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614-33-5

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  • High Quality 99% 614-33-5 Glycerol tribenzoate; 1,2,3-Propanetriol, 1,2,3-tribenzoate; 1,2,3-Propanetriol, tribenzoate; Tribenzoin; propane-1,2,3-triyl tribenzoate. Manufacturer

    Cas No: 614-33-5

  • USD $ 0.1-0.1 / Gram

  • 1 Gram

  • 100 Metric Ton/Year

  • Xi'an Xszo Chem Co., Ltd.
  • Contact Supplier

614-33-5 Usage

Chemical Properties

Glyceryl tribenzoate has a little or no odor.

Uses

Plasticizer

Check Digit Verification of cas no

The CAS Registry Mumber 614-33-5 includes 6 digits separated into 3 groups by hyphens. The first part of the number,starting from the left, has 3 digits, 6,1 and 4 respectively; the second part has 2 digits, 3 and 3 respectively.
Calculate Digit Verification of CAS Registry Number 614-33:
(5*6)+(4*1)+(3*4)+(2*3)+(1*3)=55
55 % 10 = 5
So 614-33-5 is a valid CAS Registry Number.
InChI:InChI=1/C24H20O6/c25-22(18-10-4-1-5-11-18)28-16-21(30-24(27)20-14-8-3-9-15-20)17-29-23(26)19-12-6-2-7-13-19/h1-15,21H,16-17H2

614-33-5SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 19, 2017

Revision Date: Aug 19, 2017

1.Identification

1.1 GHS Product identifier

Product name 2,3-dibenzoyloxypropyl benzoate

1.2 Other means of identification

Product number -
Other names EINECS 210-379-6

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only. Food additives -> Flavoring Agents
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:614-33-5 SDS

614-33-5Synthetic route

glycerol
56-81-5

glycerol

benzoic acid
65-85-0

benzoic acid

glyceryl tribenzoate
614-33-5

glyceryl tribenzoate

Conditions
ConditionsYield
With calcium hydroxide In 5,5-dimethyl-1,3-cyclohexadiene; decane at 220℃; for 1h; Solvent; Reagent/catalyst; Reflux; Large scale;99.2%
With H2SO4/TiO2-La2O3-solid acid catalyst at 185 - 195℃; for 12h;88.6%
at 200℃; anschl. auf 270grad;
at 200℃; dann auf 270grad im Druckrohr erhitzen;
With silicate-catalyst at 200 - 220℃; unter Entfernen des entstehenden Wassers;
benzoyl chloride
98-88-4

benzoyl chloride

glycerol
56-81-5

glycerol

glyceryl tribenzoate
614-33-5

glyceryl tribenzoate

Conditions
ConditionsYield
With dmap; triethylamine In dichloromethane at 20℃; for 16h; Cooling with ice;70%
pyridine
110-86-1

pyridine

benzoyl chloride
98-88-4

benzoyl chloride

glycerol
56-81-5

glycerol

glyceryl tribenzoate
614-33-5

glyceryl tribenzoate

benzoyl chloride
98-88-4

benzoyl chloride

furan-2,3,5(4H)-trione pyridine (1:1)

furan-2,3,5(4H)-trione pyridine (1:1)

(R,S)-2,2-dimethyl-1,3-dioxolane-4-methanol
100-79-8

(R,S)-2,2-dimethyl-1,3-dioxolane-4-methanol

glyceryl tribenzoate
614-33-5

glyceryl tribenzoate

1,2,3-tribromopropane
96-11-7

1,2,3-tribromopropane

Potassium benzoate
582-25-2

Potassium benzoate

glyceryl tribenzoate
614-33-5

glyceryl tribenzoate

Conditions
ConditionsYield
at 200℃;
2-hydroxy-2-phenylacetophenone
119-53-9

2-hydroxy-2-phenylacetophenone

benzoic acid
65-85-0

benzoic acid

glyceryl tribenzoate
614-33-5

glyceryl tribenzoate

Conditions
ConditionsYield
at 250℃;
2,3-dihydroxypropyl benzoate
3376-59-8

2,3-dihydroxypropyl benzoate

benzoyl chloride
98-88-4

benzoyl chloride

furan-2,3,5(4H)-trione pyridine (1:1)

furan-2,3,5(4H)-trione pyridine (1:1)

glyceryl tribenzoate
614-33-5

glyceryl tribenzoate

benzoyl chloride
98-88-4

benzoyl chloride

furan-2,3,5(4H)-trione pyridine (1:1)

furan-2,3,5(4H)-trione pyridine (1:1)

glycerol
56-81-5

glycerol

glyceryl tribenzoate
614-33-5

glyceryl tribenzoate

benzoic acid anhydride
93-97-0

benzoic acid anhydride

glycerol
56-81-5

glycerol

glyceryl tribenzoate
614-33-5

glyceryl tribenzoate

Conditions
ConditionsYield
at 200℃;
at 200℃;
1,2,3-tribromopropane
96-11-7

1,2,3-tribromopropane

benzoic acid
65-85-0

benzoic acid

glyceryl tribenzoate
614-33-5

glyceryl tribenzoate

Conditions
ConditionsYield
at 200℃; bei der Einwirkung auf Kaliumbenzoat;
benzoic acid anhydride
93-97-0

benzoic acid anhydride

epichlorohydrin
106-89-8

epichlorohydrin

glyceryl tribenzoate
614-33-5

glyceryl tribenzoate

Conditions
ConditionsYield
im geschlossenen Rohr;
2-benzoyloxypropane-1,3-diol
3376-49-6

2-benzoyloxypropane-1,3-diol

benzoyl chloride
98-88-4

benzoyl chloride

A

glyceryl tribenzoate
614-33-5

glyceryl tribenzoate

B

2,3-bis-benzoyloxy-propan-1-ol
76999-62-7

2,3-bis-benzoyloxy-propan-1-ol

C

benzoic acid 3-hexanoyloxy-2-hydroxypropyl ester
40593-13-3

benzoic acid 3-hexanoyloxy-2-hydroxypropyl ester

Conditions
ConditionsYield
With (S)-1-methyl-2-((morpholin-1-yl)methyl)pyrrolidine; (methylcyclopentadienyl)tin(II) chloride 1.) CH2Cl2, 0 deg C, 30 min, 2.) CH2Cl2, 5 min, 3.) CH2Cl2, 0 deg C, 1h,; Yield given. Multistep reaction. Yields of byproduct given;
sodium benzoate
532-32-1

sodium benzoate

benzoic acid-<β.β'-dichloro-isopropyl>-ester

benzoic acid-<β.β'-dichloro-isopropyl>-ester

glyceryl tribenzoate
614-33-5

glyceryl tribenzoate

Conditions
ConditionsYield
at 180 - 200℃;
at 180 - 200℃;
benzoyl chloride
98-88-4

benzoyl chloride

disodium salt of glycerol

disodium salt of glycerol

glyceryl tribenzoate
614-33-5

glyceryl tribenzoate

Conditions
ConditionsYield
With diethyl ether
1-benzoylimidazole
10364-94-0

1-benzoylimidazole

glycerol
56-81-5

glycerol

glyceryl tribenzoate
614-33-5

glyceryl tribenzoate

Conditions
ConditionsYield
With triethylamine In tetrahydrofuran for 48h;
benzoic acid
65-85-0

benzoic acid

glyceryl tribenzoate
614-33-5

glyceryl tribenzoate

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: tetrahydrofuran / 2 h
2: triethylamine / tetrahydrofuran / 48 h
View Scheme
methanol
67-56-1

methanol

glyceryl tribenzoate
614-33-5

glyceryl tribenzoate

benzoic acid methyl ester
93-58-3

benzoic acid methyl ester

Conditions
ConditionsYield
With Merrifield resin-supported N3=P(MeNCH2CH2)3N at 23 - 25℃; for 0.2h; Inert atmosphere;95%
glyceryl tribenzoate
614-33-5

glyceryl tribenzoate

titanium tetrachloride
7550-45-0

titanium tetrachloride

[{(TiCl4)2(glycerol tribenzoate)}2]

[{(TiCl4)2(glycerol tribenzoate)}2]

Conditions
ConditionsYield
In hexane for 2h; Inert atmosphere; Schlenk technique;75%
glyceryl tribenzoate
614-33-5

glyceryl tribenzoate

saccharin
81-07-2

saccharin

C24H19NO7S

C24H19NO7S

Conditions
ConditionsYield
With scandium tris(trifluoromethanesulfonate) at 150℃; for 24h; Sealed tube;75%
ethanol
64-17-5

ethanol

glyceryl tribenzoate
614-33-5

glyceryl tribenzoate

sodium ethanolate
141-52-6

sodium ethanolate

benzoic acid ethyl ester
93-89-0

benzoic acid ethyl ester

pyridine
110-86-1

pyridine

glyceryl tribenzoate
614-33-5

glyceryl tribenzoate

sodium ethanolate
141-52-6

sodium ethanolate

glycerol
56-81-5

glycerol

A

glycerol monobenzoate

glycerol monobenzoate

B

glycerol dibenzoate

glycerol dibenzoate

ethanol
64-17-5

ethanol

glyceryl tribenzoate
614-33-5

glyceryl tribenzoate

alkali

alkali

A

2,3-bis-benzoyloxy-propan-1-ol
76999-62-7

2,3-bis-benzoyloxy-propan-1-ol

B

2-hydroxy-2-phenylacetophenone
119-53-9

2-hydroxy-2-phenylacetophenone

ethanol
64-17-5

ethanol

glyceryl tribenzoate
614-33-5

glyceryl tribenzoate

alkali

alkali

A

sodium benzoate
532-32-1

sodium benzoate

B

benzoic acid ethyl ester
93-89-0

benzoic acid ethyl ester

C

glycerol
56-81-5

glycerol

glyceryl tribenzoate
614-33-5

glyceryl tribenzoate

N-(2-hydroxyethyl)-benzamide
18838-10-3

N-(2-hydroxyethyl)-benzamide

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: Merrifield resin-supported N3=P(MeNCH2CH2)3N / 0.2 h / 23 - 25 °C / Inert atmosphere
2: Merrifield resin-supported N3=P(MeNCH2CH2)3N / tetrahydrofuran / 23 - 25 °C / Inert atmosphere
View Scheme
glyceryl tribenzoate
614-33-5

glyceryl tribenzoate

aniline
62-53-3

aniline

N-Benzylaniline
758640-21-0

N-Benzylaniline

Conditions
ConditionsYield
With tris(2,4-pentanedionato)ruthenium(III); hydrogen; bis(trifluoromethanesulfonyl)amide; [2-((diphenylphospino)methyl)-2-methyl-1,3-propanediyl]bis[diphenylphosphine] In tetrahydrofuran at 130℃; under 45004.5 Torr; for 18h; Autoclave;87 %Chromat.

614-33-5Relevant articles and documents

Method for preparing amino alcohol derivative

-

Paragraph 0084; 0085; 0086, (2018/11/22)

The invention provides a method for preparing an amino alcohol derivative. The method is characterized in that substitution reaction is carried out on ester groups of dihydric alcohol carboxylic esteror polyhydric alcohol carboxylic ester to obtain the amino alcohol derivative, wherein the amidogen is derived into sulfonamido, and at least one carboxylic ester group remains. The method for preparing the amino alcohol derivative has the advantages that the raw materials are cheap and obtained easily, the use quantity of catalysts is low, the reaction condition is simple, and the selectivity ofproducts is high.

A solid acid catalysis of the preparation process of benzoic acid ester plasticizer (by machine translation)

-

Paragraph 0030; 0031, (2017/07/05)

The present invention discloses a solid acidify catalytic benzoic acid ester plasticizer of the preparation process, the preparation method is: to benzoic acid and alcohol as the raw material, with agent and catalyst in direct reaction to produce benzoic acid ester compound; catalytic system of the invention compared with the sulfuric acid, toluene sulfonic acid and sulfuric acid to sodium has a better catalytic activity, so the catalyst less consumption, in addition, because of the use of the is supported on a solid acid catalyst, after the reaction directly filtering can realize the separation of the catalyst, and the catalyst can be reused, makes the production process more simple, and can be basically prevent the generation of waste water, makes the production process more green environmental protection. (by machine translation)

Evaluation of glycerol profiles in sugarcane spirits (cacha?as)

Garcia, André C.,Serafim, Felipe A. T.,Keukeleire, Denis De,Franco, Douglas W.

, p. 57 - 63 (2015/02/19)

A new method for glycerol quantification in sugarcane spirits (cacha?as) is proposed, based on sample derivatization using benzoyl chloride followed by solid-phase extraction and high performance liquid chromatography with diode array detection analysis. The limits of detection and quantification for glycerol analysis are 0.25 mg L -1 and 0.74 mg L-1, respectively. The accuracy is of 97.5percent, the precision 93.5percent and the linearity r2 = 0.998 in the range of 0.56 mg L-1 to 112.0 mg L-1of glycerol. Experiments with forty eight samples of aged and non-aged cacha?as and seven alcoholic extracts of wood showed that the aging process contributes to increase the glycerol concentration. The average concentration of glycerol in aged cacha?as were about 10-fold higher than in non-aged cacha?as.

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