Tetrahedron Letters p. 6390 - 6392 (2008)
Update date:2022-07-31
Topics:
Mycock, David K.
Sherlock, Alexandra E.
Glossop, Paul A.
Hayes, Christopher J.
We have shown that dimethyldioxirane (DMDO) can be used to effect an oxidative partial deprotection of benzylidene acetals derived from both 1,2- and 1,3-diols to afford hydroxy benzoate products. A wide range of functional groups are tolerated, and good to excellent yields are usually observed. The reactions are easy to perform and produce little waste other than acetone.
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Doi:10.1039/d0gc03572f
(2021)Doi:10.1016/j.tetlet.2008.09.110
(2008)Doi:10.1002/hlca.19570400232
(1957)Doi:10.1039/c3ra41262h
(2013)Doi:10.1021/jo01114a003
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(1987)
