Tris(trimethylsilyl)silyl Radical Induced Bicyclization of 1,6-Dienes and 1,6-Enynes Providing 3,3-Bis(trimethylsilyl)-3-silabicyclooctanes and 3-Silabicyclooct-1-enes

DOI: 10.1246/bcsj.66.2348

Source and publish data:

Bulletin of the Chemical Society of Japan p. 2348 - 2355 (1993)

Update date:2022-07-30

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Authors:

Miura, Katsukiyo

Oshima, Koichiro

Utimoto, Kiitiro

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Article abstract of DOI:10.1246/bcsj.66.2348

Treatment of 1,6-dienes with tris(trimethylsilyl)silane in the presence of Et3B or α,α'-azobis(isobutyronitrile) afforded 3,3-bis(trimethylsilyl)-3-silabicyclo<3.3.0>octanes in addition to monocyclized cyclopentanes.Bicyclization of 1,6-enynes provided th

Full text of DOI:10.1246/bcsj.66.2348

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