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Cas Database

5470-11-1

5470-11-1

Identification

  • Product Name:Hydroxylamine,hydrochloride (1:1)

  • CAS Number: 5470-11-1

  • EINECS:226-798-2

  • Molecular Weight:69.4909

  • Molecular Formula: H3NO.HCl

  • HS Code:28251000

  • Mol File:5470-11-1.mol

Synonyms:Hydroxylamine,hydrochloride (8CI,9CI);Hydroxyammonium chloride;Hydroxylamine chloride;Hydroxylamine chlorohydrate;Hydroxylammonium chloride;Oxammonium hydrochloride;hydroxylamine hydrochloride;Hydroxylamine HCl;

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Safety information and MSDS view more

  • Pictogram(s):HarmfulXn, DangerousN

  • Hazard Codes:Xn,N,E

  • Signal Word:Warning

  • Hazard Statement:H290 May be corrosive to metalsH302 Harmful if swallowed H312 Harmful in contact with skin H315 Causes skin irritation H319 Causes serious eye irritation H317 May cause an allergic skin reaction H351 Suspected of causing cancer H400 Very toxic to aquatic life

  • First-aid measures: General adviceConsult a physician. Show this safety data sheet to the doctor in attendance.If inhaled Fresh air, rest. Refer for medical attention. In case of skin contact Remove contaminated clothes. Rinse skin with plenty of water or shower. Refer for medical attention . In case of eye contact First rinse with plenty of water for several minutes (remove contact lenses if easily possible), then refer for medical attention. If swallowed Rinse mouth. Give a slurry of activated charcoal in water to drink. Refer for medical attention . SYMPTOMS: Symptoms of exposure to this chemical include eye, skin and mucous membrane irritation; burning sensation, coughing, wheezing, laryngitis, shortness of breath, headache, nausea, vomiting and methemoglobinemia. Inhalation may be fatal as a result of spasm, inflammation and edema of the larynx and bronchi; chemical pneumonitis and pulmonary edema. ACUTE/CHRONIC HAZARDS: This chemical is very irritating to skin, eyes, and mucous membranes. When heated to decomposition, it emits toxic fumes. This compound may react violently when heated to temperatures above 115°C.

  • Fire-fighting measures: Suitable extinguishing media Fires involving this material can be controlled using a dry chemical, carbon dioxide or Halon extinguisher. Flash point data for this chemical are not available; however, it is probably combustible. Wear self-contained breathing apparatus for firefighting if necessary.

  • Accidental release measures: Use personal protective equipment. Avoid dust formation. Avoid breathing vapours, mist or gas. Ensure adequate ventilation. Evacuate personnel to safe areas. Avoid breathing dust. For personal protection see section 8. Personal protection: particulate filter respirator adapted to the airborne concentration of the substance. Sweep spilled substance into covered containers. If appropriate, moisten first to prevent dusting. Do NOT wash away into sewer. Pick up and arrange disposal. Sweep up and shovel. Keep in suitable, closed containers for disposal.

  • Handling and storage: Avoid contact with skin and eyes. Avoid formation of dust and aerosols. Avoid exposure - obtain special instructions before use.Provide appropriate exhaust ventilation at places where dust is formed. For precautions see section 2.2. Dry.

  • Exposure controls/personal protection:Occupational Exposure limit valuesBiological limit values Handle in accordance with good industrial hygiene and safety practice. Wash hands before breaks and at the end of workday. Eye/face protection Safety glasses with side-shields conforming to EN166. Use equipment for eye protection tested and approved under appropriate government standards such as NIOSH (US) or EN 166(EU). Skin protection Wear impervious clothing. The type of protective equipment must be selected according to the concentration and amount of the dangerous substance at the specific workplace. Handle with gloves. Gloves must be inspected prior to use. Use proper glove removal technique(without touching glove's outer surface) to avoid skin contact with this product. Dispose of contaminated gloves after use in accordance with applicable laws and good laboratory practices. Wash and dry hands. The selected protective gloves have to satisfy the specifications of EU Directive 89/686/EEC and the standard EN 374 derived from it. Respiratory protection Wear dust mask when handling large quantities. Thermal hazards

Supplier and reference price

  • Manufacture/Brand
  • Product Description
  • Packaging
  • Price
  • Delivery
  • Purchase
  • Manufacture/Brand:TRC
  • Product Description:Hydroxylamine Hydrochloride
  • Packaging:5g
  • Price:$ 45
  • Delivery:In stock
  • Buy Now
  • Manufacture/Brand:TCI Chemical
  • Product Description:Hydroxylamine Hydrochloride >97.0%(T)
  • Packaging:500g
  • Price:$ 65
  • Delivery:In stock
  • Buy Now
  • Manufacture/Brand:TCI Chemical
  • Product Description:Hydroxylamine Hydrochloride >97.0%(T)
  • Packaging:25g
  • Price:$ 13
  • Delivery:In stock
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  • Manufacture/Brand:SynQuest Laboratories
  • Product Description:Hydroxylamine hydrochloride 99%
  • Packaging:25 g
  • Price:$ 15
  • Delivery:In stock
  • Buy Now
  • Manufacture/Brand:SynQuest Laboratories
  • Product Description:Hydroxylamine hydrochloride 99%
  • Packaging:100 g
  • Price:$ 40
  • Delivery:In stock
  • Buy Now
  • Manufacture/Brand:SynQuest Laboratories
  • Product Description:Hydroxylamine hydrochloride 99%
  • Packaging:5 g
  • Price:$ 10
  • Delivery:In stock
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  • Manufacture/Brand:Sigma-Aldrich
  • Product Description:Hydroxylamine hydrochloride
  • Packaging:1
  • Price:$ 323
  • Delivery:In stock
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  • Manufacture/Brand:Sigma-Aldrich
  • Product Description:Hydroxylamine hydrochloride 99.999% trace metals basis
  • Packaging:250g
  • Price:$ 319
  • Delivery:In stock
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  • Manufacture/Brand:Sigma-Aldrich
  • Product Description:Hydroxylamine Hydrochloride Meets ACS Specifications, Meets Reagent Specifications for testing USP/NF monographs GR ACS
  • Packaging:500 g
  • Price:$ 308.02
  • Delivery:In stock
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  • Manufacture/Brand:Sigma-Aldrich
  • Product Description:Hydroxylammonium chloride for analysis (≤ 0.000001% Hg) ACS,ISO
  • Packaging:250 g
  • Price:$ 306.17
  • Delivery:In stock
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Relevant articles and documentsAll total 29 Articles be found

Pauling, L.,Hendricks, S. B.

, p. 641 - 651 (1926)

Schoch, E. P.,Pritchett, R. H.

, p. 2042 (1916)

Rollefson, G. K.,Oldershaw, C. F.

, p. 977 (1932)

Joint production technology of hydroxylamine, hydroxylammonium salt and cyclohexanone-oxime

-

Paragraph 0015; 0030; 0031, (2017/09/26)

The invention discloses a joint production technology of hydroxylamine, hydroxylammonium salt and cyclohexanone-oxime. The material comprises the steps that reaction liquid obtained by raw materials through an ammoximation reaction and a hydrooximation reaction is extracted and separated to obtain an organic phase, the organic phase is prepared into product cyclohexanone-oxime, or part of the organic phase and part of product cyclohexanone-oxime are adopted as raw materials for an oxime hydrolysis reaction to be hydrolyzed, the organic phase in hydrolysis liquid is circulated to return to a oximation reactor, part of an inorganic phase in the hydrolysis liquid is adopted as a raw material to be circulated to return to a hydroxylamine oximation reactor, and the other part of the inorganic phase is prepared into a hydroxylamine aqueous solution and hydroxylammonium salt. The joint production technology of hydroxylamine, hydroxylammonium salt and cyclohexanone-oxime is simple in procedure, the requirement of the ammoximation reaction for the purity of the raw material cyclohexanone and the catalyst performance is lowered, a high quality cyclohexanone-oxime product without cyclohexanone is obtained, the simplification of the downstream caprolactam technology and the improvement of the product quality are benefited, and the hydroxylamine and hydroxylammonium salt product which have high additional value are obtained simultaneously.

MAGNETIC NANOSTRUCTURES AS THERANOSTIC AGENTS

-

, (2012/12/14)

The present invention relates to magnetic nanostructures as theranostic agents, which provide dual function as diagnostic and therapeutic agents. In particular, the present invention relates to compositions comprising magnetic nanostructures and their use as targeted therapeutic agents for cancers (e.g., medulloblastoma) and Alzheimer's disease and related diseases and conditions.

Metalloprotease inhibitors

-

, (2008/06/13)

Compounds of formula (I) and pharmaceutically-acceptable derivatives thereof, are matrix metalloprotease inhibitors, useful in treatment of conditions mediated by matrix metalloproteases, such as chronic dermal ulcers.

Composition for the treatment of damaged tissue

-

, (2008/06/13)

A pharmaceutical for use in damaged tissue, such as wound, treatment (e.g. healing) is described. The pharmaceutical comprising a composition which comprises: (a) a growth factor; and (b) an inhibitor agent; and optionally (c) a pharmaceutically acceptable carrier, diluent or excipient; wherein the inhibitor agent can inhibit the action of at least one specific adverse protein (e.g. a specific protease) that is upregulated in a damaged tissue, such as a wound, environment.

Heterocyclic benzenesulphonamide compounds as bradykinine antagonists

-

, (2008/06/13)

The invention concerns compounds selected among the group consisting of (i) compounds of formula (I) wherein: Het1 represents a nitrogenous heterocycle with 5 apices, in particular imidazole, pyrazole, or triazole; Het2 represents a nitrogenous heterocycle with 4, 5 or 6 apices, selected among the heterocycles: (II) wherein R1and R2are defined as mentioned in the description; and (ii) their additive salts. The invention also concerns the method for preparing said compounds and their use in therapy, in particular for treating pathologies involving bradykinine.

Process route upstream and downstream products

Process route

2,2-dinitropropane
595-49-3

2,2-dinitropropane

hydroxylamine hydrochloride
5470-11-1

hydroxylamine hydrochloride

dinitrogen monoxide
10024-97-2

dinitrogen monoxide

Conditions
Conditions Yield
With hydrogenchloride; byproducts: acetone; with dild. HCl,cooling; pptg. of Sn with H2S,filtering,evapn.,washing with ether-alcohol;
cyclohexanone-oxime
100-64-1

cyclohexanone-oxime

hydroxylamine hydrochloride
5470-11-1

hydroxylamine hydrochloride

Conditions
Conditions Yield
With hydrogenchloride; In hexane; water; at 40 ℃; for 0.666667h; under 2250.23 Torr;
potassium nitrite
7758-09-0

potassium nitrite

hydroxylamine hydrochloride
5470-11-1

hydroxylamine hydrochloride

Conditions
Conditions Yield
With hydrogenchloride; sulfur dioxide; In water; byproducts: H2SO4; react. in water contg. ice and K-acetate leading SO2 into it,mixing,at 0°C;filtering,washing with 0.5 n HCl,hydrolysis at 100°C,for 2h; pptg. of H2SO4 with BaCl2,filtering,evapn.;
85%
hydrogenchloride
7647-01-0,15364-23-5

hydrogenchloride

hydroxylamine hydrochloride
5470-11-1

hydroxylamine hydrochloride

ammonium chloride

ammonium chloride

Conditions
Conditions Yield
In sulfuric acid; Electrolysis; mixing dild. HCl with dild. HNO3 in an amalgated lead cell as cathode under applying lead anode (anode liquid: dild. H2SO4), 15°C, current: 50 A and 25 V; evapn., then cooling, removing of NH4Cl by treating with cold abs. alc., recrystn. from alcohol;
80%
In sulfuric acid; aq. H2SO4; Electrolysis; mixing dild. HCl with dild. HNO3 in an amalgated lead cell as cathode under applying lead anode (anode liquid: dild. H2SO4), 15°C, current: 50 A and 25 V; evapn., then cooling, removing of NH4Cl by treating with cold abs. alc., recrystn. from alcohol;
80%
sodium nitrite
7632-00-0

sodium nitrite

hydroxylamine hydrochloride
5470-11-1

hydroxylamine hydrochloride

acetone oxime
127-06-0

acetone oxime

Conditions
Conditions Yield
With sulfur dioxide; sodium carbonate; acetone; In not given; react. of SO2,Na2CO3 and NaNO2;adding acetone to the formed Na-hydroxylamine disulfonate at 70 °C;neutralization with NaOH; evapn.,recrystn. from water;
53-77
ethyl nitrate
625-58-1

ethyl nitrate

tin(ll) chloride

tin(ll) chloride

hydroxylamine hydrochloride
5470-11-1

hydroxylamine hydrochloride

ammonia
7664-41-7

ammonia

tin(IV) chloride
7646-78-8

tin(IV) chloride

Conditions
Conditions Yield
With hydrogenchloride; In hydrogenchloride; byproducts: C2H5OH, H2O; in concd. HCl soln.; evapn. of the alcohol,diluting with water,pptg. of the Sn with H2S,evapn. and crystn. from alcohol;
90%
<1
Mo(NO)(NH<sub>2</sub>O)(C<sub>6</sub>H<sub>4</sub>S<sub>2</sub>C<sub>2</sub>H<sub>4</sub>S<sub>2</sub>C<sub>6</sub>H<sub>4</sub>)*C<sub>4</sub>H<sub>8</sub>O

Mo(NO)(NH2O)(C6H4S2C2H4S2C6H4)*C4H8O

{Mo(NO)(Cl)(dttd)}

{Mo(NO)(Cl)(dttd)}

hydroxylamine hydrochloride
5470-11-1

hydroxylamine hydrochloride

Conditions
Conditions Yield
With hydrogenchloride; In methanol; byproducts: NH4Cl, N2H5Cl; (N2); HCl bubbled through a soln. of the Mo-complex at 0°C for 15 min; soln. stirred for 1.5 h at room temp.; N2 bubbled through the suspn. for 15 min; ppt. filtered, washed with methanol and diethyl ether; recrystd. from hot THF;
93%
fulminic acid
51060-05-0,20411-61-4

fulminic acid

hydroxylamine hydrochloride
5470-11-1

hydroxylamine hydrochloride

Conditions
Conditions Yield
With hydrogenchloride; water; byproducts: HCOOH;
[Ni(II)(salicylaldehyde oximate)2]
54515-04-7,50897-08-0,14363-30-5

[Ni(II)(salicylaldehyde oximate)2]

ethylenediamine hydrochloride
18299-54-2

ethylenediamine hydrochloride

Ni(C<sub>6</sub>H<sub>4</sub>(O)CHNC<sub>2</sub>H<sub>4</sub>NH<sub>2</sub>)2

Ni(C6H4(O)CHNC2H4NH2)2

hydroxylamine hydrochloride
5470-11-1

hydroxylamine hydrochloride

Conditions
Conditions Yield
In methanol; stirring the soln. for 30 min between room temp. and 60°C, pptn.; filtration, washing with water, recrystn. from acetone;
90%
(E,Z)-(4-chlorophenyl)(cyclopropyl)methanone oxime
67038-82-8

(E,Z)-(4-chlorophenyl)(cyclopropyl)methanone oxime

4-chlorophenyl cyclopropyl ketone
6640-25-1

4-chlorophenyl cyclopropyl ketone

hydroxylamine hydrochloride
5470-11-1

hydroxylamine hydrochloride

Conditions
Conditions Yield

Global suppliers and manufacturers

Global( 241) Suppliers
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  • AmoyChem Co.,Ltd
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  • Chemwill Asia Co., Ltd.
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  • Hangzhou Dingyan Chem Co., Ltd
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  • EAST CHEMSOURCES LIMITED
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  • Country:China (Mainland)
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