European Journal of Organic Chemistry p. 5331 - 5335 (2011)
Update date:2022-08-03
Topics:
Ma, Yingjie
Zhang, Zibin
Ji, Xiaofan
Han, Chengyou
He, Jiuming
Abliz, Zeper
Chen, Weixiang
Huang, Feihe
The facile and efficient preparation of pillar[n]arenes (n = 5 or 6) was achieved by cyclooligomerization of 2,5-dialkoxybenzyl alcohols or 2,5-dialkoxybenzyl bromides with an appropriate Lewis acid catalyst at room temperature. The mechanism for this cyclooligomerization is presumed to be a Friedel-Crafts alkylation.
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