Synthesis p. 635 - 637 (1995)
Update date:2022-08-10
Topics:
Caille
Didierlaurent
Lefrancois
Lelievre
Sury
Aszodi
Various ethyl 4-alkyl(aryl)thioimidazole-5-carboxylates have been synthesized by the reaction of ethyl valeramidocyanoacetate with a variety of alkyl(aryl) thiols in the presence of triethylamine and subsequent phosphorus pentachloride/4-dimethylaminopyridine (DMAP) mediated cyclization of the acyclic intermediates.
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