Chemical and Pharmaceutical Bulletin p. 2082 - 2087 (1995)
Update date:2022-08-04
Topics:
Itoh
Sekizaki
Toyota
Tanizawa
N(α)-(tert-Butyloxycarbonyl)peptide p-guanidinophenyl esters were synthesized by amidination of N(α)-(tert-butyloxycarbonyl)peptide p- aminophenyl esters with 1-[N,N'-bis(benzyloxycarbonyl)amidino]pyrazole, followed by deprotection by catalytic hydrogenation, in good total yields. These synthetic esters were characterized as specific substrates for trypsin, and kinetic parameters for the trypsin-catalyzed hydrolysis are presented.
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Doi:10.1021/ja953437t
(1996)Doi:10.1016/S0040-4039(00)97245-9
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