Russian Chemical Bulletin p. 465 - 468 (1998)
Update date:2022-07-29
Topics:
Nikishin
Kislyi
Nesterov
Shestopalov
Struchkov
Semenov
The reaction of trifluoroacetylacetone with cyanothioacetamide proceeded regioselectively to form 3-cyano-6-methyl-4-trifluoromethylpyridine-2(1H)-thione from which the corresponding 2-alkylthiopyridines and 3-aminothieno[2,3-b]pyridines were obtained. The crystal and molecular structure of 3-cyano-2-ethylthio-6-methyl-4-trifluoromethylpyridine was established by X-ray diffraction analysis.
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