Russian Chemical Bulletin p. 927 - 930 (1995)
Update date:2022-08-03
Topics:
Semenov, V. V.
Ladilina, E. Yu.
Chesnokova, T. A.
Elistratova, N. K.
Kurskii, Yu. A.
Makarenko, N. P.
Reactions of Cl2MeSiSiMeCl2 with RMgCl make it possible to obtain and isolate pure disilanes containing a smaller number of functional groups, namely, RMeClSiSiMeCl2 (R = Ph), RMeClSiSiMeRCl (R = Pri, Ph), and R2MeSiSiMeRCl (R = Bui).The reaction of Cl2MeSiSiMeCl2 with BunMgCl is the least selective.The chlorides obtained were reduced with LiAlH4 into the corresponding hydrides.
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