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7784-18-1

Basic Information
CAS No.: 7784-18-1
Name: Aluminum fluoride
Molecular Structure:
Molecular Structure of 7784-18-1 (Aluminum fluoride)
Formula: AlF3
Molecular Weight: 83.98
Synonyms: Aluminumfluoride (8CI);Aluminum trifluoride;Aluminum trifluoride (AlF3);Aluminum fluoride(AlF3);
EINECS: 232-051-1
Density: 3.1 g/mL at 25 °C(lit.)
Melting Point: 250 °C
Boiling Point: 19.5 °C at 760 mmHg
Flash Point: 1250 °C
Solubility: slightly soluble in Water
Appearance: white crystalline powder, odorless
Hazard Symbols: IrritantXi
Risk Codes: 22-36/37/38
Safety: 26-37/39
Transport Information:
PSA: 0.00000
LogP: -8.65050
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    Aluminum fluoride [Name] Aluminum fluoride [7784-18-1] [Molecular formula] AlF3 [Molecular weight] 83.89 Index Name AF-0 AF-1 AF-2 AF-3

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Chemistry

Molecular Structure of Aluminum fluoride (CAS NO.7784-18-1):

IUPAC Name: trifluoroalumane
CAS Number: 7784-18-1
Molecular Formula: AlF3
Molecular Weight:83.98
H bond acceptors: 0
H bond donors: 0
Freely Rotating Bonds: 0
Polar Surface Area: 0 Å2
Flash Point: 1250°C
Enthalpy of Vaporization: 25.54 kJ/mol
Boiling Point: 19.5 °C at 760 mmHg
Vapour Pressure: 922 mmHg at 25°C
Melting Point: 250 oC
Water Solubility: Slightly soluble
Sensitive: Hygroscopic
Melting point: 250°C
Sublimation: 1250 ºC
Merck: 14,339
EINECS: 232-051-1
InChI
InChI=1/Al.3FH/h;3*1H/q+3;;;/p-3
Smiles
[Al](F)(F)F
Product Categories: Inorganics; Inorganic Fluorides; Aluminum Salts; AluminumMetal and Ceramic Science; Crystal Grade Inorganics; Metal and Ceramic Science; Salts

Production

 The production of Aluminum fluoride (CAS NO.7784-18-1):

  Fluoride acid method will come from 18% in phosphate fluoride acid solution heated to about 78 ℃ , then add the reactor with aluminum hydroxide at 100 ℃ for the reaction of aluminum fluoride solution, centrifugation to remove hydrated silicic acid, the filtrate into the crystal device at 90 ℃ under the insulation 3 ~ 5h, have aluminum fluoride trihydrate (AIF3.3H2O) crystals.

 After centrifugal separation, the aluminum fluoride trihydrate crystals (moisture 5%) has been dealing with two boiling furnace dehydrated, the first a boiling furnace temperature was controlled at about 205 ℃, first to remove most of the water.
As a result,aluminum fluoride trihydrate the total water content (including crystal water) from 45% to 6% or so, and then in the second fluidized bed furnace in the off the rest of the water, the furnace temperature was controlled at 590 ~ 600 ℃. Dehydrated materials are cooled, the system may anhydrous aluminum fluoride.

 H2SiF6 +2 AI (OH) 3 → 2A1F3 + SiO2 +4 H2O

 AlF3 . 3H2O [△] → AlF3 +3 H2O

 France aluminum hydroxide aluminum hydroxide anhydrous hydrofluoric acid reacts with the aluminum fluoride trihydrate. Then crystallization, filtration, have aluminum fluoride trihydrate.At last by drying (burning) dehydration, obtained anhydrous aluminum fluoride.

 AI (OH) 3 +3 HF → AIF3.  3 H2O

 AlF3 . 3H2O [△] → A1F3 +3 H2O

Toxicity Data With Reference

Organism Test Type Route Reported Dose (Normalized Dose) Effect Source
frog LDLo subcutaneous 1680mg/kg (1680mg/kg)   Comptes Rendus des Seances de la Societe de Biologie et de Ses Filiales. Vol. 124, Pg. 133, 1937.
mammal (species unspecified) LD50 intraperitoneal 1450mg/kg (1450mg/kg)   Meditsina Truda i Promyshlennaya Ekologiya. Industrial Medicine and Ecology. Vol. (7), Pg. 32, 1994.
mouse LD50 oral 103mg/kg (103mg/kg)   Gigiena i Sanitariya. For English translation, see HYSAAV. Vol. 30(4), Pg. 16, 1965.

Consensus Reports

Reported in EPA TSCA Inventory.

Safety Profile

A poison by ingestion. Moderately toxic by subcutaneous route. A severe eye irritant. Violently impact-sensitive when in contact with Na and K. When heated to decomposition it emits toxic fumes of F. See also FLUORIDES and ALUMINUM COMPOUNDS.
Hazard Codes: HarmfulXn,ToxicT,IrritantXi
Risk Statements: 22-36/37/38
R22:Harmful if swallowed. 
R36/37/38:Irritating to eyes, respiratory system and skin.
Safety Statements: 26-37/39
S26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. 
S37/39:Wear suitable gloves and eye/face protection.
RIDADR: 3260
WGK Germany: 1
RTECS: BD0725000
Hazard Note: Highly Toxic/Irritant
HazardClass: 8
PackingGroup: III

Standards and Recommendations

OSHA PEL: TWA 2.5 mg(F)/m3
ACGIH TLV: TWA 2.5 mg(F)/m3; BEI: 3 mg/g creatinine of fluorides in urine prior to shift; 10 mg/g creatinine of fluorides in urine at end of shift; TWA 2 mg(Al)/m3
NIOSH REL: (Fluorides, Inorganic) TWA 2.5 mg(F)/m3

Specification

  Aluminum fluoride , with CAS number of 7784-18-1, can be called Fluorid hlinity ; Aluminumfluoride (8CI) . It is a white powder, Aluminum fluoride (CAS NO.7784-18-1) can be flux for non-ferrous metals and can be used for the system to take other aluminum fluoride.