxide

A

calcium(II) nitrate
13477-34-4

calcium(II) nitrate

B

magnesium oxide

magnesium oxide

Conditions
ConditionsYield
In water addn. of HNO3 to dolomite also dissolves Mg; removal as Mg(OH)2 with CaO;;
dolomite

dolomite

nitric acid
7697-37-2

nitric acid

calcium(II) nitrate
13477-34-4

calcium(II) nitrate

Conditions
ConditionsYield
In water dolomite slurry filtered and treated with HNO3; CaCO3 dissolves, and MgCO3 remains undissolved;;
With calcium(II) nitrate In water dolomite dissolved in Ca(NO3)3 soln. containing at most 1% HNO3;;
In water amt. of applied acid insufficient to dissolve also MgCO3;;
dolomite

dolomite

nitric acid
7697-37-2

nitric acid

calcium hydroxide

calcium hydroxide

A

calcium(II) nitrate
13477-34-4

calcium(II) nitrate

B

magnesium oxide

magnesium oxide

Conditions
ConditionsYield
In water addn. of HNO3 to dolomite also dissolves Mg; removal as Mg(OH)2 with Ca(OH)2;;
ammonium nitrate

ammonium nitrate

dolomite

dolomite

calcium(II) nitrate
13477-34-4

calcium(II) nitrate

Conditions
ConditionsYield
In ammonia CaCO3 portion of dolomite dissolves in liquid ammonia containing an equivalent amt. of NH4NO3;;
tricalcium diphosphate

tricalcium diphosphate

nitrosylchloride
2696-92-6

nitrosylchloride

calcium(II) nitrate
13477-34-4

calcium(II) nitrate

Conditions
ConditionsYield
In water intermediately formed nitrogen oxides react to form the nitrates;;
In water intermediately formed nitrogen oxides react to form the nitrates;;
calcium(II) sulfide

calcium(II) sulfide

nitric acid
7697-37-2

nitric acid

A

hydrogen sulfide
7783-06-4

hydrogen sulfide

B

calcium(II) nitrate
13477-34-4

calcium(II) nitrate

Conditions
ConditionsYield
In water
calcium(II) sulfide

calcium(II) sulfide

ammonium nitrate

ammonium nitrate

calcium(II) nitrate
13477-34-4

calcium(II) nitrate

Conditions
ConditionsYield
trituration at moderate temp.;;
trituration at moderate temp.;;
calcium oxide

calcium oxide

A

dinitrogen trioxide
10544-73-7

dinitrogen trioxide

B

calcium(II) nitrate
13477-34-4

calcium(II) nitrate

Conditions
ConditionsYield
With nitrogen oxides; Fe(OH)3 or Al(OH)3 or Cr(OH)3 In water absorption of nitrogen oxides in suspensions of heavy metal hydroxides and with CaO; then interaction of the intermediately formed nitrates;;
With nitrogen oxides In water absorption of nitrogen oxides in suspensions of heavy metal hydroxides and with CaO; then interaction of the intermediately formed nitrates;;
nitrogen
7727-37-9

nitrogen

oxygen
80937-33-3

oxygen

calcium oxide

calcium oxide

calcium(II) nitrate
13477-34-4

calcium(II) nitrate

Conditions
ConditionsYield
In neat (no solvent) High Pressure; react. of atmospheric N2 and O2 with CaO at 800 - 900°C under high pressure;;
In neat (no solvent) High Pressure; react. of atmospheric N2 and O2 with CaO at 800 - 900°C under high pressure;;
nitric acid
7697-37-2

nitric acid

calcium oxide

calcium oxide

calcium(II) nitrate
13477-34-4

calcium(II) nitrate

Conditions
ConditionsYield
With phosphate minerals In water Decompn. of phosphate minerals by HNO3; to avoid pptn. of Ca phosphates during neutralization of Ca(NO3)2 solns. because of residual phosphate, neutralization is done with concd. solns. of Ca(NO3)2 satd. with CaO;;
ammonium nitrate

ammonium nitrate

calcium oxide

calcium oxide

A

calcium(II) nitrate
13477-34-4

calcium(II) nitrate

B

ammonia
7664-41-7

ammonia

C

water
7732-18-5

water

Conditions
ConditionsYield
In neat (no solvent) solving of CaO in molten NH4NO3;;
In neat (no solvent) solving of CaO in molten NH4NO3;;
ammonium nitrate

ammonium nitrate

calcium oxide

calcium oxide

calcium(II) nitrate
13477-34-4

calcium(II) nitrate

Conditions
ConditionsYield
byproducts: NH3; H2O;
ammonium nitrate

ammonium nitrate

calcium oxide

calcium oxide

A

calcium(II) nitrate
13477-34-4

calcium(II) nitrate

B

ammonia
7664-41-7

ammonia

Conditions
ConditionsYield
In water indirect reaction with HNO3; from destillation gases NH4NO3 is formed by HNO3; NH4NO3 reacted with CaO and NH3 again oxidized to form HNO3 which retuens into the cycle;;
silver nitrate

silver nitrate

calcium oxide

calcium oxide

A

calcium(II) nitrate
13477-34-4

calcium(II) nitrate

B

silver(l) oxide
20667-12-3

silver(l) oxide

Conditions
ConditionsYield
heating a mixture of AgNO3 and CaO (50 mol %) at 190°C;;
nitrogen(II) oxide
10102-43-9

nitrogen(II) oxide

Nitrogen dioxide
10102-44-0

Nitrogen dioxide

calcium oxide

calcium oxide

A

calcium nitrite

calcium nitrite

B

calcium(II) nitrate
13477-34-4

calcium(II) nitrate

Conditions
ConditionsYield
In neat (no solvent) ratio nitrate : nitrite depending on temp.;;
In neat (no solvent) ratio nitrate : nitrite depending on temp.;;
nitrogen(II) oxide
10102-43-9

nitrogen(II) oxide

Nitrogen dioxide
10102-44-0

Nitrogen dioxide

calcium oxide

calcium oxide

calcium(II) nitrate
13477-34-4

calcium(II) nitrate

Conditions
ConditionsYield
In neat (no solvent) use of slake lime dehydrated at 400 - 650°C;;
In neat (no solvent) CaO used in coarse-grained or pelltized form;;
In neat (no solvent) use of quicklime calcined at 700 - 750°C;;
oxygen
80937-33-3

oxygen

calcium oxide

calcium oxide

A

nitrogen
7727-37-9

nitrogen

B

calcium(II) nitrate
13477-34-4

calcium(II) nitrate

C

nitrogen(II) oxide
10102-43-9

nitrogen(II) oxide

D

Nitrogen dioxide
10102-44-0

Nitrogen dioxide

Conditions
ConditionsYield
With nitrogen oxides In neat (no solvent) nitrogen oxides (formed by combustion of air or oxidn. of NH3) react at 230-480 °C with CaO and O2 to form Ca(NO3)2 and Ca(NO2)2, the latter decomposes forming CaO, NO, N2; at >480°C also NO2 forms and oxidizes Ca(NO2)2 to Ca(NO3)2;;
With nitrogen oxides In neat (no solvent) nitrogen oxides (formed by combustion of air or oxidn. of NH3) react at 230-480 °C with CaO and O2 to form Ca(NO3)2 and Ca(NO2)2, the latter decomposes forming CaO, NO, N2; at >480°C also NO2 forms and oxidizes Ca(NO2)2 to Ca(NO3)2;;
ammonia
7664-41-7

ammonia

calcium oxide

calcium oxide

calcium(II) nitrate
13477-34-4

calcium(II) nitrate

Conditions
ConditionsYield
In neat (no solvent) surface oxidation of NH3 at 360 °C on lime surfaces containing 0.2-2.5% NiO or CuO as activators;;
In neat (no solvent) surface oxidation of NH3 at 360 °C on lime surfaces containing 0.2-2.5% NiO or CuO as activators;;
tricalcium diphosphate

tricalcium diphosphate

Nitrogen dioxide
10102-44-0

Nitrogen dioxide

A

calcium hydrogen phosphate
7789-77-7

calcium hydrogen phosphate

B

calcium(II) nitrate
13477-34-4

calcium(II) nitrate

Conditions
ConditionsYield
reaction of NO2 with moist Ca phosphate;;
reaction of NO2 with moist Ca phosphate;;
Nitrate

Nitrate

calcium(II) nitrate
13477-34-4

calcium(II) nitrate

Conditions
ConditionsYield
With phosphoric acid byproducts: Na-phosphates; by product of Na phosphate synthesis : treatment of crude phosphate with nitrates (except alkali nitrates and group II nitrates) at elevated temp.;;
With phosphoric acid byproducts: Na-phosphates; by product of Na phosphate synthesis : treatment of crude phosphate with nitrates (except alkali nitrates and group II nitrates) at elevated temp.;;
nitric acid
7697-37-2

nitric acid

A

calcium hydrogen phosphate
7789-77-7

calcium hydrogen phosphate

B

calcium dihydrogen phosphate

calcium dihydrogen phosphate

C

calcium(II) nitrate
13477-34-4

calcium(II) nitrate

Conditions
ConditionsYield
With phosphate minerals Decompn. of phosphate minerals by HNO3;;
nitric acid
7697-37-2

nitric acid

calcium(II) nitrate
13477-34-4

calcium(II) nitrate

Conditions
ConditionsYield
With calcium chloride no reaction at low temp.;0%
With calcium chloride evapn. with excess of HNO3 soln.;>99
With CaCl2 no reaction at low temp.;0%
With CaCl2 evapn. with excess of HNO3 soln.;>99
nitric acid
7697-37-2

nitric acid

calcium chloride

calcium chloride

calcium(II) nitrate
13477-34-4

calcium(II) nitrate

Conditions
ConditionsYield
In water react. at bp. of the soln., eventually under pressure;;
With MnO2 or H2SO4 In water with fuming (brown) HNO3 at 20°C or with highly concd.HNO3 in presence of MnO2 or H2SO4 at 50 - 60°C;;
In water react. at bp. of the soln., eventually under pressure;;
calcium fluoride

calcium fluoride

nitric acid
7697-37-2

nitric acid

calcium(II) nitrate
13477-34-4

calcium(II) nitrate

Conditions
ConditionsYield
In water Ca(NO3)2 as by-product;;
nitric acid
7697-37-2

nitric acid

Phosphate
14265-44-2

Phosphate

calcium(II) nitrate
13477-34-4

calcium(II) nitrate

Conditions
ConditionsYield
With calcium oxide In water addn. of excess of HNO3 to phosphates formed 3Ca(NO3)2*12H2O*HNO3; neutralisation with milk of lime;; pptn.;;
With calcium oxide In water addn. of excess of HNO3 to phosphates formed 3Ca(NO3)2*12H2O*HNO3; neutralisation with milk of lime;; pptn.;;
sulfuric acid
7664-93-9

sulfuric acid

calcium(II) ion

calcium(II) ion

nitric acid
7697-37-2

nitric acid

Phosphate
14265-44-2

Phosphate

A

calcium sulfate

calcium sulfate

B

calcium(II) nitrate
13477-34-4

calcium(II) nitrate

Conditions
ConditionsYield
In neat (no solvent)
In neat (no solvent)
calcium aluminate

calcium aluminate

nitric acid
7697-37-2

nitric acid

A

aluminum trihydroxide

aluminum trihydroxide

B

calcium(II) nitrate
13477-34-4

calcium(II) nitrate

calcium(II) nitrate
13477-34-4

calcium(II) nitrate

calcium manganese(IV) oxide

calcium manganese(IV) oxide

Conditions
ConditionsYield
With air; glycine In water mixt. blended and heated; calcined at 800-850°C for 2 h; ball milled in ethanol for 24 h; pressed; burn out of binder in vac. at 450°C; sintered at 1100-1550°C for 2 h in air; cooled; XRD; SEM; TEM;100%
calcium(II) nitrate
13477-34-4

calcium(II) nitrate

lanthanum(III) nitrate

lanthanum(III) nitrate

La0.30Ca0.70MnO3.00

La0.30Ca0.70MnO3.00

Conditions
ConditionsYield
With air; glycine In water mixt. blended and heated; calcined at 800-850°C for 2 h; ball milled in ethanol for 24 h; pressed; burn out of binder in vac. at 450°C; sintered at 1100-1550°C for 2 h in air; cooled; XRD; SEM; TEM;100%
diammonium hydrogenphosphate

diammonium hydrogenphosphate

calcium(II) nitrate
13477-34-4

calcium(II) nitrate

calcium hydroxyapatite

calcium hydroxyapatite

Conditions
ConditionsYield
With magnesium(II) nitrate; nitric acid; urea mixing stoich. components solns., heating at 85°C for 192 h or at90°C for 72 h or at 95°C for 48 h; XRD, SEM;99%
With nitric acid; urea mixing stoich. components solns., heating at 85°C for 192 h or at90°C for 72 h or at 95°C for 48 h; XRD, SEM;99%
methanol
67-56-1

methanol

[Cu(pyrimidine-2-olate-N1,N3)2]n*nH2O

[Cu(pyrimidine-2-olate-N1,N3)2]n*nH2O

calcium(II) nitrate
13477-34-4

calcium(II) nitrate

[Cu(pyrimidine-2-olate-N1,N3)2]*0.5Ca(nitrate)2*0.4methanol*0.4water

[Cu(pyrimidine-2-olate-N1,N3)2]*0.5Ca(nitrate)2*0.4methanol*0.4water

Conditions
ConditionsYield
In methanol; water stirring suspn. of copper compd. in 0.05 M soln. of calcium nitrate in 4:1 mixt. of methanol and water for 1 wk at room temp.; elem. anal.;99%
[2,2]bipyridinyl
366-18-7

[2,2]bipyridinyl

diammonium phosphate

diammonium phosphate

cobalt(II) nitrate hexahydrate

cobalt(II) nitrate hexahydrate

hexaammonium heptamolybdate tetrahydrate

hexaammonium heptamolybdate tetrahydrate

calcium(II) nitrate
13477-34-4

calcium(II) nitrate

3C10H8N2*8Ca(2+)*Co(3+)*5H(1+)*31H2O*5H3N*6O4P(3-)*Mo12O44P2(6-)

3C10H8N2*8Ca(2+)*Co(3+)*5H(1+)*31H2O*5H3N*6O4P(3-)*Mo12O44P2(6-)

Conditions
ConditionsYield
In water at 60 - 65℃; for 1h;97%
sodium molybdate

sodium molybdate

calcium(II) nitrate
13477-34-4

calcium(II) nitrate

calcium molybdate

calcium molybdate

Conditions
ConditionsYield
In melt byproducts: NaNO3; melt of NaNO3, 450.+-.5°C, periodically mixed, 40 min; poured into a dish, left to cool, washed repeatedly (10-20 times) with water, dried at 200°C to constant mass, elem. anal.;96.34%
In water contains Cu or Co when precipitated at pH 8 to 8.5;;
With aq. HNO3; aq. NaOH In water High Pressure; adjusted (aq. HNO3/aq. NaOH) pH of Ca compd. soln. to 1.5, soln. of Mo compd. slowly dropped under vigorous stirring, stirred for 45 min, transferred into autoclave, sealed, heated at 150°C for 6 h, cooled naturally to room temp.; product collected by centrifugation, washed several times with distd. water and abs. ethanol, dried at 80°C for 6 h;
In water contains Cu or Co when precipitated at pH 8 to 8.5;;
In ethylene glycol High Pressure; microwave radiation method; each 0.005 mol of Ca(NO3)2 and Na2MoO4 sep. dissolved in ethylene glycol, two solns. mixed and stirred for 30 min, mixt. trensferred into autoclave, heated at 50% of 600 W microwave for 20min (60 s on and 60 s off); white ppt. filtered, washed (distd. H2O, abs. EtOH), dried (80 °C, 24 h, air); XRD;
phosphotungstic acid

phosphotungstic acid

calcium(II) nitrate
13477-34-4

calcium(II) nitrate

calcium phosphotungstate

calcium phosphotungstate

Conditions
ConditionsYield
at 95℃; for 6h;96%
potassium tungstate

potassium tungstate

calcium(II) nitrate
13477-34-4

calcium(II) nitrate

calcium tungstate

calcium tungstate

Conditions
ConditionsYield
In melt byproducts: KNO3; melt of KNO3, 450.+-.5°C, periodically mixed, 40 min; poured into a dish, left to cool, washed repeatedly (10-20 times) with water, dried at 200°C to constant mass, elem. anal.;95.69%
sodium tungstate

sodium tungstate

calcium(II) nitrate
13477-34-4

calcium(II) nitrate

calcium tungstate

calcium tungstate

Conditions
ConditionsYield
With sodium nitrate In melt mixt. of NaNO3, Ca(NO3)2 and Na2WO4 heated in fused quartz tube at 400°C for 40-50 min with periodic stirring of the melt; poured into porcelain cup; cooled; washed with H2O; dried to const. weight at 200°C; elem. anal.;95.24%
In water heating at 1000°C, fluorescent product;
In not given
aluminium trinitrate
7784-27-2

aluminium trinitrate

calcium(II) nitrate
13477-34-4

calcium(II) nitrate

calcium hexaaluminate

calcium hexaaluminate

Conditions
ConditionsYield
In solid Kinetics; in electric furnace at 1670 K; XRD;95%
In solid Kinetics; in electric furnace at 1570 K;90%
In solid Kinetics; in electric furnace at 1770 K;83%
bis(4'-(4'''-benzo-15-crown-5)methyloxy-2,2':6',2''-terpyridine)zinc(II) hexafluorophosphate

bis(4'-(4'''-benzo-15-crown-5)methyloxy-2,2':6',2''-terpyridine)zinc(II) hexafluorophosphate

calcium(II) nitrate
13477-34-4

calcium(II) nitrate

[Ca2(Zn(II)(4'-(4'''-benzo-15-crown-5)methyloxy-2,2':6',2''-terpyridine)2)(NO3)2](hexafluorophosphate)2

[Ca2(Zn(II)(4'-(4'''-benzo-15-crown-5)methyloxy-2,2':6',2''-terpyridine)2)(NO3)2](hexafluorophosphate)2

Conditions
ConditionsYield
In acetonitrile Zn complex dissolved on heating in MeCN, Ca nitrate added in MeCN with stirring, crystn. 2 d; ppt. filtered off, washed with ice-cooled MeCN, dried in vac. at 60 °C, elem. anal.;92%
potassium cyanide

potassium cyanide

1,10-Phenanthroline
66-71-7

1,10-Phenanthroline

ethanol
64-17-5

ethanol

4(CH3)4N(1+)*Nb6Cl18(4-)=((CH3)4N)4Nb6Cl18

4(CH3)4N(1+)*Nb6Cl18(4-)=((CH3)4N)4Nb6Cl18

calcium(II) nitrate
13477-34-4

calcium(II) nitrate

A

[Ca(1,10-phenanthroline)2(H2O)2]2[Nb6Cl12(CN)6]*(1,10-phenanthroline)2*4H2O

[Ca(1,10-phenanthroline)2(H2O)2]2[Nb6Cl12(CN)6]*(1,10-phenanthroline)2*4H2O

B

[Ca(1,10-phenanthroline)2(H2O)3]2[Nb6Cl12(CN)6]*(1,10-phenanthroline)*1.6(EtOH)

[Ca(1,10-phenanthroline)2(H2O)3]2[Nb6Cl12(CN)6]*(1,10-phenanthroline)*1.6(EtOH)

Conditions
ConditionsYield
In ethanol; water aq. soln. Ca(NO3)2 and soln. phen in EtOH were added to aq. soln. Nb complex and KCN; ppt. was collected by centrifugation, washed with H2O, dried under vac.;A 5%
B 90%
cadmium(II) nitrate tetrhydrate

cadmium(II) nitrate tetrhydrate

5-t-butylisophthalic acid
2359-09-3

5-t-butylisophthalic acid

calcium(II) nitrate
13477-34-4

calcium(II) nitrate

[Me2NH2]2[Cd2Ca(5-tert-butylisophthalate)4]

[Me2NH2]2[Cd2Ca(5-tert-butylisophthalate)4]

Conditions
ConditionsYield
In methanol; N,N-dimethyl-formamide High Pressure; mixt. of Cd salt (1 equiv.), acid (2 equiv.) and Ca salt (2 equiv.) in DMF/MeOH (1/1) was heated to 160°C for 4 h in autoclave; heated at160°C for 2 d; cooled to room temp. over 2 d; filtered; washed (DMF, MeOH); dried in air at room temp.; elem. anal.;87%
cadmium(II) nitrate tetrhydrate

cadmium(II) nitrate tetrhydrate

isophthalic acid
121-91-5

isophthalic acid

calcium(II) nitrate
13477-34-4

calcium(II) nitrate

N,N-dimethyl-formamide
68-12-2, 33513-42-7

N,N-dimethyl-formamide

[CdCa(isophthalate)2(N,N-dimethylformamide)2]

[CdCa(isophthalate)2(N,N-dimethylformamide)2]

Conditions
ConditionsYield
In methanol; N,N-dimethyl-formamide High Pressure; mixt. of Cd salt (1 equiv.), acid (2 equiv.) and Ca salt (2 equiv.) in DMF/MeOH (1/1) was heated to 160°C for 4 h in autoclave; heated at160°C for 2 d; cooled to room temp. over 2 d; filtered; washed (DMF, MeOH); dried in air at room temp.; elem. anal.;86%
cadmium(II) nitrate tetrhydrate

cadmium(II) nitrate tetrhydrate

5-Hydroxyisophthalic acid
618-83-7

5-Hydroxyisophthalic acid

calcium(II) nitrate
13477-34-4

calcium(II) nitrate

[CdCa(5-hydroxyisophthalate)2(H2O)2]*Me2NH

[CdCa(5-hydroxyisophthalate)2(H2O)2]*Me2NH

Conditions
ConditionsYield
In methanol; N,N-dimethyl-formamide High Pressure; mixt. of Cd salt (1 equiv.), acid (2 equiv.) and Ca salt (2 equiv.) in DMF/MeOH (1/1) was heated to 160°C for 4 h in autoclave; heated at160°C for 2 d; cooled to room temp. over 2 d; filtered; washed (DMF, MeOH); dried in air at room temp.; elem. anal.;85%
mono-K,Li-heptadecatungstodiphosphate*18H2O 18H2O*K9LiO61P2W17, α1

mono-K,Li-heptadecatungstodiphosphate*18H2O 18H2O*K9LiO61P2W17, α1

calcium(II) nitrate
13477-34-4

calcium(II) nitrate

mono-K,Ca-heptadecatungstodiphosphate*19H2O CaK8O61P2W17*19H2O, α1

mono-K,Ca-heptadecatungstodiphosphate*19H2O CaK8O61P2W17*19H2O, α1

Conditions
ConditionsYield
In water soln. of metal salt added to Li salt by stirring; filtered, soln. pptd. with KCl, filtered, washed with EtOH and Et2O, air-dried, elem. anal.;80%
barite

barite

calcium(II) nitrate
13477-34-4

calcium(II) nitrate

barium(II) nitrate

barium(II) nitrate

Conditions
ConditionsYield
In melt byproducts: CaSO4; ratio of BaSO4 to Ca(NO3)2 = 1:2 because of reversible reaction; quick cooling; crystn. (water);75%
In melt byproducts: CaSO4; ratio of BaSO4 to Ca(NO3)2 = 1:2 because of reversible reaction; quick cooling; crystn. (water);75%
calcium(II) nitrate
13477-34-4

calcium(II) nitrate

sodium chloride
7647-14-5

sodium chloride

sodium nitrate
7631-99-4

sodium nitrate

Conditions
ConditionsYield
In water preparation on cation exchange resins, 52% Ca-nitrate soln., 26% NaCl-soln.;; crystn.;;70%
In water preparation on cation exchange resins, 52% Ca-nitrate soln., 26% NaCl-soln.;; crystn.;;70%
In water equilibrium in aq. soln.;;
2,2′-{1,2-phenylenebis[oxyacetyl(N,N-diethylthiourea)]}

2,2′-{1,2-phenylenebis[oxyacetyl(N,N-diethylthiourea)]}

calcium(II) nitrate
13477-34-4

calcium(II) nitrate

silver nitrate

silver nitrate

C40H56Ag2CaN8O8S4

C40H56Ag2CaN8O8S4

Conditions
ConditionsYield
Stage #1: 2,2′-{1,2-phenylenebis[oxyacetyl(N,N-diethylthiourea)]}; calcium(II) nitrate; silver nitrate In methanol; water at 20℃; for 0.5h;
Stage #2: With triethylamine In methanol; water
67%
(N,N'-2,2-dimethylpropylenedi(3-methoxysalicylideneiminato)Cu dihydrate

(N,N'-2,2-dimethylpropylenedi(3-methoxysalicylideneiminato)Cu dihydrate

calcium(II) nitrate
13477-34-4

calcium(II) nitrate

[Cu(N,N'-2,2-dimethylpropylenedi(3-methoxysalicylideneimine))]2Ca(NO3)2*H2O
954111-03-6

[Cu(N,N'-2,2-dimethylpropylenedi(3-methoxysalicylideneimine))]2Ca(NO3)2*H2O

Conditions
ConditionsYield
In methanol Cu-compd. and 1 equiv. of alkaline earth-compd. were stirred in MeOH for3 h; ppt. was filtered off, dried, elem. anal.;65%
monoaqua 3-methoxysalicylaldehyde-ethyldiamine copper(II)
157143-69-6, 41754-70-5

monoaqua 3-methoxysalicylaldehyde-ethyldiamine copper(II)

calcium(II) nitrate
13477-34-4

calcium(II) nitrate

[Cu(N,N'-ethylenedi(3-methoxysalicylideneimine))]2Ca(NO3)2*2H2O

[Cu(N,N'-ethylenedi(3-methoxysalicylideneimine))]2Ca(NO3)2*2H2O

Conditions
ConditionsYield
In methanol Cu-compd. and 1 equiv. of alkaline earth-compd. were stirred in MeOH for3 h; ppt. was filtered off, dried, elem. anal.;65%
C36H44Au2N2O4P2S2*8H2O

C36H44Au2N2O4P2S2*8H2O

calcium(II) nitrate
13477-34-4

calcium(II) nitrate

nickel(II) acetate tetrahydrate
6018-89-9

nickel(II) acetate tetrahydrate

cobalt(II) diacetate tetrahydrate
6147-53-1

cobalt(II) diacetate tetrahydrate

A

6C26H24P2*12C5H9NO2S(2-)*12Au(1+)*2.01Ni(2+)*3.99Co(3+)*8NO3(1-)*23.01H2O*2.01H(1+)*Ca(2+)

6C26H24P2*12C5H9NO2S(2-)*12Au(1+)*2.01Ni(2+)*3.99Co(3+)*8NO3(1-)*23.01H2O*2.01H(1+)*Ca(2+)

B

2C26H24P2*4C5H9NO2S(2-)*4Au(1+)*2Ni(2+)

2C26H24P2*4C5H9NO2S(2-)*4Au(1+)*2Ni(2+)

Conditions
ConditionsYield
Stage #1: C36H44Au2N2O4P2S2*8H2O; nickel(II) acetate tetrahydrate; cobalt(II) diacetate tetrahydrate With air In methanol at 20℃; for 3h;
Stage #2: calcium(II) nitrate In methanol; water at 20℃; for 168h;
A 65%
B 16%
sodium sulfide

sodium sulfide

calcium(II) nitrate
13477-34-4

calcium(II) nitrate

sodium sulfite
7757-83-7

sodium sulfite

A

calcium sulfate

calcium sulfate

B

sodium sulfate
7757-82-6

sodium sulfate

C

sodium nitrite
7632-00-0

sodium nitrite

Conditions
ConditionsYield
In neat (no solvent) formation at heating under glowing;;A n/a
B n/a
C 60%
manganese(II)carbonate

manganese(II)carbonate

calcium(II) nitrate
13477-34-4

calcium(II) nitrate

citric acid monohydrate
5949-29-1

citric acid monohydrate

[MnCa2(HCit)2(H2O)4]n

[MnCa2(HCit)2(H2O)4]n

Conditions
ConditionsYield
In water High Pressure; under aerobic conditions; Ca salt (1.95 mmol), citric acid hydrate (2 mmol), and MnCO3 (1 mmol) dissolved in H2O, mixt. heated 160°C in sealed teflon tube for 3 d; elem. anal.;60%
N,N'-bis(3-methoxysalicylidene)ethylenediamine
7396-77-2

N,N'-bis(3-methoxysalicylidene)ethylenediamine

calcium(II) nitrate
13477-34-4

calcium(II) nitrate

manganese (II) acetate tetrahydrate
6156-78-1

manganese (II) acetate tetrahydrate

[Mn(MeOsalen)(H2O)2](NO3)

[Mn(MeOsalen)(H2O)2](NO3)

[Mn(MeOsalen)(H2O)2](NO3)*0.25H2O

[Mn(MeOsalen)(H2O)2](NO3)*0.25H2O

Conditions
ConditionsYield
In ethanol at 20℃; for 2h;A 60%
B 20%
4-(2,3,4-tricarboxylphenyl)-2,2':6,2''-terpyridine

4-(2,3,4-tricarboxylphenyl)-2,2':6,2''-terpyridine

calcium(II) nitrate
13477-34-4

calcium(II) nitrate

C24H13N3O6(2-)*Ca(2+)*4H2O

C24H13N3O6(2-)*Ca(2+)*4H2O

Conditions
ConditionsYield
With water at 10 - 140℃; for 72h; Temperature; Autoclave;60%
(tetrahydrothiophene)gold(I) chloride
39929-21-0

(tetrahydrothiophene)gold(I) chloride

2,2′-{1,2-phenylenebis[oxyacetyl(N,N-diethylthiourea)]}

2,2′-{1,2-phenylenebis[oxyacetyl(N,N-diethylthiourea)]}

calcium(II) nitrate
13477-34-4

calcium(II) nitrate

C40H56Au2N8O8S4(2-)*Ca(2+)

C40H56Au2N8O8S4(2-)*Ca(2+)

Conditions
ConditionsYield
Stage #1: (tetrahydrothiophene)gold(I) chloride; 2,2′-{1,2-phenylenebis[oxyacetyl(N,N-diethylthiourea)]}; calcium(II) nitrate With water In methanol at 20℃; for 0.5h;
Stage #2: With triethylamine In methanol at 50℃; for 1h;
60%
calcium(II) nitrate
13477-34-4

calcium(II) nitrate

acetic anhydride
108-24-7

acetic anhydride

calcium acetate
62-54-4

calcium acetate

Conditions
ConditionsYield
In acetic anhydride H2O free;;59%
In acetic anhydride H2O free;;59%
calcium(II) nitrate
13477-34-4

calcium(II) nitrate

N,N-dimethyl-formamide
68-12-2, 33513-42-7

N,N-dimethyl-formamide

3,4-dimethylthieno[2,3-b]thiophene-2,5-dicarboxylic acid

3,4-dimethylthieno[2,3-b]thiophene-2,5-dicarboxylic acid

[Ca(DMTDC)(N,N-dimethylformamide)]

[Ca(DMTDC)(N,N-dimethylformamide)]

Conditions
ConditionsYield
at 95℃; for 24h; High pressure;58.7%
2,3-dicarboxypyrazine
89-01-0

2,3-dicarboxypyrazine

calcium(II) nitrate
13477-34-4

calcium(II) nitrate

water
7732-18-5

water

silver nitrate

silver nitrate

Ag2Ca(2,3-pyrazinedicarboxalate)2(H2O)

Ag2Ca(2,3-pyrazinedicarboxalate)2(H2O)

Conditions
ConditionsYield
With sodium hydroxide at 100℃; for 72h; pH=7;57%

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