Synthesis of 24-Methyl Sterols Stereospecifically labelled with 2H in the Isopropyl Methyl Groups. 13C NMR Spectral Assignment of C-26 and C-27 Resonances

DOI: 10.1039/c39900000263

Source and publish data:

Journal of the Chemical Society. Chemical communications p. 263 - 264 (1990)

Update date:2022-07-29

Topics:

Authors:

Colombo, Diego

Ronchetti, Fiamma

Russo, Giovanni

Toma, Lucio

Read Full Text PDF DownLoad Join now for total 90,000,000 free articles

Article abstract of DOI:10.1039/c39900000263

Through analysis of the 13C NMR spectra of (25S)-<27-2H>campesterol (1) and (25R)-<26-2H>dihydrobrassicasterol (2), the C-26 and C-27 resonances have been unambigously assigned; the biosynthetic applications are discussed.

Full text of DOI:10.1039/c39900000263

View Article Online / Journal Homepage / Table of Contents for this issue

View Article Online

Products guided by the article

Product name:(+/-)-4-benzyloxy-2,3-dimethylbutan-1-ol

Cas No:127593-78-6

R&D Labs maybe for 127593-78-6

Winchem Industrial Co. Ltd.(expird)

Contact:86-574-83851061 86-574-87083208

Address:Room 905, No.3 Building,East Business Center, 456 Xingning Road, Ningbo City,China
Xuzhou Tianrun Chemical Co.,Ltd

website:http://www.tianrunchem.cn

Contact:86-516-83832636

Address:fuxing road
Angel Yeast Co., Ltd.

Contact:+86-717-6370352

Address:168 Chengdong Avenue, Yichang, Hubei 443003, P. R.China
Xinjiang Zhongtai Chemical Co., Ltd.

Contact:+86-991-8788172

Address:NO.78 XISHAN RD.URUMQI，CHINA
Li's chemicals

Contact:+86-15850770348

Address:51 OF XIANGFANGCUN ROAD, Nanjing 210002, China

Relevant to this article

Synthesis of Carbon-Branched Sugars Involving an Unprecedented 1,5- or 1,6-Alkyl Transposition Reaction

Doi:10.1002/ejoc.201900752
(2019)
SYNTHESIS OF 1-ALKYNYLBICYCLO<1.1.1>PENTANES

Doi:10.1016/S0040-4039(01)93718-9
(1989)
Spectral luminescent properties of 2-aryl-5-(2,4,6-trimethylphenyl)-1Н-1,3,4-oxadiazoles

Doi:10.1134/S1070428017050281
(2017)
N-heterocyclic carbene complexes of Rh(I) and electronic effects on catalysts for 1,2-addition of phenylboronic acid to aldehydes

Doi:10.1002/aoc.1746
(2011)
REACTION OF α-BROMOACETOPHENONE PHENYLSULFONYLHYDRAZONES. A NEW SYNTHETIC ROUTE TO 2-ARYLIMIDAZOISOQUINOLINES AND -QUINOLINES

Doi:10.3987/COM-91-5851
(1991)
Improved one-pot synthesis of C₃-symmetric clickphos and related ligands: Structures of unique triazole-zinc complexes

Doi:10.1002/ejoc.201001505
(2011)

Article Doi