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N,N-Dimethyldecylamine Manufacturer/High quality/Best price/In stock
Cas No: 1120-24-7
USD $ 3.0-3.0 / Kilogram 1 Kilogram 1-100 Metric Ton/Month Dayang Chem (Hangzhou) Co.,Ltd. Contact Supplier
N,N-Dimethyldecylamine
Cas No: 1120-24-7
No Data No Data No Data Chemwill Asia Co., Ltd. Contact Supplier
Factory Supply Decyldimethylamine
Cas No: 1120-24-7
No Data 1 1 Ality Chemical Corporation Contact Supplier
acetic acid [2-acetamido-6-acetyloxy-4-(carbamoyloxymethyl)-7-methyl-5,8-dioxo-2,3-dihydro-1H-pyrrolo[1,2-a]indol-3-yl] ester
Cas No: 1120-24-7
No Data 10 Milligram Amadis Chemical Co., Ltd. Contact Supplier
N,N-Dimethyldecylamine
Cas No: 1120-24-7
USD $ 8.0-8.0 / Gram 1 Gram 100 Metric Ton/Year Jinan Finer Chemical Co., Ltd Contact Supplier
Manufacturer supply CAS 1120-24-7 with best quality
Cas No: 1120-24-7
USD $ 139.0-210.0 / Kilogram 1 Kilogram 1000 Kilogram/Day Zhuozhou Wenxi import and Export Co., Ltd Contact Supplier
1-Decanamine,N,N-dimethyl- 1120-24-7
Cas No: 1120-24-7
No Data 1 Kilogram 10000 Metric Ton/Month Shanghai Upbio Tech Co.,Ltd Contact Supplier
1-Decanamine,N,N-dimethyl-
Cas No: 1120-24-7
No Data No Data 10000 Metric Ton/Month Henan Wentao Chemical Product Co., Ltd. Contact Supplier
N,N-Dimethyldecylamine
Cas No: 1120-24-7
USD $ 100.0-100.0 / Kilogram 1 Kilogram 1000 Kilogram/Month Baoji Guokang Healthchem co.,ltd Contact Supplier
1-Decanamine,N,N-dimethyl-
Cas No: 1120-24-7
No Data 1 Kilogram 1 Metric Ton/Day Shandong Hanjiang Chemical Co., Ltd. Contact Supplier

1120-24-7 Usage

Chemical Properties

liquid
InChI:InChI=1/C12H27N/c1-4-5-6-7-8-9-10-11-12-13(2)3/h4-12H2,1-3H3

1120-24-7SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 10, 2017

Revision Date: Aug 10, 2017

1.Identification

1.1 GHS Product identifier

Product name N,N-Dimethyldecan-1-amine

1.2 Other means of identification

Product number -
Other names N,N-DiMethyldecylaMine

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only. Intermediates,Surface active agents
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:1120-24-7 SDS

1120-24-7Synthetic route

N,N-dimethyldecanamide
14433-76-2

N,N-dimethyldecanamide

N,N-dimethyldecylamine
1120-24-7

N,N-dimethyldecylamine

Conditions
ConditionsYield
With tris(pentafluorophenyl)borate; [Ru(1,1,1-tris(di(3,5-dimethoxyphenyl)phosphino-methyl)ethane)(trimethylenemethane)]; hydrogen In tetrahydrofuran at 160℃; under 75007.5 Torr; for 16h;97%
With 9-borabicyclo[3.3.1]nonane In tetrahydrofuran at 25℃; for 1h; Inert atmosphere;88%
With n-pentyl methyl ketone; Dimethylphenylsilane; triethylamine; (μ3;η2;η3;η5-acenaphthylene)Ru3(CO)7 In various solvent(s) at 20℃; for 2h;79%
1-dodecene
112-41-4

1-dodecene

hydrogen cyanide
74-90-8

hydrogen cyanide

N,N-dimethyldecylamine
1120-24-7

N,N-dimethyldecylamine

Conditions
ConditionsYield
With sulfuric acid In methanol at 5 - 35℃; for 2h; Solvent; Temperature; Large scale;95.61%
1-bromo dodecane
112-29-8

1-bromo dodecane

dimethyl amine
124-40-3

dimethyl amine

N,N-dimethyldecylamine
1120-24-7

N,N-dimethyldecylamine

Conditions
ConditionsYield
With sodium hydroxide In water; toluene for 72h; Autoclave;95%
1-bromo dodecane
112-29-8

1-bromo dodecane

N,N-dimethylammonium chloride
506-59-2

N,N-dimethylammonium chloride

N,N-dimethyldecylamine
1120-24-7

N,N-dimethyldecylamine

Conditions
ConditionsYield
With sodium hydroxide In ethanol; water at 100℃; for 24h;91%
caprinaldehyde
112-31-2

caprinaldehyde

N,N-dimethyl-formamide
68-12-2, 33513-42-7

N,N-dimethyl-formamide

N,N-dimethyldecylamine
1120-24-7

N,N-dimethyldecylamine

Conditions
ConditionsYield
With formic acid at 190℃; for 6h;87%
formaldehyd
50-00-0

formaldehyd

1-aminodecane
2016-57-1

1-aminodecane

N,N-dimethyldecylamine
1120-24-7

N,N-dimethyldecylamine

Conditions
ConditionsYield
With formic acid In methanol; water Reflux;75%
non-1-ene
124-11-8

non-1-ene

dimethyl amine
124-40-3

dimethyl amine

N,N-dimethyldecylamine
1120-24-7

N,N-dimethyldecylamine

Conditions
ConditionsYield
With (acetylacetonato)dicarbonylrhodium (l); dodecacarbonyl-triangulo-triruthenium; carbon monoxide; hydrogen; triphenylphosphine In N,N-dimethyl-formamide at 150℃; under 30003 Torr; for 1h; Autoclave;74%
1-Decanol
112-30-1

1-Decanol

dimethyl amine
124-40-3

dimethyl amine

N,N-dimethyldecylamine
1120-24-7

N,N-dimethyldecylamine

Conditions
ConditionsYield
With C19H32Cl2IrN2; potassium carbonate In water at 130℃; for 40h; Sealed tube; Green chemistry;70%
non-1-ene
124-11-8

non-1-ene

dimethyl amine
124-40-3

dimethyl amine

A

nonane
111-84-2

nonane

B

N,N-dimethyldecylamine
1120-24-7

N,N-dimethyldecylamine

Conditions
ConditionsYield
With (acetylacetonato)dicarbonylrhodium (l); dodecacarbonyl-triangulo-triruthenium; carbon monoxide; hydrogen; triphenylphosphine In N,N-dimethyl-formamide at 150℃; under 9000.9 Torr; for 1h; Autoclave;A 8%
B 69%
non-1-ene
124-11-8

non-1-ene

carbon monoxide
201230-82-2

carbon monoxide

N,N-dimethyl-formamide
68-12-2, 33513-42-7

N,N-dimethyl-formamide

A

caprinaldehyde
112-31-2

caprinaldehyde

B

N,N-dimethyldecylamine
1120-24-7

N,N-dimethyldecylamine

Conditions
ConditionsYield
With (acetylacetonato)dicarbonylrhodium (l); hydrogen; triphenylphosphine at 80℃; under 15001.5 Torr; for 3h; Autoclave;A 65%
B 7%
formaldehyd
50-00-0

formaldehyd

formic acid
64-18-6

formic acid

1-aminodecane
2016-57-1

1-aminodecane

N,N-dimethyldecylamine
1120-24-7

N,N-dimethyldecylamine

Conditions
ConditionsYield
In methanol; water Reflux;63%
non-1-ene
124-11-8

non-1-ene

carbon monoxide
201230-82-2

carbon monoxide

dimethyl amine
124-40-3

dimethyl amine

A

caprinaldehyde
112-31-2

caprinaldehyde

B

N,N-dimethyldecylamine
1120-24-7

N,N-dimethyldecylamine

C

decene-1-yl-dimethylamine
861539-91-5

decene-1-yl-dimethylamine

Conditions
ConditionsYield
With (acetylacetonato)dicarbonylrhodium (l); hydrogen; triphenylphosphine In N,N-dimethyl-formamide at 130℃; under 15001.5 Torr; for 3h; Autoclave;A 9%
B 45%
C 16%
With (acetylacetonato)dicarbonylrhodium (l); hydrogen; triphenylphosphine In N,N-dimethyl-formamide at 130℃; under 15001.5 Torr; for 1h; Autoclave;A 13%
B 44%
C 10%
With (acetylacetonato)dicarbonylrhodium (l); dodecacarbonyl-triangulo-triruthenium; hydrogen; triphenylphosphine In N,N-dimethyl-formamide at 80℃; under 9000.9 Torr; for 3h; Autoclave;A 29%
B 7%
C 38%
With (acetylacetonato)dicarbonylrhodium (l); dodecacarbonyl-triangulo-triruthenium; hydrogen; triphenylphosphine In N,N-dimethyl-formamide at 80℃; under 9000.9 Torr; for 6h; Autoclave;A 21%
B 21%
C 29%
non-1-ene
124-11-8

non-1-ene

dimethyl amine
124-40-3

dimethyl amine

A

nonane
111-84-2

nonane

B

N,N-dimethyldecylamine
1120-24-7

N,N-dimethyldecylamine

C

decene-1-yl-dimethylamine
861539-91-5

decene-1-yl-dimethylamine

Conditions
ConditionsYield
With (acetylacetonato)dicarbonylrhodium (l); carbon monoxide; hydrogen; triphenylphosphine In N,N-dimethyl-formamide at 150℃; under 9000.9 Torr; for 2h; Autoclave;A 11%
B 42%
C 6%
non-1-ene
124-11-8

non-1-ene

carbon monoxide
201230-82-2

carbon monoxide

N,N-dimethyl-formamide
68-12-2, 33513-42-7

N,N-dimethyl-formamide

A

caprinaldehyde
112-31-2

caprinaldehyde

B

N,N-dimethyldecylamine
1120-24-7

N,N-dimethyldecylamine

C

decene-1-yl-dimethylamine
861539-91-5

decene-1-yl-dimethylamine

Conditions
ConditionsYield
With (acetylacetonato)dicarbonylrhodium (l); hydrogen; triphenylphosphine at 130℃; under 15001.5 Torr; for 3h; Autoclave;A 39%
B 16%
C 10%
With (acetylacetonato)dicarbonylrhodium (l); hydrogen; triphenylphosphine at 150℃; under 30003 Torr; for 6h; Autoclave;A 6%
B 29%
C 6%
non-1-ene
124-11-8

non-1-ene

carbon monoxide
201230-82-2

carbon monoxide

dimethyl amine
124-40-3

dimethyl amine

A

caprinaldehyde
112-31-2

caprinaldehyde

B

nonane
111-84-2

nonane

C

N,N-dimethyldecylamine
1120-24-7

N,N-dimethyldecylamine

D

decene-1-yl-dimethylamine
861539-91-5

decene-1-yl-dimethylamine

Conditions
ConditionsYield
With (acetylacetonato)dicarbonylrhodium (l); hydrogen; triphenylphosphine In N,N-dimethyl-formamide at 150℃; under 9000.9 Torr; for 0.5h; Autoclave;A 15%
B 11%
C 16%
D 17%
N,N-dimethyl-10-amino-1-decene
27397-10-0

N,N-dimethyl-10-amino-1-decene

N,N-dimethyldecylamine
1120-24-7

N,N-dimethyldecylamine

Conditions
ConditionsYield
With ethyl acetate; platinum Hydrogenation;
decyl-trimethyl-ammonium; hydroxide
62417-63-4

decyl-trimethyl-ammonium; hydroxide

A

1-Decanol
112-30-1

1-Decanol

B

1-Decene
872-05-9

1-Decene

C

N,N-dimethyldecylamine
1120-24-7

N,N-dimethyldecylamine

N,N-dimethyldecanamide
14433-76-2

N,N-dimethyldecanamide

A

1-Decanol
112-30-1

1-Decanol

B

N,N-dimethyldecylamine
1120-24-7

N,N-dimethyldecylamine

Conditions
ConditionsYield
With sodium dimethylaminoborohydride In tetrahydrofuran at 66℃; for 55h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
With ethanol; sodium In hexane at 0℃; for 0.333333h; Inert atmosphere; Overall yield = 73 %; Overall yield = 57.8 mg; chemoselective reaction;
anhydro
29183-39-9

anhydro

A

6,7-dibenzoyl-1,3,5-triphenyl-cyclopenta[c]pyran
78501-30-1

6,7-dibenzoyl-1,3,5-triphenyl-cyclopenta[c]pyran

B

N,N-dimethyldecylamine
1120-24-7

N,N-dimethyldecylamine

C

1,2,3-tribenzoylcyclopropane
5633-67-0, 877469-07-3

1,2,3-tribenzoylcyclopropane

D

1,4-diphenylbut-2-ene-1,4-dione
959-28-4

1,4-diphenylbut-2-ene-1,4-dione

Conditions
ConditionsYield
at 150℃; for 3h;A 400 mg
B 2.85 g
C n/a
D 200 mg
decyl chloride
1002-69-3

decyl chloride

dimethyl amine
124-40-3

dimethyl amine

N,N-dimethyldecylamine
1120-24-7

N,N-dimethyldecylamine

Conditions
ConditionsYield
In water at 140 - 150℃;
trimethyl-n-decyl-ammonium hydroxide

trimethyl-n-decyl-ammonium hydroxide

N,N-dimethyldecylamine
1120-24-7

N,N-dimethyldecylamine

Iododecane
2050-77-3

Iododecane

dimethyl amine
124-40-3

dimethyl amine

N,N-dimethyldecylamine
1120-24-7

N,N-dimethyldecylamine

Conditions
ConditionsYield
With PS-triphenylphosphine; di-isopropyl azodicarboxylate In tetrahydrofuran
1-Decanol
112-30-1

1-Decanol

N,N-dimethyldecylamine
1120-24-7

N,N-dimethyldecylamine

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: zinc chloride, hydrogen chloride / 140 °C
2: H2O / 140 - 150 °C
View Scheme
n-decanoyl chloride
112-13-0

n-decanoyl chloride

N,N-dimethyldecylamine
1120-24-7

N,N-dimethyldecylamine

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: benzene / 1.) 0 deg C, 1 h, 2.) r.t., 1 h
2: LiAlH4 / tetrahydrofuran / 5 h / Heating
View Scheme
1-Decanol
112-30-1

1-Decanol

methylamine
74-89-5

methylamine

A

N,N-dimethyldecylamine
1120-24-7

N,N-dimethyldecylamine

B

N-methyldidecylamine
7396-58-9

N-methyldidecylamine

C

tri(n-decyl)amine
1070-01-5

tri(n-decyl)amine

Conditions
ConditionsYield
filim type catalyst C at 185℃; for 4.5h; Product distribution / selectivity;A 0.7 %Chromat.
B 93.6 %Chromat.
C 1.2 %Chromat.
N,N-dimethyldecanamide
14433-76-2

N,N-dimethyldecanamide

A

1-Decanol
112-30-1

1-Decanol

B

N-decyl-N-methylamine
7516-82-7

N-decyl-N-methylamine

C

N,N-dimethyldecylamine
1120-24-7

N,N-dimethyldecylamine

D

N-methyldidecylamine
7396-58-9

N-methyldidecylamine

Conditions
ConditionsYield
With hydrogen; dimethyl amine; CuCr catalyst (Leuna 1970T) at 250℃; under 7500.75 Torr; Product distribution / selectivity;
With hydrogen; dimethyl amine; CuCr catalyst Leuna 1970T at 250℃; under 7500.75 Torr; Product distribution / selectivity; Gas phase;A 0.1 %Chromat.
B 2.7 %Chromat.
C 96.3 %Chromat.
D 0.7 %Chromat.
With hydrogen; CuCr catalyst (Leuna 1970T) at 250℃; under 7500.75 Torr; Product distribution / selectivity;
With hydrogen; CuCr catalyst Leuna 1970T at 250℃; under 7500.75 Torr; Product distribution / selectivity; Gas phase;A 2.0 %Chromat.
B 0.4 %Chromat.
C 92.5 %Chromat.
D 4.7 %Chromat.
N,N-dimethyldecanamide
14433-76-2

N,N-dimethyldecanamide

A

1-Decanol
112-30-1

1-Decanol

B

N,N-dimethyldecylamine
1120-24-7

N,N-dimethyldecylamine

C

N-methyldidecylamine
7396-58-9

N-methyldidecylamine

Conditions
ConditionsYield
With hydrogen; CuCr-type catalyst (Leuna 1970T) at 250℃; under 7500.75 Torr; Product distribution / selectivity; Gas phase;
N,N-dimethyldecanamide
14433-76-2

N,N-dimethyldecanamide

A

N-decyl-N-methylamine
7516-82-7

N-decyl-N-methylamine

B

N,N-dimethyldecylamine
1120-24-7

N,N-dimethyldecylamine

Conditions
ConditionsYield
With hydrogen; dimethyl amine; CuCr-type catalyst (Leuna 1970T) at 250℃; under 7500.75 Torr; Product distribution / selectivity; Gas phase;
non-1-ene
124-11-8

non-1-ene

Methyl formate
107-31-3

Methyl formate

dimethyl amine
124-40-3

dimethyl amine

A

N,N-dimethyldecylamine
1120-24-7

N,N-dimethyldecylamine

B

N,N-dimethyl-2-propylheptan-1-amine

N,N-dimethyl-2-propylheptan-1-amine

C

C12H27N
1542249-01-3

C12H27N

D

C12H27N
1542249-05-7

C12H27N

E

C12H27N
1542249-12-6

C12H27N

Conditions
ConditionsYield
With acetylacetonatodicarbonylrhodium(l); dodecacarbonyl-triangulo-triruthenium; water; triphenylphosphine In N,N-dimethyl-formamide at 170℃; for 6h; Autoclave; Green chemistry;
N,N-dimethyldecylamine
1120-24-7

N,N-dimethyldecylamine

2-oxo-3-(phenyl)propionic acid
156-06-9

2-oxo-3-(phenyl)propionic acid

DiMeClOA-PhPA

DiMeClOA-PhPA

Conditions
ConditionsYield
In acetone100%
furan-2-yl-oxo-acetic acid
1467-70-5

furan-2-yl-oxo-acetic acid

N,N-dimethyldecylamine
1120-24-7

N,N-dimethyldecylamine

FAA-DiMeC10A

FAA-DiMeC10A

Conditions
ConditionsYield
In acetone100%
1 ,6-dibromohexane
629-03-8

1 ,6-dibromohexane

N,N-dimethyldecylamine
1120-24-7

N,N-dimethyldecylamine

C30H66N2(2+)*2Br(1-)
18699-36-0

C30H66N2(2+)*2Br(1-)

Conditions
ConditionsYield
In acetonitrile at 82℃; for 48h; Menshutkin Reaction;99%
In acetonitrile at 60℃; for 24h;92%
N,N-dimethyldecylamine
1120-24-7

N,N-dimethyldecylamine

4-Vinylbenzyl chloride
1592-20-7

4-Vinylbenzyl chloride

decyldimethyl-(4-vinylbenzyl)ammonium chloride

decyldimethyl-(4-vinylbenzyl)ammonium chloride

Conditions
ConditionsYield
In acetonitrile at 40℃; for 239h;99%
N,N-dimethyldecylamine
1120-24-7

N,N-dimethyldecylamine

3-chloroprop-1-ene
107-05-1

3-chloroprop-1-ene

allyldecyldimethylammonium chloride

allyldecyldimethylammonium chloride

Conditions
ConditionsYield
In acetonitrile at 60℃; for 49h;99%
N,N-dimethyldecylamine
1120-24-7

N,N-dimethyldecylamine

N,N-dimethyldecylamine-N-oxide
2605-79-0

N,N-dimethyldecylamine-N-oxide

Conditions
ConditionsYield
With dihydrogen peroxide; benzonitrile; Mg-Al-O-t-Bu HT (Catalyst B) In methanol; water at 65℃; for 0.5h; Product distribution / selectivity;98%
With dihydrogen peroxide; layered double hydroxide WO4(2-) at 20℃; for 2.5h;97%
With dihydrogen peroxide In methanol; water75%
With 1-decyl-4-(trifluoromethyl)pyrimidinium triflate; dihydrogen peroxide In aq. phosphate buffer; chloroform at 25℃; for 24h; Green chemistry; chemoselective reaction;67%
N,N-dimethyldecylamine
1120-24-7

N,N-dimethyldecylamine

1,12-dibromododecane
3344-70-5

1,12-dibromododecane

C36H78N2(2+)*2Br(1-)
87723-19-1

C36H78N2(2+)*2Br(1-)

Conditions
ConditionsYield
In acetonitrile at 82℃; for 48h; Menshutkin Reaction;97%
In acetonitrile for 24h; Menshutkin Reaction; Heating;95%
In acetonitrile at 60℃; for 24h;91%
In methanol66%
(1R,2S,5R)-1-(chloromethoxy)-2-isopropyl-5-methylcyclohexane
26127-08-2

(1R,2S,5R)-1-(chloromethoxy)-2-isopropyl-5-methylcyclohexane

N,N-dimethyldecylamine
1120-24-7

N,N-dimethyldecylamine

Decyl-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyloxymethyl)-dimethyl-ammonium; chloride

Decyl-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyloxymethyl)-dimethyl-ammonium; chloride

Conditions
ConditionsYield
In hexane at 20℃; for 0.5h; Menschutkin reaction;97%
1,8-dibromooctane
4549-32-0

1,8-dibromooctane

N,N-dimethyldecylamine
1120-24-7

N,N-dimethyldecylamine

C32H70N2(2+)*2Br(1-)
87723-17-9

C32H70N2(2+)*2Br(1-)

Conditions
ConditionsYield
In acetonitrile at 82℃; for 48h; Menshutkin Reaction;97%
In acetonitrile at 60℃; for 24h;93%
In ethanol at 100℃; for 48h;
N,N-dimethyldecylamine
1120-24-7

N,N-dimethyldecylamine

(±)-chloromethyl menthyl ether

(±)-chloromethyl menthyl ether

decyl[(±)-menthoxymethyl]dimethylammonium chloride

decyl[(±)-menthoxymethyl]dimethylammonium chloride

Conditions
ConditionsYield
In hexane at 20℃; for 3h; Menshutkin Reaction;96.5%
N,N-dimethyldecylamine
1120-24-7

N,N-dimethyldecylamine

1,3-dibromo-propane
109-64-8

1,3-dibromo-propane

N,N-dimethyl(3-bromopropyl)decyl ammonium bromide

N,N-dimethyl(3-bromopropyl)decyl ammonium bromide

Conditions
ConditionsYield
With tetra-(n-butyl)ammonium iodide In ethanol for 8h; Reflux;95.8%
1,4-dibromo-butane
110-52-1

1,4-dibromo-butane

N,N-dimethyldecylamine
1120-24-7

N,N-dimethyldecylamine

C28H62N2(2+)*2Br(1-)
87723-15-7

C28H62N2(2+)*2Br(1-)

Conditions
ConditionsYield
In acetonitrile at 60℃; for 24h;95%
In methanol92%
1-bromo dodecane
112-29-8

1-bromo dodecane

N,N-dimethyldecylamine
1120-24-7

N,N-dimethyldecylamine

didecyldimethylammonium chloride
7173-51-5

didecyldimethylammonium chloride

Conditions
ConditionsYield
Stage #1: 1-bromo dodecane; N,N-dimethyldecylamine
Stage #2: With hydrogenchloride In water
95%
N,N-dimethyldecylamine
1120-24-7

N,N-dimethyldecylamine

3β-bromoacetate-ergosta-5,7,12-triene

3β-bromoacetate-ergosta-5,7,12-triene

N,N-dimethyl-(3β-acetate-ergosta-5,7,12-triene)-N-decylammonium bromide

N,N-dimethyl-(3β-acetate-ergosta-5,7,12-triene)-N-decylammonium bromide

Conditions
ConditionsYield
In acetonitrile for 2h; Reflux;95%
N,N-dimethyldecylamine
1120-24-7

N,N-dimethyldecylamine

1,2-bis(2-chloroethoxy)ethane
112-26-5

1,2-bis(2-chloroethoxy)ethane

C30H66N2O2(2+)*2Cl(1-)

C30H66N2O2(2+)*2Cl(1-)

Conditions
ConditionsYield
In acetonitrile for 24h; Menshutkin Reaction; Heating;94%
N,N-dimethyldecylamine
1120-24-7

N,N-dimethyldecylamine

iodomethylbenzene
620-05-3

iodomethylbenzene

n-decylbenzyldimethylammonium iodide

n-decylbenzyldimethylammonium iodide

Conditions
ConditionsYield
In methanol at 60℃; for 3h; Large scale;93.2%
N,N-dimethyldecylamine
1120-24-7

N,N-dimethyldecylamine

chloroacetonitrile
107-14-2

chloroacetonitrile

ethyl ester of p-toluenesulfonic acid
80-40-0

ethyl ester of p-toluenesulfonic acid

(cyanomethyl)dimethyldecylammonium tosylate

(cyanomethyl)dimethyldecylammonium tosylate

Conditions
ConditionsYield
Stage #1: N,N-dimethyldecylamine; chloroacetonitrile In acetic acid butyl ester at 60℃; for 6h;
Stage #2: ethyl ester of p-toluenesulfonic acid In acetic acid butyl ester at 80℃; for 1.5h;
93%
N,N-dimethyldecylamine
1120-24-7

N,N-dimethyldecylamine

bromoacetyl 5α-cholestan-3β-oate

bromoacetyl 5α-cholestan-3β-oate

N,N-dimethyl-(3β-acetate-5β-cholestan)-N-decylammonium bromide

N,N-dimethyl-(3β-acetate-5β-cholestan)-N-decylammonium bromide

Conditions
ConditionsYield
In acetonitrile for 2h; Reflux;93%
N,N-dimethyldecylamine
1120-24-7

N,N-dimethyldecylamine

Na(1+)*Ga(N3)4(1-)=Na[Ga(N3)4]
203391-71-3

Na(1+)*Ga(N3)4(1-)=Na[Ga(N3)4]

((CH3)2N(C10H21))Ga(N3)3
255884-17-4

((CH3)2N(C10H21))Ga(N3)3

Conditions
ConditionsYield
In toluene Ar atmosphere, addn. of amine to solution of gallium compound at -78°C, warming to room temp. with stirring (12 h); filtration, removement of solvent (vacuum distillation, 25°C), washing (n-pentane); elem. anal.;92%
N,N-dimethyldecylamine
1120-24-7

N,N-dimethyldecylamine

3-oxa-1,5-dichloropentane
111-44-4

3-oxa-1,5-dichloropentane

diethyl ether-α,ω-didecyldimethylammonium chloride

diethyl ether-α,ω-didecyldimethylammonium chloride

Conditions
ConditionsYield
In acetonitrile for 24h; Menshutkin Reaction; Heating;92%
With sodium carbonate In isopropyl alcohol at 55 - 83℃; for 8h;
1-(bromomethyl)-4-(prop-1-en-2-yl)cyclohexene
939791-33-0

1-(bromomethyl)-4-(prop-1-en-2-yl)cyclohexene

N,N-dimethyldecylamine
1120-24-7

N,N-dimethyldecylamine

(4R)-N,N-dimethyl-N-{[4-(prop-1-en-2-yl)cyclohex-1-en-1-yl]methyl}decylammonium bromide

(4R)-N,N-dimethyl-N-{[4-(prop-1-en-2-yl)cyclohex-1-en-1-yl]methyl}decylammonium bromide

Conditions
ConditionsYield
In benzene at 20℃; Reflux;92%
methyl 3α-bromoacetoxy-5β-cholan-24-oate
856408-82-7

methyl 3α-bromoacetoxy-5β-cholan-24-oate

N,N-dimethyldecylamine
1120-24-7

N,N-dimethyldecylamine

N,N-dimethyl-(methyl 3α-acetoxy-5β-cholan-24-oate)-N-decylammonium bromide

N,N-dimethyl-(methyl 3α-acetoxy-5β-cholan-24-oate)-N-decylammonium bromide

Conditions
ConditionsYield
In acetonitrile at 81℃; for 3h;91%
N,N-dimethyldecylamine
1120-24-7

N,N-dimethyldecylamine

3-Bromomethyl-1,8-dihydroxy-6-methoxy-9,10-anthraquinone
121210-64-8

3-Bromomethyl-1,8-dihydroxy-6-methoxy-9,10-anthraquinone

N-((4,5-dihydroxy-7-methoxy-9,10-anthraquinone-2-yl)methyl)-N,N-dimethyldecan-1-aminium bromide
1412421-78-3

N-((4,5-dihydroxy-7-methoxy-9,10-anthraquinone-2-yl)methyl)-N,N-dimethyldecan-1-aminium bromide

Conditions
ConditionsYield
In chloroform for 24h; Reflux;90.1%
1,4-bis(bromomethyl)benzene
623-24-5

1,4-bis(bromomethyl)benzene

N,N-dimethyldecylamine
1120-24-7

N,N-dimethyldecylamine

1,4-bis[N-(1-decyl)-N,N-dimethylammoniummethyl]benzene dibromide
87723-20-4

1,4-bis[N-(1-decyl)-N,N-dimethylammoniummethyl]benzene dibromide

Conditions
ConditionsYield
In propan-1-ol for 8h;90%
In methanol89%
N,N-dimethyldecylamine
1120-24-7

N,N-dimethyldecylamine

carbonic acid dimethyl ester
616-38-6

carbonic acid dimethyl ester

trimethylmono-n-decylammonium monomethylcarbonate

trimethylmono-n-decylammonium monomethylcarbonate

Conditions
ConditionsYield
In methanol at 120℃; for 48h; Autoclave;90%
In methanol; ethylene glycol
N,N-dimethyldecylamine
1120-24-7

N,N-dimethyldecylamine

1,10-dibromodecane
4101-68-2

1,10-dibromodecane

N,N'-bis-decyl-N,N,N',N'-tetramethyl-N,N'-decanediyl-di-ammonium; dibromide
87723-18-0

N,N'-bis-decyl-N,N,N',N'-tetramethyl-N,N'-decanediyl-di-ammonium; dibromide

Conditions
ConditionsYield
In acetonitrile at 60℃; for 24h;90%
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