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1,4-Dioxan-2-one Manufacturer/High quality/Best price/In stock
Cas No: 3041-16-5
USD $ 3.0-3.0 / Kilogram 1 Kilogram 1-100 Metric Ton/Month Dayang Chem (Hangzhou) Co.,Ltd. Contact Supplier
High quality 1,4-Dioxan-2-One supplier in China
Cas No: 3041-16-5
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Factory Supply 1,4-dioxan-2-one
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No Data 1 1 Ality Chemical Corporation Contact Supplier
1,4-Dioxan-2-one
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No Data 10 Milligram Amadis Chemical Co., Ltd. Contact Supplier
2-Oxo-1,4-dioxane
Cas No: 3041-16-5
No Data No Data No Data Chemwill Asia Co., Ltd. Contact Supplier
1,4-Dioxan-2-one 3041-16-5
Cas No: 3041-16-5
No Data 1 Kilogram 10 Metric Ton/Month Henan Tianfu Chemical Co., Ltd. Contact Supplier
Pharmaceutical 1,4-Dioxan-2-one cas no 3041-16-5
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No Data 100 Gram 20000 Kilogram/Day Hubei XinRunde Chemical Co., Ltd Contact Supplier
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USD $ 139.0-210.0 / Kilogram 1 Kilogram 1000 Kilogram/Day Zhuozhou Wenxi import and Export Co., Ltd Contact Supplier
BLOOM TECH Advanced API/Technology support p-Dioxanone CAS 3041-16-5
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No Data 1 Gram 3 Metric Ton/Month Shaanxi BLOOM TECH Co.,Ltd Contact Supplier
1,4-Dioxan-2-one 3041-16-5
Cas No: 3041-16-5
No Data 1 Kilogram 10000 Metric Ton/Month Shanghai Upbio Tech Co.,Ltd Contact Supplier

3041-16-5 Usage

InChI:InChI=1/C4H6O3/c5-4-3-6-1-2-7-4/h1-3H2

3041-16-5SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 11, 2017

Revision Date: Aug 11, 2017

1.Identification

1.1 GHS Product identifier

Product name 1,4-Dioxan-2-one

1.2 Other means of identification

Product number -
Other names 1,4-dioxanone

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only.
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:3041-16-5 SDS

3041-16-5Synthetic route

diethylene glycol
111-46-6

diethylene glycol

p-dioxanone
3041-16-5

p-dioxanone

Conditions
ConditionsYield
With pyridine; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; trichloroisocyanuric acid In acetonitrile Inert atmosphere;100%
In water at 180℃; under 3750.38 Torr; for 4h; Catalytic behavior;100%
With 1-methyl-1H-imidazole; [2,2]bipyridinyl; tetrakis(acetonitrile)copper(I) trifluoromethanesulfonate; 9-azabicyclo<3.3.1>nonane-N-oxyl In acetonitrile at 22℃; for 2h; Reagent/catalyst;98%
diethylene glycol
111-46-6

diethylene glycol

A

1,4-dioxane-2-ol
22347-47-3

1,4-dioxane-2-ol

B

p-dioxanone
3041-16-5

p-dioxanone

Conditions
ConditionsYield
With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; nitromethane; oxygen; 1,10-ethyleneisoalloxazinium chloride at 40℃; for 24h;A 6 %Spectr.
B 90%
With 1-methyl-1H-imidazole; [2,2]bipyridinyl; tetrakis(acetonitrile)copper(I) trifluoromethanesulfonate; 9-azabicyclo<3.3.1>nonane-N-oxyl In acetonitrile at 22℃; for 2h; Reagent/catalyst;A 38%
B 87%
With 1-methyl-1H-imidazole; [2,2]bipyridinyl; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; tetrakis(acetonitrile)copper(I) trifluoromethanesulfonate In acetonitrile at 22℃; for 2h; Reagent/catalyst;A 45%
B 45%
With 1-methyl-1H-imidazole; [2,2]bipyridinyl; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; tetrakis(acetonitrile)copper(I) trifluoromethanesulfonate In acetonitrile at 22℃; for 12h; Temperature; Reagent/catalyst;A 44%
B 34%
With 0.5C32H30N4O4Pd2(4+)*2CF3O3S(1-); oxygen In acetonitrile at 60℃; under 760.051 Torr; for 26h; Reagent/catalyst; Temperature;
2-(2-methoxyethoxy)acetic acid
16024-56-9

2-(2-methoxyethoxy)acetic acid

p-dioxanone
3041-16-5

p-dioxanone

Conditions
ConditionsYield
With hydrogen bromide In water at 0℃; pH=3; Reflux;60%
With hydrogen bromide at 150℃;
1,4-dioxane
123-91-1

1,4-dioxane

p-dioxanone
3041-16-5

p-dioxanone

Conditions
ConditionsYield
With chromium(VI) oxide; Salpetersaeuretrimethylsilylester In acetonitrile for 24h; Ambient temperature;52%
With TS-1 (titanium silicate); dihydrogen peroxide5%
With hydrogenchloride; sodium hypochlorite
2-acetoxy-3-chloro-[1,4]dioxane
56127-61-8

2-acetoxy-3-chloro-[1,4]dioxane

A

p-dioxanone
3041-16-5

p-dioxanone

B

acetyl chloride
75-36-5

acetyl chloride

Conditions
ConditionsYield
at 190℃;
trans-2,3-dichloro-1,4-dioxane
95-59-0, 3883-42-9, 3883-43-0

trans-2,3-dichloro-1,4-dioxane

p-dioxanone
3041-16-5

p-dioxanone

Conditions
ConditionsYield
With formic acid at 200℃;
(2-chloroethoxy)-acetic acid
14869-41-1

(2-chloroethoxy)-acetic acid

p-dioxanone
3041-16-5

p-dioxanone

Conditions
ConditionsYield
With sodium hydroxide unter vermindertem Druck;
C11H11N2O4

C11H11N2O4

A

formaldehyd
50-00-0

formaldehyd

B

ethylene glycol monoformate
628-35-3

ethylene glycol monoformate

C

ethylene glycol diformate
629-15-2

ethylene glycol diformate

D

4-cyanonitrosobenzene
31125-07-2

4-cyanonitrosobenzene

E

1,4-dioxane-2-ol
22347-47-3

1,4-dioxane-2-ol

F

p-dioxanone
3041-16-5

p-dioxanone

Conditions
ConditionsYield
With dinitrogen monoxide In water Mechanism; Product distribution; Rate constant; Ambient temperature; Irradiation; other ethers;
diethylene glycol
111-46-6

diethylene glycol

A

2-methyl-1,3-dioxolane
497-26-7

2-methyl-1,3-dioxolane

B

1,4-dioxane
123-91-1

1,4-dioxane

C

1,4-dioxene
543-75-9

1,4-dioxene

D

p-dioxanone
3041-16-5

p-dioxanone

Conditions
ConditionsYield
With zeolite NaY; copper at 280℃; further catalysts and conditions; Yield given;
With zeolite NaY; copper at 280℃; Product distribution; effect of support on selectivity of dioxene formation; further catalysts and conditions;
<β-oxy-ethoxy>-acetic acid

<β-oxy-ethoxy>-acetic acid

p-dioxanone
3041-16-5

p-dioxanone

Conditions
ConditionsYield
Bei der Destillation;
chloroacetic acid ethyl ester
105-39-5

chloroacetic acid ethyl ester

monosodium-compound of ethylene glycol

monosodium-compound of ethylene glycol

p-dioxanone
3041-16-5

p-dioxanone

Conditions
ConditionsYield
With ethylene glycol Erhitzen des Reaktionsprodukts mit wss. Salzsaeure;
chloroacetic acid ethyl ester
105-39-5

chloroacetic acid ethyl ester

monosodium-compound of glycol

monosodium-compound of glycol

p-dioxanone
3041-16-5

p-dioxanone

Conditions
ConditionsYield
With benzene
trans-2,3-dichloro-1,4-dioxane
95-59-0, 3883-42-9, 3883-43-0

trans-2,3-dichloro-1,4-dioxane

water containing formic acid

water containing formic acid

p-dioxanone
3041-16-5

p-dioxanone

Conditions
ConditionsYield
at 200℃;
1,4-dioxane
123-91-1

1,4-dioxane

A

1,4-dioxane-2-ol
22347-47-3

1,4-dioxane-2-ol

B

p-dioxanone
3041-16-5

p-dioxanone

Conditions
ConditionsYield
With 3,3-dimethyldioxirane In acetone at 25℃; Kinetics;A 11 % Chromat.
B 44 % Chromat.
With oxygen at 80℃; for 24h; Catalytic behavior; Reagent/catalyst; Temperature; Time;A 90 %Chromat.
B 7 %Chromat.
2-(2-hydroxyethoxy)acetic acid
13382-47-3

2-(2-hydroxyethoxy)acetic acid

p-dioxanone
3041-16-5

p-dioxanone

Conditions
ConditionsYield
With hydrogen bromide; sodium hydrogencarbonate at 20℃; pH=3;104 g
ethanol
64-17-5

ethanol

p-dioxanone
3041-16-5

p-dioxanone

(2-chloro-ethoxy)-acetic acid ethyl ester
17229-14-0

(2-chloro-ethoxy)-acetic acid ethyl ester

Conditions
ConditionsYield
With thionyl chloride100%
p-dioxanone
3041-16-5

p-dioxanone

aniline
62-53-3

aniline

2-(2-hydroxyethoxy)-N-phenylacetamide

2-(2-hydroxyethoxy)-N-phenylacetamide

Conditions
ConditionsYield
With 1,3,4,6,7,8-hexahydro-2H-pyrimido[1,2-a]pyrimidine In neat (no solvent) at 40℃; for 24h;98%
p-dioxanone
3041-16-5

p-dioxanone

dimethyl amine
124-40-3

dimethyl amine

2-hydroxyethoxy-acetic acid-N,N-dimethylamide
939969-03-6

2-hydroxyethoxy-acetic acid-N,N-dimethylamide

Conditions
ConditionsYield
In 1,4-dioxane at 5 - 20℃; for 2.08333h; Product distribution / selectivity;95.9%
In acetonitrile at 5 - 20℃; for 2.08333h; Product distribution / selectivity;61.4%
In tetrahydrofuran at 5 - 20℃; for 2.08333h; Product distribution / selectivity;59.8%
In ethanol at 5 - 20℃; for 2.08333h; Product distribution / selectivity;50.4%
In toluene at 5 - 20℃; for 2.08333h; Product distribution / selectivity;40.6%
p-dioxanone
3041-16-5

p-dioxanone

ethyl acetate
141-78-6

ethyl acetate

ethyl 4-(2-hydroxyethoxy)-3-oxobutanoate
251324-96-6

ethyl 4-(2-hydroxyethoxy)-3-oxobutanoate

Conditions
ConditionsYield
With lithium diisopropyl amide In tetrahydrofuran at -78℃; for 3h;92%
sulfuric acid
7664-93-9

sulfuric acid

p-dioxanone
3041-16-5

p-dioxanone

(2-Bromo-ethoxy)-acetic acid
1135131-50-8

(2-Bromo-ethoxy)-acetic acid

Conditions
ConditionsYield
With hydrogen bromide In (2S)-N-methyl-1-phenylpropan-2-amine hydrate90%
2,3-Diaminopyridine
452-58-4

2,3-Diaminopyridine

p-dioxanone
3041-16-5

p-dioxanone

2-(2-hydroxyethoxymethyl)-pyrido[2,3-d]-1H-imidazole
307931-37-9

2-(2-hydroxyethoxymethyl)-pyrido[2,3-d]-1H-imidazole

Conditions
ConditionsYield
In 1,3,5-trimethyl-benzene for 10h; Heating / reflux;87%
N-<3-<3-(1-piperidinylmethyl)phenoxy>propyl>amine
73278-98-5

N-<3-<3-(1-piperidinylmethyl)phenoxy>propyl>amine

p-dioxanone
3041-16-5

p-dioxanone

2-(2-Hydroxy-ethoxy)-N-[3-(3-piperidin-1-ylmethyl-phenoxy)-propyl]-acetamide
132767-66-9

2-(2-Hydroxy-ethoxy)-N-[3-(3-piperidin-1-ylmethyl-phenoxy)-propyl]-acetamide

Conditions
ConditionsYield
84%
p-dioxanone
3041-16-5

p-dioxanone

1,2-diamino-benzene
95-54-5

1,2-diamino-benzene

2-(2-hydroxyethoxymethyl)-1H-benzimidazole
307931-39-1

2-(2-hydroxyethoxymethyl)-1H-benzimidazole

Conditions
ConditionsYield
In 1,3,5-trimethyl-benzene for 10h; Heating / reflux;77%
p-dioxanone
3041-16-5

p-dioxanone

2,2'-oxybis-acetic acid
110-99-6

2,2'-oxybis-acetic acid

Conditions
ConditionsYield
With dinitrogen tetraoxide In chloroform75%
p-dioxanone
3041-16-5

p-dioxanone

ethylene glycol
107-21-1

ethylene glycol

α,ω-dihydroxy oligo(p-dioxanone), prepared by ring-opening polymerization with ethylene glycol as initiator, Mn = 2300 g/mol (GPC), Mn = 2500 g/mol (NMR), Mn = 1600 g/mol (VPO), Mw/Mn = 1.50; monomer(s): p-dioxanone; ethylene glycol

α,ω-dihydroxy oligo(p-dioxanone), prepared by ring-opening polymerization with ethylene glycol as initiator, Mn = 2300 g/mol (GPC), Mn = 2500 g/mol (NMR), Mn = 1600 g/mol (VPO), Mw/Mn = 1.50; monomer(s): p-dioxanone; ethylene glycol

Conditions
ConditionsYield
at 110℃; for 48h;75%
p-dioxanone
3041-16-5

p-dioxanone

benzylamine
100-46-9

benzylamine

N-benzyl-2-(2-hydroxyethoxy)acetamide

N-benzyl-2-(2-hydroxyethoxy)acetamide

Conditions
ConditionsYield
With dibutyltin diacetate In tetrahydrofuran at 65℃; for 4h;73%
p-dioxanone
3041-16-5

p-dioxanone

ethylene glycol
107-21-1

ethylene glycol

α,ω-dihydroxy oligo(p-dioxanone), prepared by ring-opening polymerization with ethylene glycol as initiator and dibutyltin oxide as catalyst, Mn = 2100 g/mol (GPC); monomer(s): p-dioxanone; ethylene glycol

α,ω-dihydroxy oligo(p-dioxanone), prepared by ring-opening polymerization with ethylene glycol as initiator and dibutyltin oxide as catalyst, Mn = 2100 g/mol (GPC); monomer(s): p-dioxanone; ethylene glycol

Conditions
ConditionsYield
di(n-butyl)tin oxide at 110℃; for 3h;70%
p-dioxanone
3041-16-5

p-dioxanone

ethylene glycol
107-21-1

ethylene glycol

α,ω-dihydroxy oligo(p-dioxanone), prepared by ring-opening polymerization with ethylene glycol as initiator and dibutyltin oxide as catalyst, Mn = 2200 g/mol (GPC); monomer(s): p-dioxanone; ethylene glycol

α,ω-dihydroxy oligo(p-dioxanone), prepared by ring-opening polymerization with ethylene glycol as initiator and dibutyltin oxide as catalyst, Mn = 2200 g/mol (GPC); monomer(s): p-dioxanone; ethylene glycol

Conditions
ConditionsYield
at 110℃; for 48h;70%
p-dioxanone
3041-16-5

p-dioxanone

ethylene glycol
107-21-1

ethylene glycol

α,ω-dihydroxy oligo(p-dioxanone), prepared by ring-opening polymerization with ethylene glycol as initiator, Mn = 1800 g/mol (GPC), Mn = 2100 g/mol (NMR), Mn = 1400 g/mol (VPO), Mw/Mn = 1.55; monomer(s): p-dioxanone; ethylene glycol

α,ω-dihydroxy oligo(p-dioxanone), prepared by ring-opening polymerization with ethylene glycol as initiator, Mn = 1800 g/mol (GPC), Mn = 2100 g/mol (NMR), Mn = 1400 g/mol (VPO), Mw/Mn = 1.55; monomer(s): p-dioxanone; ethylene glycol

Conditions
ConditionsYield
at 110℃; for 48h;70%
p-dioxanone
3041-16-5

p-dioxanone

ethylene glycol
107-21-1

ethylene glycol

α,ω-dihydroxy oligo(p-dioxanone), prepared by ring-opening polymerization with ethylene glycol as initiator, Mn = 2300 g/mol (GPC), Mn = 2700 g/mol (NMR), Mn = 1900 g/mol (VPO), Mw/Mn = 1.62; monomer(s): p-dioxanone; ethylene glycol

α,ω-dihydroxy oligo(p-dioxanone), prepared by ring-opening polymerization with ethylene glycol as initiator, Mn = 2300 g/mol (GPC), Mn = 2700 g/mol (NMR), Mn = 1900 g/mol (VPO), Mw/Mn = 1.62; monomer(s): p-dioxanone; ethylene glycol

Conditions
ConditionsYield
di(n-butyl)tin oxide at 110℃; for 3h;70%
p-dioxanone
3041-16-5

p-dioxanone

ethylene glycol
107-21-1

ethylene glycol

α,ω-dihydroxy oligo(p-dioxanone), prepared by ring-opening polymerization with ethylene glycol as initiator, Mn = 2600 g/mol (GPC), Mn = 3000 g/mol (NMR), Mn = 1900 g/mol (VPO), Mw/Mn = 1.50; monomer(s): p-dioxanone; ethylene glycol

α,ω-dihydroxy oligo(p-dioxanone), prepared by ring-opening polymerization with ethylene glycol as initiator, Mn = 2600 g/mol (GPC), Mn = 3000 g/mol (NMR), Mn = 1900 g/mol (VPO), Mw/Mn = 1.50; monomer(s): p-dioxanone; ethylene glycol

Conditions
ConditionsYield
at 110℃; for 48h;70%
p-dioxanone
3041-16-5

p-dioxanone

ethylene glycol
107-21-1

ethylene glycol

α,ω-dihydroxy oligo(p-dioxanone), prepared by ring-opening polymerization with ethylene glycol as initiator, Mn = 2931 g/mol (GPC), Mn = 3000 g/mol (NMR), Mn = 2100 g/mol (VPO), Mw/Mn = 1.52; monomer(s): p-dioxanone; ethylene glycol

α,ω-dihydroxy oligo(p-dioxanone), prepared by ring-opening polymerization with ethylene glycol as initiator, Mn = 2931 g/mol (GPC), Mn = 3000 g/mol (NMR), Mn = 2100 g/mol (VPO), Mw/Mn = 1.52; monomer(s): p-dioxanone; ethylene glycol

Conditions
ConditionsYield
di(n-butyl)tin oxide at 110℃; for 3h;70%
p-dioxanone
3041-16-5

p-dioxanone

sodium 2-(2-hydroxyethoxy)acetate
142047-97-0

sodium 2-(2-hydroxyethoxy)acetate

Conditions
ConditionsYield
With water; sodium hydroxide Reflux;66%
p-dioxanone
3041-16-5

p-dioxanone

ethylene glycol
107-21-1

ethylene glycol

α,ω-dihydroxy oligo(p-dioxanone), prepared by ring-opening polymerization with ethylene glycol as initiator, Mn = 1900 g/mol (GPC), Mn = 2300 g/mol (NMR), Mn = 1600 g/mol (VPO), Mw/Mn = 1.73; monomer(s): p-dioxanone; ethylene glycol

α,ω-dihydroxy oligo(p-dioxanone), prepared by ring-opening polymerization with ethylene glycol as initiator, Mn = 1900 g/mol (GPC), Mn = 2300 g/mol (NMR), Mn = 1600 g/mol (VPO), Mw/Mn = 1.73; monomer(s): p-dioxanone; ethylene glycol

Conditions
ConditionsYield
di(n-butyl)tin oxide at 110℃; for 3h;65%
p-dioxanone
3041-16-5

p-dioxanone

ethylene glycol
107-21-1

ethylene glycol

α,ω-dihydroxy oligo(p-dioxanone), prepared by ring-opening polymerization with ethylene glycol as initiator, Mn = 4200 g/mol (GPC), Mn = 3000 g/mol (NMR), Mn = 3100 g/mol (VPO), Mw/Mn = 1.24; monomer(s): p-dioxanone; ethylene glycol

α,ω-dihydroxy oligo(p-dioxanone), prepared by ring-opening polymerization with ethylene glycol as initiator, Mn = 4200 g/mol (GPC), Mn = 3000 g/mol (NMR), Mn = 3100 g/mol (VPO), Mw/Mn = 1.24; monomer(s): p-dioxanone; ethylene glycol

Conditions
ConditionsYield
at 110℃; for 48h;63%
bromoethyl-2-benzyl ether
1462-37-9

bromoethyl-2-benzyl ether

p-dioxanone
3041-16-5

p-dioxanone

C13H16O4

C13H16O4

Conditions
ConditionsYield
Stage #1: p-dioxanone With sodium hydride In N,N-dimethyl-formamide at 0℃; for 1h; Inert atmosphere;
Stage #2: bromoethyl-2-benzyl ether In N,N-dimethyl-formamide at 70℃; for 12h; Inert atmosphere;
23%
p-dioxanone
3041-16-5

p-dioxanone

phenylmagnesium bromide

phenylmagnesium bromide

2-(2-hydroxy-ethoxy)-1,1-diphenyl-ethanol
23219-05-8

2-(2-hydroxy-ethoxy)-1,1-diphenyl-ethanol

p-dioxanone
3041-16-5

p-dioxanone

(4-chlorphenyl)magnesium bromide
873-77-8

(4-chlorphenyl)magnesium bromide

1,1-bis-(4-chloro-phenyl)-2-(2-hydroxy-ethoxy)-ethanol
101168-13-2

1,1-bis-(4-chloro-phenyl)-2-(2-hydroxy-ethoxy)-ethanol

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