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928-45-0 Usage

Chemical Properties

Colourless Oil

Check Digit Verification of cas no

The CAS Registry Mumber 928-45-0 includes 6 digits separated into 3 groups by hyphens. The first part of the number,starting from the left, has 3 digits, 9,2 and 8 respectively; the second part has 2 digits, 4 and 5 respectively.
Calculate Digit Verification of CAS Registry Number 928-45:
(5*9)+(4*2)+(3*8)+(2*4)+(1*5)=90
90 % 10 = 0
So 928-45-0 is a valid CAS Registry Number.
InChI:InChI=1/C4H9NO3/c1-2-3-4-8-5(6)7/h2-4H2,1H3

928-45-0SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 13, 2017

Revision Date: Aug 13, 2017

1.Identification

1.1 GHS Product identifier

Product name butyl nitrate

1.2 Other means of identification

Product number -
Other names Nitric acid, butyl ester

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only.
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:928-45-0 SDS

928-45-0Synthetic route

butan-1-ol
71-36-3

butan-1-ol

butyl nitrate
928-45-0

butyl nitrate

Conditions
ConditionsYield
With N-nitro-2,4,6-trimethylpyridinium tetrafluoroborate In acetonitrile at 0℃; for 2h;100%
With carbon dioxide; dinitrogen pentoxide at 0℃; under 45004.5 - 60006 Torr; for 0.5h; Autoclave;94%
With nitric acid; urea; europium(III) trifluoromethanesulfonate In cyclohexane at 80℃; for 10h; Schlenk technique;90%
N-Butyl-2,4,6-triphenylpyridinium nitrate
73377-40-9

N-Butyl-2,4,6-triphenylpyridinium nitrate

butyl nitrate
928-45-0

butyl nitrate

Conditions
ConditionsYield
at 250℃; under 760 Torr; for 3h;50%
1-bromo-butane
109-65-9

1-bromo-butane

butyl nitrate
928-45-0

butyl nitrate

Conditions
ConditionsYield
With silver nitrate; acetonitrile
With silver nitrate In acetonitrile
1-iodo-butane
542-69-8

1-iodo-butane

butyl nitrate
928-45-0

butyl nitrate

Conditions
ConditionsYield
With silver nitrate; acetonitrile
With nitric acid at -10℃;
ethene
74-85-1

ethene

butyl nitrate
928-45-0

butyl nitrate

Conditions
ConditionsYield
With nitric acid Electrolysis.an Platinanoden;
sodium butanolate
2372-45-4

sodium butanolate

butyl nitrate
928-45-0

butyl nitrate

Conditions
ConditionsYield
With dichloromethane; dinitrogen tetraoxide; butan-1-ol at -80℃;
1-picryl-pyridinium; nitrate

1-picryl-pyridinium; nitrate

butan-1-ol
71-36-3

butan-1-ol

butyl nitrate
928-45-0

butyl nitrate

butyl-nitro-amine; ammonium salt
69153-16-8

butyl-nitro-amine; ammonium salt

butyl nitrate
928-45-0

butyl nitrate

Conditions
ConditionsYield
With nitrylfluoride In acetonitrile
di-n-butyloxymethane
2568-90-3

di-n-butyloxymethane

A

butyl nitrate
928-45-0

butyl nitrate

B

n-butoxymethyl-nitrate
127510-61-6

n-butoxymethyl-nitrate

Conditions
ConditionsYield
With dinitrogen pentoxide In dichloromethane at 0 - 10℃;
n-butane
106-97-8

n-butane

A

n-Butyl nitrite
544-16-1

n-Butyl nitrite

B

butyl nitrate
928-45-0

butyl nitrate

C

sec-butyl nitrite
924-43-6

sec-butyl nitrite

D

2-nitrobutane
600-24-8, 116783-22-3

2-nitrobutane

E

2-butyl nitrate
924-52-7

2-butyl nitrate

F

1-nitrobutane
627-05-4

1-nitrobutane

Conditions
ConditionsYield
With dihydrogen peroxide; Nitrogen dioxide at 24.9℃; under 300.02 Torr; Rate constant; Product distribution; Mechanism; boric-acid-coated surface; various pressure and carrier-gas composition;A 6 % Chromat.
B 0.3 % Chromat.
C 31 % Chromat.
D 51 % Chromat.
E 3 % Chromat.
F 7 % Chromat.
n-butane
106-97-8

n-butane

A

butyl nitrate
928-45-0

butyl nitrate

B

2-butyl nitrate
924-52-7

2-butyl nitrate

Conditions
ConditionsYield
With methyl nitrite; ultra-zero air; nitrogen(II) oxide at 25.9℃; for 0.333333h; Product distribution; Rate constant; Irradiation; other alkyl peroxy radical generator (Cl2);
n-butane
106-97-8

n-butane

A

butyl nitrate
928-45-0

butyl nitrate

B

sec-butyl nitrite
924-43-6

sec-butyl nitrite

C

2-nitrobutane
600-24-8, 116783-22-3

2-nitrobutane

D

2-butyl nitrate
924-52-7

2-butyl nitrate

E

butyraldehyde
123-72-8

butyraldehyde

F

butanone
78-93-3

butanone

Conditions
ConditionsYield
With dihydrogen peroxide; oxygen; Nitrogen dioxide at 24.9℃; under 300.02 Torr; Rate constant; Product distribution; Mechanism; boric-acid-coated surface; various O2 concn.;
pentanal
110-62-3

pentanal

A

butyl nitrate
928-45-0

butyl nitrate

B

peroxyacetyl nitrate
2278-22-0

peroxyacetyl nitrate

C

peroxy-n-butyryl nitrate

peroxy-n-butyryl nitrate

D

n-pentanoyl peroxynitrate
154292-37-2

n-pentanoyl peroxynitrate

Conditions
ConditionsYield
With air; nitrogen(II) oxide Nitration; sunlight; Further byproducts given. Title compound not separated from byproducts;
peroxypentanoic acid
28384-48-7

peroxypentanoic acid

A

methyl nitrate
598-58-3

methyl nitrate

B

butyl nitrate
928-45-0

butyl nitrate

C

peroxyacetyl nitrate
2278-22-0

peroxyacetyl nitrate

D

n-pentanoyl peroxynitrate
154292-37-2

n-pentanoyl peroxynitrate

Conditions
ConditionsYield
With nitric acid In dodecane Nitration; Title compound not separated from byproducts;
acetic acid
64-19-7

acetic acid

N-butylamine
109-73-9

N-butylamine

sodium nitrite

sodium nitrite

A

butyl nitrate
928-45-0

butyl nitrate

B

sec-Butyl acetate
105-46-4

sec-Butyl acetate

C

acetic acid butyl ester
123-86-4

acetic acid butyl ester

Conditions
ConditionsYield
Mechanism;
n-butane
106-97-8

n-butane

A

ethyl nitrate
625-58-1

ethyl nitrate

B

butyl nitrate
928-45-0

butyl nitrate

C

2-butyl nitrate
924-52-7

2-butyl nitrate

D

peroxyacetyl nitrate
2278-22-0

peroxyacetyl nitrate

E

peroxy-n-butyryl nitrate

peroxy-n-butyryl nitrate

F

butanone
78-93-3

butanone

G

C2H5C(O)OONO2

C2H5C(O)OONO2

Conditions
ConditionsYield
With air; Nitrogen dioxide at 25℃; for 6h; Product distribution; Mechanism; Kinetics; Irradiation; also addition of NO;A 1.3 % Chromat.
B 1.3 % Chromat.
C 16 % Chromat.
D 23 % Chromat.
E 1.3 % Chromat.
F 37 % Chromat.
G n/a
valeric acid
109-52-4

valeric acid

NaNO3

NaNO3

natrium carbonate

natrium carbonate

A

n-Butyl nitrite
544-16-1

n-Butyl nitrite

B

butyl nitrate
928-45-0

butyl nitrate

C

butyl valerate
591-68-4

butyl valerate

D

racbutanediol-(2.3)-dinitrate(?)

racbutanediol-(2.3)-dinitrate(?)

Conditions
ConditionsYield
Reaktion des Natriumsalzes; Produkt 5: Octan; Produkt 6: Octandioldinitrat.Electrolysis;
sodium proprionate
137-40-6

sodium proprionate

CaCO3

CaCO3

butyl nitrate
928-45-0

butyl nitrate

Conditions
ConditionsYield
With sodium nitrate; water Electrolysis;
(-)-1-deuterio-butylamine
70458-10-5, 119247-49-3

(-)-1-deuterio-butylamine

acetic acid
64-19-7

acetic acid

sodium nitrite

sodium nitrite

A

butyl nitrate
928-45-0

butyl nitrate

B

(+)-1-acetoxy-1-deuterio-butane

(+)-1-acetoxy-1-deuterio-butane

C

(+-)2-acetoxy-1-deuterio-butane

(+-)2-acetoxy-1-deuterio-butane

ethene
74-85-1

ethene

nitric acid
7697-37-2

nitric acid

platinum

platinum

A

ethyl nitrate
625-58-1

ethyl nitrate

B

butyl nitrate
928-45-0

butyl nitrate

C

1,2-ethyl dinitrate
628-96-6

1,2-ethyl dinitrate

D

diethylene glycol dinitrate
693-21-0

diethylene glycol dinitrate

Conditions
ConditionsYield
Electrolysis;
ethene
74-85-1

ethene

nitric acid
7697-37-2

nitric acid

acetic acid
64-19-7

acetic acid

platinum

platinum

A

ethyl nitrate
625-58-1

ethyl nitrate

B

butyl nitrate
928-45-0

butyl nitrate

C

1,2-ethyl dinitrate
628-96-6

1,2-ethyl dinitrate

D

diethylene glycol dinitrate
693-21-0

diethylene glycol dinitrate

Conditions
ConditionsYield
Electrolysis;
ethene
74-85-1

ethene

acetone
67-64-1

acetone

Ca(NO3)2

Ca(NO3)2

platinum

platinum

A

ethyl nitrate
625-58-1

ethyl nitrate

B

butyl nitrate
928-45-0

butyl nitrate

C

1,2-ethyl dinitrate
628-96-6

1,2-ethyl dinitrate

D

diethylene glycol dinitrate
693-21-0

diethylene glycol dinitrate

Conditions
ConditionsYield
Electrolysis;
ethene
74-85-1

ethene

acetic acid
64-19-7

acetic acid

NaNO3

NaNO3

platinum

platinum

A

ethyl nitrate
625-58-1

ethyl nitrate

B

butyl nitrate
928-45-0

butyl nitrate

C

1,2-ethyl dinitrate
628-96-6

1,2-ethyl dinitrate

D

diethylene glycol dinitrate
693-21-0

diethylene glycol dinitrate

Conditions
ConditionsYield
Electrolysis;
ethene
74-85-1

ethene

water
7732-18-5

water

acetone
67-64-1

acetone

NaNO3

NaNO3

platinum

platinum

A

ethyl nitrate
625-58-1

ethyl nitrate

B

butyl nitrate
928-45-0

butyl nitrate

C

1,2-ethyl dinitrate
628-96-6

1,2-ethyl dinitrate

D

diethylene glycol dinitrate
693-21-0

diethylene glycol dinitrate

Conditions
ConditionsYield
Electrolysis;
sodium proprionate
137-40-6

sodium proprionate

sodium perchlorate

sodium perchlorate

CaCO3

CaCO3

A

ethyl nitrate
625-58-1

ethyl nitrate

B

butyl nitrate
928-45-0

butyl nitrate

C

1,2-ethyl dinitrate
628-96-6

1,2-ethyl dinitrate

D

1,4-butanediol dinitrate
3457-91-8

1,4-butanediol dinitrate

Conditions
ConditionsYield
Elektrolyse an Platinanode.Electrolysis;
sodium proprionate
137-40-6

sodium proprionate

NaNO3

NaNO3

CaCO3

CaCO3

A

ethyl nitrate
625-58-1

ethyl nitrate

B

butyl nitrate
928-45-0

butyl nitrate

C

1,2-ethyl dinitrate
628-96-6

1,2-ethyl dinitrate

D

1,4-butanediol dinitrate
3457-91-8

1,4-butanediol dinitrate

Conditions
ConditionsYield
Produkt5:Aethylpropionat ;Elektrolyse an Platinanode.Electrolysis;
sodium proprionate
137-40-6

sodium proprionate

sodium sulfate

sodium sulfate

CaCO3

CaCO3

A

ethyl nitrate
625-58-1

ethyl nitrate

B

butyl nitrate
928-45-0

butyl nitrate

C

1,2-ethyl dinitrate
628-96-6

1,2-ethyl dinitrate

D

1,4-butanediol dinitrate
3457-91-8

1,4-butanediol dinitrate

Conditions
ConditionsYield
Elektrolyse an Platinanode.Electrolysis;
1-methyl-1H-imidazole
616-47-7

1-methyl-1H-imidazole

butyl nitrate
928-45-0

butyl nitrate

1-butyl-3-methylimidazolium nitrate
179075-88-8

1-butyl-3-methylimidazolium nitrate

Conditions
ConditionsYield
at 120℃; for 0.5h; Microwave irradiation;96%
In ethyl acetate for 24h; Reflux;89%
piperidine
110-89-4

piperidine

butyl nitrate
928-45-0

butyl nitrate

1-butyl-piperidine
4945-48-6

1-butyl-piperidine

Conditions
ConditionsYield
Mehrtaegiges Stehenlassen.;
butyl nitrate
928-45-0

butyl nitrate

butyraldehyde
123-72-8

butyraldehyde

Conditions
ConditionsYield
zersetzt sich beim Erhitzen explosionsartig;
butyl nitrate
928-45-0

butyl nitrate

p-toluidine
106-49-0

p-toluidine

A

N-butyl-4-methylaniline
10387-24-3

N-butyl-4-methylaniline

B

para-methyl anilinium nitrate
32954-54-4

para-methyl anilinium nitrate

Conditions
ConditionsYield
at 100℃;
butyl nitrate
928-45-0

butyl nitrate

diphenylamine
122-39-4

diphenylamine

N-nitrosodiphenylamine
382165-80-2

N-nitrosodiphenylamine

Conditions
ConditionsYield
at 100℃;
butyl nitrate
928-45-0

butyl nitrate

aniline
62-53-3

aniline

A

N-(n-butyl)aniline
1126-78-9

N-(n-butyl)aniline

B

anilinium nitrate
542-15-4

anilinium nitrate

Conditions
ConditionsYield
at 100℃;
butyl nitrate
928-45-0

butyl nitrate

toluene
108-88-3

toluene

A

1-methyl-4-nitrobenzene
99-99-0

1-methyl-4-nitrobenzene

B

1-methyl-2-nitrobenzene
88-72-2

1-methyl-2-nitrobenzene

Conditions
ConditionsYield
With sulfuric acid at 40 - 60℃;
butyl nitrate
928-45-0

butyl nitrate

o-toluidine
95-53-4

o-toluidine

o-toluidine nitrate
32954-52-2

o-toluidine nitrate

Conditions
ConditionsYield
at 100℃;
butyl nitrate
928-45-0

butyl nitrate

trifluoroacetic acid
76-05-1

trifluoroacetic acid

n-butyl trifluoroacetate
367-64-6

n-butyl trifluoroacetate

cycloactanone
502-49-8

cycloactanone

butyl nitrate
928-45-0

butyl nitrate

A

2-nitrocyclooctanone
13154-28-4

2-nitrocyclooctanone

B

butyl 8-nitrooctanoate
82781-91-7

butyl 8-nitrooctanoate

butyl nitrate
928-45-0

butyl nitrate

butan-1-ol
71-36-3

butan-1-ol

Conditions
ConditionsYield
With dihexylamine at 60℃; Rate constant;
butyl nitrate
928-45-0

butyl nitrate

sulfuric acid
7664-93-9

sulfuric acid

toluene
108-88-3

toluene

1-methyl-4-nitrobenzene
99-99-0

1-methyl-4-nitrobenzene

928-45-0Relevant articles and documents

Practical catalytic nitration directly with commercial nitric acid for the preparation of aliphatic nitroesters

An, Jichao,He, Pan,Li, Wenhao,Liu, Peipei,Si, Mengyuan,Yang, Bo,Yang, Guanyu

supporting information, p. 6612 - 6616 (2020/09/21)

To pursue a sustainable and efficient approach for aliphatic nitroester preparation from alcohol, europium-triflate-catalyzed nitration, which directly uses commercial nitric acid, has been successfully developed. Gram scalability with operational ease showed its practicability.

Synthesis of nitric acid esters from alcohols in a dinitrogen pentoxide/carbon dioxide liquid system

Kuchurov, Ilya V.,Fomenkov, Igor V.,Zlotin, Sergei G.,Tartakovsky, Vladimir A.

experimental part, p. 67 - 69 (2012/07/02)

Organic nitric acid esters have been prepared in 89-98% yield by the nitration of the corresponding alcohols and polyols with N2O5 in liquid CO2.

Rate coefficients for the reactions of Cl atoms with a series of C3-C6 hydroxyalkyl nitrates at 296 ± 2 K

Treves, Keren,Shragina, Lea,Rudich, Yinon

, p. 5902 - 5907 (2007/10/03)

Rate coefficients for the gas-phase reactions of chlorine atoms with a series of C3-C6 hydroxyalkyl nitrates of atmospheric interest have been determined at 296 ± 2 K and atmospheric pressure. The experiments were conducted using the relative rate technique combined with solid-phase microextraction (SPME) sampling followed by gas chromatography (GC) analysis with an electron capture detector (ECD). The experiments were performed in a collapsible 100 L PVF-film (Tedlar) reaction chamber. It is shown that the presence of the hydroxy group enhances the reactivity of the hydroxyalkyl nitrates toward the Cl atom as compared to the corresponding alkyl nitrates and alkyl dinitrates. The Cl atom reactivity toward the hydroxyalkyl nitrates increases with the length of the alkyl chain and with increasing separation between the hydroxy and the nitrooxy groups. Tropospheric lifetimes are calculated using the determined rate coefficients and the atmospheric implications are briefly discussed.

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