Journal of Organic Chemistry p. 7920 - 7926 (1995)
Update date:2022-07-30
Topics:
Madsen, Robert
Roberts, Carmichael
Fraser-Reid, Bert
Primary and secondary amines are readily protected as N-pent-4-enoyl derivatives, the resulting N-pent-4-enamides being usually highly crystalline.Deprotection is rapidly and efficiently effected under mild conditions by treatment with 3 equiv of iodine in aqueous THF solution.Although an oxidizing medium, these deprotection conditions do not affect oxidizable functionalities including p-methoxybenzyl ethers and alkyl sulfides.
View MoreAnhui Qingyun Pharmaceutical and Chemical Co.,Ltd
Contact:+86-551-63633067
Address:Shuangfeng Road Hefei Anhui
website:http://www.orchid-chem.com
Contact:+86-571-85395792
Address:607, North Zhongshan Road, Hangzhou 310000 China
Contact:86-531-67875205
Address:No.9-2,South of Shanda Road, Jinan ,China
Jinan Kaypharm Chemical Co.,Ltd
Contact:86-0531-86986780
Address:Room101,No189-2,Huayuan Road,Jinan City,Shandong Province
Huaihua Baohua Biotechnology Co.,Ltd
website:http://www.baochengchem.com
Contact:86-519-82698291
Address:HouYang chemical development zone,Jintan,Jiangsu,China (213200)
Doi:10.1016/0040-4039(95)01826-4
(1995)Doi:10.1002/jhet.5570320502
(1995)Doi:10.1021/ja00154a049
(1995)Doi:10.1016/0040-4020(95)00881-8
(1995)Doi:10.1021/jo980321h
(1998)Doi:10.1016/j.tet.2017.11.011
(2018)