Canadian Journal of Chemistry p. 1922 - 1924 (1996)
Update date:2022-08-03
Topics:
Gasafi-Martin
Oberendfellner
von Werner
Reduction of the dihalogeno complexes RuCl2(PPh3)4 and NiBr2L2 (L = tertiary phosphine) with sodium hydride in MeCN in the presence of tetrafluoroethylene gives complexes containing five-membered MC4F8 rings. 1,2-Dihydrotetrafluoroethane is a by-product of these syntheses, especially when hydrogen is added. The M - C bonds of the metalla-perfluorocyclopentane complexes are remarkably stable against hydrogenolysis.
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(2021)
