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2-(Phenylmethoxy)-naphthalene Manufacturer/High quality/Best price/In stock
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Benzyl-2-Naphthylether
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613-62-7 Usage

Synthesis Reference(s)

Tetrahedron Letters, 20, p. 3543, 1979 DOI: 10.1016/S0040-4039(01)95457-7
InChI:InChI=1/C17H14O/c1-2-6-14(7-3-1)13-18-17-11-10-15-8-4-5-9-16(15)12-17/h1-12H,13H2

613-62-7 Well-known Company Product Price

Brand (Code)Product description CAS number Packaging Price Detail
Alfa Aesar (B21796)  Benzyl 2-naphthyl ether, 99%    613-62-7 25g 372.0CNY Detail
Alfa Aesar (B21796)  Benzyl 2-naphthyl ether, 99%    613-62-7 100g 1046.0CNY Detail
Alfa Aesar (B21796)  Benzyl 2-naphthyl ether, 99%    613-62-7 500g 2871.0CNY Detail

613-62-7SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 18, 2017

Revision Date: Aug 18, 2017

1.Identification

1.1 GHS Product identifier

Product name Benzyl 2-Naphthyl Ether

1.2 Other means of identification

Product number -
Other names Naphthalene, 2-(phenylmethoxy)-

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only.
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:613-62-7 SDS

613-62-7Synthetic route

naphthalen-2-yl acetate
1523-11-1

naphthalen-2-yl acetate

benzyl bromide
100-39-0

benzyl bromide

2-benzyloxynaphthalene
613-62-7

2-benzyloxynaphthalene

Conditions
ConditionsYield
With sodium methylate In N,N-dimethyl-formamide for 0.5h; Ambient temperature;100%
With 18-crown-6 ether; potassium carbonate In acetone for 1.5h; Heating;79%
sodium 2-naphtholate
875-83-2

sodium 2-naphtholate

benzyl chloride
100-44-7

benzyl chloride

2-benzyloxynaphthalene
613-62-7

2-benzyloxynaphthalene

Conditions
ConditionsYield
In various solvent(s) at 110℃; for 24h;97%
In dimethyl sulfoxide at 25℃; for 12h;92%
With ethanol
With tris(dibutylamino)cyclopropenium tetrafluoroborate at 25℃; for 24h; Inert atmosphere;
at 25℃; for 24h; Ionic liquid;
2-(dimethyl-1,1’-dimethylethylsilyloxy)naphthalene
62790-91-4

2-(dimethyl-1,1’-dimethylethylsilyloxy)naphthalene

benzyl bromide
100-39-0

benzyl bromide

2-benzyloxynaphthalene
613-62-7

2-benzyloxynaphthalene

Conditions
ConditionsYield
With cesium fluoride In N,N-dimethyl-formamide for 12h; Ambient temperature;97%
benzyl bromide
100-39-0

benzyl bromide

β-naphthol
135-19-3

β-naphthol

2-benzyloxynaphthalene
613-62-7

2-benzyloxynaphthalene

Conditions
ConditionsYield
With sodium hydroxide; phosphonium resin In dichloromethane; water for 48h; Ambient temperature;96%
With potassium carbonate In acetonitrile Reflux;93%
With caesium carbonate In acetonitrile for 5h; Heating;92%
benzyl chloride
100-44-7

benzyl chloride

β-naphthol
135-19-3

β-naphthol

2-benzyloxynaphthalene
613-62-7

2-benzyloxynaphthalene

Conditions
ConditionsYield
With potassium hydroxide; 3-butyl-1-methyl-1H-imidazol-3-ium hexafluorophosphate at 25℃; for 2h; Williamson synthesis;93%
With sodium hydroxide; diphenylether; tetrabutylammomium bromide In water; toluene at 90℃; for 3h; low energy microwave irradiation;92%
copper; copper dichloride for 0.0333333h; Alkylation; Irradiation;90%
2-bromonaphthalene
580-13-2

2-bromonaphthalene

benzyl alcohol
100-51-6

benzyl alcohol

2-benzyloxynaphthalene
613-62-7

2-benzyloxynaphthalene

Conditions
ConditionsYield
With copper(l) iodide; sodium carbonate; 2-(pyrrolidin-1-yl)acetic acid In N,N-dimethyl-formamide at 100℃; Reagent/catalyst; Solvent;93%
With potassium tert-butylate; C11H21ClN2NiO; bis(pinacol)diborane In toluene at 60℃; for 24h;51%
With potassium tert-butylate In 1-methyl-pyrrolidin-2-one at 200℃; for 0.75h; Microwave irradiation;35%
7-(benzyloxy)-naphthalen-2-yl-4-methylbenzenesulfonate

7-(benzyloxy)-naphthalen-2-yl-4-methylbenzenesulfonate

2-benzyloxynaphthalene
613-62-7

2-benzyloxynaphthalene

Conditions
ConditionsYield
With dimethylamine borane; potassium carbonate; triphenylphosphine; nickel In N,N-dimethyl-formamide at 120℃; for 6h;92%
1-bromo-2-(phenylmethoxy)naphthalene
41908-23-0

1-bromo-2-(phenylmethoxy)naphthalene

(R)-2,2'-bis(benzyloxy)-1,1'-binaphthalene

(R)-2,2'-bis(benzyloxy)-1,1'-binaphthalene

B

2-benzyloxynaphthalene
613-62-7

2-benzyloxynaphthalene

Conditions
ConditionsYield
With (1,2-dimethoxyethane)dichloronickel(II); (3aS,8aR)-2-(6-cyclohexylpyridin-2-yl)-3a,8a-dihydro-8H-indeno[1,2-d]oxazole; sodium iodide In N,N-dimethyl-formamide at 0℃; for 36h; Reagent/catalyst; Temperature; Electrochemical reaction; Molecular sieve; Glovebox; enantioselective reaction;A 88%
B 10 %Spectr.
With (1,2-dimethoxyethane)dichloronickel(II); (3aS,8aR)-2-(6-cyclohexylpyridin-2-yl)-3a,8a-dihydro-8H-indeno[1,2-d]oxazole; sodium iodide In N,N-dimethyl-formamide at 15℃; for 12h; Reagent/catalyst; Electrochemical reaction; Glovebox; enantioselective reaction;A 10 %Spectr.
B 85 %Spectr.
benzyloxydiphenylphosphine
53772-44-4

benzyloxydiphenylphosphine

β-naphthol
135-19-3

β-naphthol

2-benzyloxynaphthalene
613-62-7

2-benzyloxynaphthalene

Conditions
ConditionsYield
With 2,6-dimethyl-1,4-benzoquinone In dichloromethane at 20℃; for 0.5h;84%
With 2,6-dimethyl-1,4-benzoquinone In dichloromethane at 20℃; for 0.5h;84%
6-benzyloxy-2-bromonaphthalene
2234-45-9

6-benzyloxy-2-bromonaphthalene

2-benzyloxynaphthalene
613-62-7

2-benzyloxynaphthalene

Conditions
ConditionsYield
With sodium hydride; lithium iodide In tetrahydrofuran; mineral oil at 50℃; for 8h; Sealed tube;79%
N,N,N-­trimethyl-­1-­phenylmethanaminium trifluoromethanesulfonate
260783-80-0

N,N,N-­trimethyl-­1-­phenylmethanaminium trifluoromethanesulfonate

β-naphthol
135-19-3

β-naphthol

2-benzyloxynaphthalene
613-62-7

2-benzyloxynaphthalene

Conditions
ConditionsYield
With 18-crown-6 ether; potassium tert-butylate In toluene at 120℃; for 3h; Schlenk technique; Inert atmosphere;75%
benzyltrimethylammonium chloride
56-93-9

benzyltrimethylammonium chloride

β-naphthol
135-19-3

β-naphthol

A

2-Methoxynaphthalene
93-04-9

2-Methoxynaphthalene

B

2-benzyloxynaphthalene
613-62-7

2-benzyloxynaphthalene

Conditions
ConditionsYield
With diethylene glycol dimethyl ether; potassium carbonate at 155℃; for 6h;A n/a
B 73%
N-benzyl-N,N,N-triethylammonium chloride
56-37-1

N-benzyl-N,N,N-triethylammonium chloride

β-naphthol
135-19-3

β-naphthol

2-benzyloxynaphthalene
613-62-7

2-benzyloxynaphthalene

Conditions
ConditionsYield
With diethylene glycol dimethyl ether; potassium carbonate at 155℃; for 6h; optical yield given as %de;47%
benzyl chloride
100-44-7

benzyl chloride

β-naphthol
135-19-3

β-naphthol

A

2-benzyloxynaphthalene
613-62-7

2-benzyloxynaphthalene

B

1-benzyl-2-naphthol
36441-31-3

1-benzyl-2-naphthol

Conditions
ConditionsYield
With sodium hydroxide; 1-cetyl-4-aza-1-azonia bicyclo[2.2.2]octane chloride In Petroleum ether at 25℃; for 15h;A 36%
B 30%
phenyldiazomethane
908094-04-2

phenyldiazomethane

β-naphthol
135-19-3

β-naphthol

2-benzyloxynaphthalene
613-62-7

2-benzyloxynaphthalene

benzyl bromide
100-39-0

benzyl bromide

sodium 2-naphtholate
875-83-2

sodium 2-naphtholate

2-benzyloxynaphthalene
613-62-7

2-benzyloxynaphthalene

Conditions
ConditionsYield
With acetone
benzyl bromide
100-39-0

benzyl bromide

A

2-benzyloxynaphthalene
613-62-7

2-benzyloxynaphthalene

B

1-benzyl-2-naphthol
36441-31-3

1-benzyl-2-naphthol

Conditions
ConditionsYield
With 1,4-dioxane; lithium
sodium 2-naphtholate
875-83-2

sodium 2-naphtholate

A

2-benzyloxynaphthalene
613-62-7

2-benzyloxynaphthalene

B

1-benzyl-2-naphthol
36441-31-3

1-benzyl-2-naphthol

Conditions
ConditionsYield
With 1,4-dioxane
sodium 2-naphtholate
875-83-2

sodium 2-naphtholate

benzyl chloride
100-44-7

benzyl chloride

A

2-benzyloxynaphthalene
613-62-7

2-benzyloxynaphthalene

B

1-benzyl-2-naphthol
36441-31-3

1-benzyl-2-naphthol

Conditions
ConditionsYield
With water at 110℃;
benzyldimethylphenylammonium chloride
3204-68-0

benzyldimethylphenylammonium chloride

β-naphthol
135-19-3

β-naphthol

2-benzyloxynaphthalene
613-62-7

2-benzyloxynaphthalene

Conditions
ConditionsYield
With sodium hydroxide
benzyltrimethylammonium iodide
4525-46-6

benzyltrimethylammonium iodide

β-naphthol
135-19-3

β-naphthol

2-benzyloxynaphthalene
613-62-7

2-benzyloxynaphthalene

Conditions
ConditionsYield
In N,N-dimethyl-formamide
benzyl bromide
100-39-0

benzyl bromide

sodium 2-naphtholate
875-83-2

sodium 2-naphtholate

A

2-benzyloxynaphthalene
613-62-7

2-benzyloxynaphthalene

B

1-benzyl-2-naphthol
36441-31-3

1-benzyl-2-naphthol

Conditions
ConditionsYield
In various solvent(s) at 87℃; for 2h;A 97 % Spectr.
B 3 % Spectr.
In various solvent(s) at 87℃; for 2h; molten tetraalkylammonium or -phosphonium halides as solvents; highly regioselective O-alkylation; reaction with benzyl chloride;A 97 % Spectr.
B 3 % Spectr.
benzyl chloride
100-44-7

benzyl chloride

β-naphthol
135-19-3

β-naphthol

A

1,1-dibenzyl-1,2-dihydronaphthalen-2-one
74849-12-0

1,1-dibenzyl-1,2-dihydronaphthalen-2-one

B

2-benzyloxynaphthalene
613-62-7

2-benzyloxynaphthalene

C

1-benzyl-2-naphthol
36441-31-3

1-benzyl-2-naphthol

D

1-Benzyl-2-naphthyl-benzyl-aether
95391-89-2

1-Benzyl-2-naphthyl-benzyl-aether

Conditions
ConditionsYield
With aluminum oxide; sodium methylate at 50℃; for 48h; Yield given. Yields of byproduct given;
β-naphthol
135-19-3

β-naphthol

benzyl alcohol
100-51-6

benzyl alcohol

2-benzyloxynaphthalene
613-62-7

2-benzyloxynaphthalene

Conditions
ConditionsYield
With dicyclohexyl-carbodiimide
sodium 2-naphtholate
875-83-2

sodium 2-naphtholate

A

1,1-dibenzyl-1,2-dihydronaphthalen-2-one
74849-12-0

1,1-dibenzyl-1,2-dihydronaphthalen-2-one

B

2-benzyloxynaphthalene
613-62-7

2-benzyloxynaphthalene

C

1-benzyl-2-naphthol
36441-31-3

1-benzyl-2-naphthol

D

1-Benzyl-2-naphthyl-benzyl-aether
95391-89-2

1-Benzyl-2-naphthyl-benzyl-aether

Conditions
ConditionsYield
With PhCH2X; N-benzyl-N,N,N-triethylammonium chloride In toluene at 20 - 90℃; for 1h; Product distribution; influence of catalyst, its concentration, and temperature on C/O-alkylation ratio;
2-naphtholate
15147-55-4

2-naphtholate

benzyl chloride
100-44-7

benzyl chloride

2-benzyloxynaphthalene
613-62-7

2-benzyloxynaphthalene

Conditions
ConditionsYield
With tetrabutylammonium perchlorate In acetonitrile at 22℃; Rate constant;
potassium 2-naphthoxide
36294-21-0

potassium 2-naphthoxide

benzyl chloride
100-44-7

benzyl chloride

2-benzyloxynaphthalene
613-62-7

2-benzyloxynaphthalene

Conditions
ConditionsYield
With tetrabutylammonium tetrafluoroborate In dimethyl sulfoxide at 20℃; Kinetics; Substitution; Electrolysis;
benzyl chloride
100-44-7

benzyl chloride

β-naphthol
135-19-3

β-naphthol

aqueous alcoholic KOH-solution

aqueous alcoholic KOH-solution

2-benzyloxynaphthalene
613-62-7

2-benzyloxynaphthalene

β-naphthol
135-19-3

β-naphthol

sodium benzyl isodiazotate

sodium benzyl isodiazotate

2-benzyloxynaphthalene
613-62-7

2-benzyloxynaphthalene

Conditions
ConditionsYield
With ethanol
2-benzyloxynaphthalene
613-62-7

2-benzyloxynaphthalene

A

toluene
108-88-3

toluene

B

β-naphthol
135-19-3

β-naphthol

Conditions
ConditionsYield
With 0.5%Pd/TiO2; isopropyl alcohol In water at 24.84℃; for 2h; Inert atmosphere; Sealed tube; Irradiation;A 99%
B 97%
2-benzyloxynaphthalene
613-62-7

2-benzyloxynaphthalene

1-nitonaphthalen-2-yl benzoate
72771-44-9

1-nitonaphthalen-2-yl benzoate

Conditions
ConditionsYield
With ammonium cerium(IV) nitrate In acetic acid at 60 - 80℃; for 1.5h;97%
With ammonium cerium(IV) nitrate In acetic acid at 70 - 80℃; for 0.5h;1.92 g
2-benzyloxynaphthalene
613-62-7

2-benzyloxynaphthalene

C26H11Co2F13O8

C26H11Co2F13O8

C26H16Co2O7

C26H16Co2O7

Conditions
ConditionsYield
With C20H12AuF9NO4PS2 at 20℃; for 0.25h; Nicholas Reaction; Inert atmosphere; Molecular sieve;96%
2-benzyloxynaphthalene
613-62-7

2-benzyloxynaphthalene

β-naphthol
135-19-3

β-naphthol

Conditions
ConditionsYield
With triethylammonium formate; palladium on activated charcoal for 0.166667h; Ambient temperature;95%
With biphenyl; lithium In tetrahydrofuran; methanol at -78℃; for 40h;71%
With hydrogen; palladium diacetate; pyrographite In tetrahydrofuran; methanol at 25℃; under 760.051 Torr; for 12h;66%
2-benzyloxynaphthalene
613-62-7

2-benzyloxynaphthalene

2-(deuterio(phenyl)methoxy)naphthalene

2-(deuterio(phenyl)methoxy)naphthalene

Conditions
ConditionsYield
Stage #1: 2-benzyloxynaphthalene With tert.-butyl lithium In tetrahydrofuran; pentane at -78℃; for 0.416667h; Schlenk technique; Inert atmosphere;
Stage #2: With deuteromethanol In tetrahydrofuran; water; pentane Schlenk technique; Inert atmosphere;
91%
Acetyl bromide
506-96-7

Acetyl bromide

2-benzyloxynaphthalene
613-62-7

2-benzyloxynaphthalene

naphthalen-2-yl acetate
1523-11-1

naphthalen-2-yl acetate

Conditions
ConditionsYield
With lithium bromide In dichloromethane at 30 - 35℃; for 24h; Inert atmosphere;90%
2-benzyloxynaphthalene
613-62-7

2-benzyloxynaphthalene

(2,3-dimethoxyphenyl)(phenyl)methanol
56139-07-2

(2,3-dimethoxyphenyl)(phenyl)methanol

Conditions
ConditionsYield
Stage #1: 2-benzyloxynaphthalene With tert.-butyl lithium In tetrahydrofuran; pentane at -78 - -55℃; for 0.75h; Wittig Rearrangement; Schlenk technique; Inert atmosphere;
Stage #2: With deuteromethanol; water In tetrahydrofuran; pentane at -55 - -30℃; Wittig Rearrangement; Schlenk technique; Inert atmosphere;
88%
2-benzyloxynaphthalene
613-62-7

2-benzyloxynaphthalene

6-(benzyloxy)-1,2,3,4-tetrahydronaphthalene

6-(benzyloxy)-1,2,3,4-tetrahydronaphthalene

Conditions
ConditionsYield
With hydrogen In tert-butyl alcohol at 135℃; for 40h; Autoclave;83%
2-benzyloxynaphthalene
613-62-7

2-benzyloxynaphthalene

C13H12N(1+)

C13H12N(1+)

N-(2-(naphthalen-2-yloxy)-1,2-diphenylethyl)aniline

N-(2-(naphthalen-2-yloxy)-1,2-diphenylethyl)aniline

Conditions
ConditionsYield
Stage #1: 2-benzyloxynaphthalene With tert.-butyl lithium In tetrahydrofuran; pentane at -78℃; for 0.416667h; Schlenk technique; Inert atmosphere;
Stage #2: C13H12N(1+) In tetrahydrofuran; pentane at -78 - 20℃; Schlenk technique; Inert atmosphere; diastereoselective reaction;
79%
2-benzyloxynaphthalene
613-62-7

2-benzyloxynaphthalene

ethylamine
75-04-7

ethylamine

1-ethylamino-2-benzyloxy-1,4-dihydronaphthalene

1-ethylamino-2-benzyloxy-1,4-dihydronaphthalene

Conditions
ConditionsYield
With benzene-1,3-dicarbonitrile In water; acetonitrile for 12h; Irradiation;76%
2-benzyloxynaphthalene
613-62-7

2-benzyloxynaphthalene

ammonium thiocyanate
1147550-11-5

ammonium thiocyanate

C18H13NOS

C18H13NOS

Conditions
ConditionsYield
With oxygen; Nitrogen dioxide; trifluoroacetic acid In acetonitrile at 15℃; for 3h;76%
2-benzyloxynaphthalene
613-62-7

2-benzyloxynaphthalene

isopropylamine
75-31-0

isopropylamine

2-benzyloxy-1-isopropylamino-1,4-dihydronaphthalene

2-benzyloxy-1-isopropylamino-1,4-dihydronaphthalene

Conditions
ConditionsYield
With benzene-1,3-dicarbonitrile In water; acetonitrile for 10h; Irradiation;71%
2-benzyloxynaphthalene
613-62-7

2-benzyloxynaphthalene

potassium thioacyanate
333-20-0

potassium thioacyanate

2-(benzyloxy)naphthalene-1-carbonitrile
52805-40-0

2-(benzyloxy)naphthalene-1-carbonitrile

Conditions
ConditionsYield
With silica sulfuric acid In neat (no solvent, solid phase) at 100℃; for 12h; regioselective reaction;71%
propylamine
107-10-8

propylamine

2-benzyloxynaphthalene
613-62-7

2-benzyloxynaphthalene

2-benzyloxy-1-propylamino-1,4-dihydronaphthalene

2-benzyloxy-1-propylamino-1,4-dihydronaphthalene

Conditions
ConditionsYield
With benzene-1,3-dicarbonitrile In water; acetonitrile for 10h; Irradiation;68%
benzoic acid ethyl ester
93-89-0

benzoic acid ethyl ester

2-benzyloxynaphthalene
613-62-7

2-benzyloxynaphthalene

2-(naphthalen-2-yloxy)-1,2-diphenylethanone

2-(naphthalen-2-yloxy)-1,2-diphenylethanone

Conditions
ConditionsYield
Stage #1: 2-benzyloxynaphthalene With tert.-butyl lithium In tetrahydrofuran; pentane at -78℃; for 0.416667h; Schlenk technique; Inert atmosphere;
Stage #2: benzoic acid ethyl ester In tetrahydrofuran; pentane at -78 - 20℃; Schlenk technique; Inert atmosphere;
66%
2-benzyloxynaphthalene
613-62-7

2-benzyloxynaphthalene

1-bromo-2-(phenylmethoxy)naphthalene
41908-23-0

1-bromo-2-(phenylmethoxy)naphthalene

Conditions
ConditionsYield
With aluminum tri-bromide; [bis(acetoxy)iodo]benzene In acetonitrile at 23℃;62%
With sulfuric acid; dihydrogen peroxide; potassium bromide weiteres Reagens: Aethanol;
With bromine
formaldehyd
50-00-0

formaldehyd

4-fluorobenzoic acid ethyl ester
451-46-7

4-fluorobenzoic acid ethyl ester

2-benzyloxynaphthalene
613-62-7

2-benzyloxynaphthalene

(1R*,2S*)-1-(4-fluorophenyl)-2-(naphthalen-2-yloxy)-2-phenylpropane-1,3-diol

(1R*,2S*)-1-(4-fluorophenyl)-2-(naphthalen-2-yloxy)-2-phenylpropane-1,3-diol

Conditions
ConditionsYield
Stage #1: 2-benzyloxynaphthalene With tert.-butyl lithium In tetrahydrofuran; pentane at -78 - -70℃; for 0.5h; Inert atmosphere;
Stage #2: 4-fluorobenzoic acid ethyl ester In tetrahydrofuran; pentane at -70 - 20℃; for 1.08333h; Inert atmosphere;
Stage #3: formaldehyd In tetrahydrofuran; pentane at 20℃; for 2h; Inert atmosphere;
62%
2-benzyloxynaphthalene
613-62-7

2-benzyloxynaphthalene

methylamine
74-89-5

methylamine

2-benzyloxy-1-methylamino-1,4-dihydronaphthalene
149438-75-5

2-benzyloxy-1-methylamino-1,4-dihydronaphthalene

Conditions
ConditionsYield
With benzene-1,3-dicarbonitrile In water; acetonitrile for 10h; Irradiation;60%

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