Tetrahedron Letters p. 8703 - 8706 (1996)
Update date:2022-08-17
Topics:
Crimmins, Michael T.
Wang, Zhuo
McKerlie, Lynne A.
The total synthesis of the phytoalexin (±)-lubiminol 1 has been accomplished. The synthesis relies on a conjugate addition-cyclization reaction to prepare a photosubstrate for a stereoselective intramolecular photoaddition reaction. The photoadduct is and formed into the required spiro [5.4] decane through a radical fragmentation-rearrangement reaction.
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