Synthesis of 24-Methyl Sterols Stereospecifically labelled with 2H in the Isopropyl Methyl Groups. 13C NMR Spectral Assignment of C-26 and C-27 Resonances

DOI: 10.1039/c39900000263

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Journal of the Chemical Society. Chemical communications p. 263 - 264 (1990)

Update date:2022-07-29

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Authors:

Colombo, Diego

Ronchetti, Fiamma

Russo, Giovanni

Toma, Lucio

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Article abstract of DOI:10.1039/c39900000263

Through analysis of the 13C NMR spectra of (25S)-<27-2H>campesterol (1) and (25R)-<26-2H>dihydrobrassicasterol (2), the C-26 and C-27 resonances have been unambigously assigned; the biosynthetic applications are discussed.

Full text of DOI:10.1039/c39900000263

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