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High quality (R)-Lactate supplier in China
Cas No: 10326-41-7
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whmule Best price fast delivery cas 10326-41-7 D-(?)-Lactic acid china supplier
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USD $ 6.0-12.0 / Gram 50 Gram 100000 Kilogram/Day WUHAN MULEI NEW MATERIAL CO., LTD Contact Supplier
D(-)-lactic acid
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(2R)-2-hydroxypropanoate
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D-(-)-Lactic acid
Cas No: 10326-41-7
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(R)-Lactate
Cas No: 10326-41-7
USD $ 3.0-3.0 / Kilogram 1 Kilogram 1-100 Metric Ton/Month Dayang Chem (Hangzhou) Co.,Ltd. Contact Supplier
D(-)-lactic acid
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USD $ 1.0-1.0 / Kilogram 1 Kilogram 1000 Metric Ton/Year Henan Sinotech Import&Export Corporation Contact Supplier
TIANFU-CHEM - (R)-Lactate
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USD $ 1000.0-1000.0 / Kilogram 1 Kilogram 10 Metric Ton/Month Henan Tianfu Chemical Co., Ltd. Contact Supplier
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BLOOM TECH Advanced API/Technology support D-(-)-Lactic acid CAS 10326-41-7
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10326-41-7 Usage

InChI:InChI=1/C3H6O3/c1-2(4)3(5)6/h2,4H,1H3,(H,5,6)/t2-/m0/s1

10326-41-7 Well-known Company Product Price

Brand (Code)Product description CAS number Packaging Price Detail
TCI America (L0266)  D-Lactic Acid  >90.0%(T) 10326-41-7 25g 3,320.00CNY Detail
TCI America (L0266)  D-Lactic Acid  >90.0%(T) 10326-41-7 5g 950.00CNY Detail

10326-41-7SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 10, 2017

Revision Date: Aug 10, 2017

1.Identification

1.1 GHS Product identifier

Product name (R)-lactic acid

1.2 Other means of identification

Product number -
Other names D-lactate

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only.
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:10326-41-7 SDS

10326-41-7Synthetic route

2-oxo-propionic acid
127-17-3

2-oxo-propionic acid

D-Lactic acid
10326-41-7

D-Lactic acid

Conditions
ConditionsYield
With phosphonic Acid; lactate dehydrogenase V152R mutant; phosphorous dehydrogenase I151R mutant; NAD In aq. buffer at 30℃; for 12h; pH=7.5; Reagent/catalyst; Time; Enzymatic reaction;100%
With phosphate buffer; ADH (EC 1.1.1.2); MV2+; nicotinamide adenine dinucleotide phosphate In water; tert-butyl alcohol for 30h; electrolysis' other reaction system;8.3E-6 mol
With Leuconostoc lactis ketoacid reductase; NADH In aq. phosphate buffer at 35℃; for 10h; pH=7; Enzymatic reaction; enantioselective reaction;65.2 %Chromat.
(2R)-propane-1,2-diol
4254-14-2

(2R)-propane-1,2-diol

D-Lactic acid
10326-41-7

D-Lactic acid

Conditions
ConditionsYield
Stage #1: (2R)-propane-1,2-diol With Rh(OTf)(trop2NH)(PPh3); water; cyclohexanone; sodium hydroxide at 20℃; for 5h; Inert atmosphere;
Stage #2: With hydrogenchloride In water Inert atmosphere; chemoselective reaction;
91%
1-dodecyl L-lactate
232944-80-8

1-dodecyl L-lactate

A

D-Lactic acid
10326-41-7

D-Lactic acid

B

1-dodecyl alcohol
112-53-8

1-dodecyl alcohol

Conditions
ConditionsYield
With 2C33H37N*H2O7S2; water at 80℃; for 4h;A 80%
B 87%
methyl lactate
547-64-8

methyl lactate

A

D-Lactic acid
10326-41-7

D-Lactic acid

B

(S)-Methyl lactate
27871-49-4

(S)-Methyl lactate

Conditions
ConditionsYield
With Dactylosporangium aurantiacum esterase WDEst9 In aq. buffer at 30℃; for 3h; pH=8.5; Catalytic behavior; Concentration; pH-value; Reagent/catalyst; Solvent; Temperature; Time; Green chemistry; Enzymatic reaction; enantioselective reaction;A n/a
B 86.7%
D-Alanine
338-69-2

D-Alanine

D-Lactic acid
10326-41-7

D-Lactic acid

Conditions
ConditionsYield
With sulfuric acid; sodium nitrite82%
With trifluoroacetic acid; sodium nitrite In water at 20℃; for 6h;62%
With sulfuric acid; sodium nitrite In water at 0℃; for 2h;
Isobutyl (R)-lactate
61597-96-4

Isobutyl (R)-lactate

D-Lactic acid
10326-41-7

D-Lactic acid

Conditions
ConditionsYield
With lithium hydroxide monohydrate In tetrahydrofuran; water at 0 - 20℃; for 48h; Inert atmosphere;77%
D-Alanine
338-69-2

D-Alanine

A

D-Lactic acid
10326-41-7

D-Lactic acid

B

D-lactide
4511-42-6

D-lactide

Conditions
ConditionsYield
With sulfuric acid; sodium nitrite In water at 0 - 20℃; stereoselective reaction;A 58%
B < 3 %Spectr.
propylene glycol
57-55-6

propylene glycol

D-Lactic acid
10326-41-7

D-Lactic acid

Conditions
ConditionsYield
With phosphate buffer; Gluconobacter oxydans DSM 2003 cells at 28℃; for 20h; pH=6.0;48%
ethyl 2-hydroxypropionate
97-64-3, 2676-33-7

ethyl 2-hydroxypropionate

A

L-Lactic acid
79-33-4

L-Lactic acid

B

D-Lactic acid
10326-41-7

D-Lactic acid

C

(R)-Ethyl lactate
7699-00-5

(R)-Ethyl lactate

Conditions
ConditionsYield
With ammonium hydroxide at 30℃; pH=6.9;A n/a
B n/a
C 34.5%
citric acid
77-92-9

citric acid

A

Oxalacetic acid
328-42-7

Oxalacetic acid

B

L-Lactic acid
79-33-4

L-Lactic acid

C

D-Lactic acid
10326-41-7

D-Lactic acid

D

3-hydroxy-2-butanon
513-86-0, 52217-02-4

3-hydroxy-2-butanon

E

acetic acid
64-19-7

acetic acid

F

2-oxo-propionic acid
127-17-3

2-oxo-propionic acid

Conditions
ConditionsYield
With Leuconostoc mesenteroides at 30℃; for 1h; potassium phosphate buffer, pH 5.0; other conditions also investigated; several substrates investigated;A 0.66%
B 0.06%
C 1.77%
D 6.86%
E 15.5%
F 0.05%
citric acid
77-92-9

citric acid

A

Oxalacetic acid
328-42-7

Oxalacetic acid

B

L-Lactic acid
79-33-4

L-Lactic acid

C

D-Lactic acid
10326-41-7

D-Lactic acid

D

acetic acid
64-19-7

acetic acid

E

2-oxo-propionic acid
127-17-3

2-oxo-propionic acid

F

dimethylglyoxal
431-03-8

dimethylglyoxal

Conditions
ConditionsYield
With Leuconostoc mesenteroides at 30℃; for 1h; potassium phosphate buffer, pH 5.0; other conditions also investigated; several substrates investigated;A 0.66%
B 0.06%
C 1.77%
D 15.5%
E 0.05%
F 1.72%
LACTIC ACID
849585-22-4

LACTIC ACID

D-Lactic acid
10326-41-7

D-Lactic acid

Conditions
ConditionsYield
mit Hilfe von Chinin;
mit Hilfe von Morphin;
With MORPHIN
mit Hilfe von Strychnin;
D-Fructose
57-48-7

D-Fructose

D-Lactic acid
10326-41-7

D-Lactic acid

Conditions
ConditionsYield
bei der Vergaerung durch Bacterium coli communis (zu mehr als 75prozent aus l-Milchsaeure besteht);
bei der Vergaerung durch Lactobacillus Leichmanni;
pyruvic acid menthyl ester
53651-68-6

pyruvic acid menthyl ester

D-Lactic acid
10326-41-7

D-Lactic acid

Conditions
ConditionsYield
With aluminium amalgam und Verseifung der Produkte mit alkoholischem Kaliumhydroxyd;
(R)-2-chloropropionic acid
7474-05-7

(R)-2-chloropropionic acid

D-Lactic acid
10326-41-7

D-Lactic acid

Conditions
ConditionsYield
With water; silver(l) oxide
(S)-2-bromopropanoic acid
32644-15-8

(S)-2-bromopropanoic acid

D-Lactic acid
10326-41-7

D-Lactic acid

Conditions
ConditionsYield
With potassium hydroxide
R-(+)-2-bromopropionic acid
10009-70-8

R-(+)-2-bromopropionic acid

D-Lactic acid
10326-41-7

D-Lactic acid

Conditions
ConditionsYield
With water; silver carbonate
(S)-2-iodo-propionic acid
18791-44-1

(S)-2-iodo-propionic acid

furan-2,3,5(4H)-trione pyridine (1:1)

furan-2,3,5(4H)-trione pyridine (1:1)

D-Lactic acid
10326-41-7

D-Lactic acid

Conditions
ConditionsYield
Hydrolysis;
(S)-2-iodo-propionic acid
18791-44-1

(S)-2-iodo-propionic acid

A

LACTIC ACID
849585-22-4

LACTIC ACID

B

D-Lactic acid
10326-41-7

D-Lactic acid

Conditions
ConditionsYield
With sodium hydroxide Hydrolysis;
mannitol
69-65-8

mannitol

D-Lactic acid
10326-41-7

D-Lactic acid

Conditions
ConditionsYield
bei der Vergaerung durch eine auf Birnen gefundene Mikrobe;
bei der Vergaerung durch Bacterium formicicum;
durch Vergaerung mit Pneumokokkus(Friedlaender);
mannitol
69-65-8

mannitol

A

ethanol
64-17-5

ethanol

B

D-Lactic acid
10326-41-7

D-Lactic acid

C

acetic acid
64-19-7

acetic acid

D

butan-1-ol
71-36-3

butan-1-ol

Conditions
ConditionsYield
bei der Vergaerung durch Clostridium thermocellum;Produkt 5:Buttersaeure;
D-sorbitol
50-70-4

D-sorbitol

A

D-Fructose
57-48-7

D-Fructose

B

D-Lactic acid
10326-41-7

D-Lactic acid

C

D-glucose
50-99-7

D-glucose

Conditions
ConditionsYield
beim Durchleiten von sorbithaltigem Rinderblut durch isolierte Hundeleber;
L-arabinose
5328-37-0

L-arabinose

D-Lactic acid
10326-41-7

D-Lactic acid

Conditions
ConditionsYield
durch Vergaerung mit Pneumokokkus(Friedlaender);
2-amino-2-deoxyglucose
3416-24-8

2-amino-2-deoxyglucose

D-Lactic acid
10326-41-7

D-Lactic acid

Conditions
ConditionsYield
bei der Einw. von Bac. subtilis und Bac. prodigiosus;
D-glucose
50-99-7

D-glucose

D-Lactic acid
10326-41-7

D-Lactic acid

Conditions
ConditionsYield
bei der Gaerung der alkalischen Loesungen durch den Bacillus acidi laevolactici;
at 36℃; bei der Gaerung der alkalischen Loesungen durch den Bacillus acidi laevolactici;
bei der Vergaerung durch eine auf Birnen gefundene Mikrobe;
D-Galactose
59-23-4

D-Galactose

D-Lactic acid
10326-41-7

D-Lactic acid

Conditions
ConditionsYield
durch Vergaerung mit Pneumokokkus(Friedlaender);
bei der Vergaerung durch Lactobacillus Leichmanni;
Conditions
ConditionsYield
bei der Gaerung der alkalischen Loesungen durch den Typhusbazillus;
durch Vergaerung mit Pneumokokkus(Friedlaender);
durch den Pilz Rhizopus chinensis;
beim Vergaeren durch Betacoccus arabinosaceus;
Vergaerung durch Lactobacillus leichmannii sowie Reinigung ueber das Zinksalz und durch folgende Einw. eines Ionenaustausch-Harzes;
D-glucosaminic acid
3646-68-2

D-glucosaminic acid

A

D-Lactic acid
10326-41-7

D-Lactic acid

B

succinic acid
110-15-6

succinic acid

Conditions
ConditionsYield
durch Escherishia Coli;
D-glucosaminic acid
3646-68-2

D-glucosaminic acid

A

D-Lactic acid
10326-41-7

D-Lactic acid

B

oxalic acid
144-62-7

oxalic acid

C

acetic acid
64-19-7

acetic acid

Conditions
ConditionsYield
nach Verabreichung an Hunde und Kaninchen im Harn ausscheiden;
fructose-1,6-bisphosphate
488-69-7

fructose-1,6-bisphosphate

D-Lactic acid
10326-41-7

D-Lactic acid

Conditions
ConditionsYield
With GLUTATHIONE; toluene bei der Vergaerung durch Hefe;
With GLUTATHIONE; toluene bei der Vergaerung durch Hefe; in diesen Gaerensaetzen entsteht vielleicht intermediaer Methylglyoxal durch einen nichtfermentativen Prozess;
D-Lactic acid
10326-41-7

D-Lactic acid

2-oxo-propionic acid
127-17-3

2-oxo-propionic acid

Conditions
ConditionsYield
With oxygen at 100℃; under 75.0075 Torr; for 8h; Temperature; Pressure; Autoclave;94.3%
With mutant 3-isopropylmalate dehydrogenase(Gly89-Gly-Leu90); nicotinamide adenine dinucleotide In water at 60℃; for 2h; pH=7.8; Enzyme kinetics;
With nicotinamide flucytosine dinucleotide at 25℃; pH=7.5; aq. buffer; Enzymatic reaction;
With D-lactate dehydrogenase of Planctomyces brasiliensis at 25℃; for 1h; pH=7; Concentration; pH-value; Reagent/catalyst; Temperature; Enzymatic reaction;
With D-lactate oxidase from Saccharomyces cerevisiae; oxygen; catalase In aq. buffer at 30℃; pH=7.4; Reagent/catalyst; Enzymatic reaction;
D-Lactic acid
10326-41-7

D-Lactic acid

didecyldimethylammonium chloride
7173-51-5

didecyldimethylammonium chloride

didecyldimethylammonium L-lactate
1308889-80-6

didecyldimethylammonium L-lactate

Conditions
ConditionsYield
Stage #1: D-Lactic acid With potassium hydroxide In water Reflux;
Stage #2: didecyldimethylammonium chloride In water at 20℃; for 5h;
94%
D-Lactic acid
10326-41-7

D-Lactic acid

((S)-1-Phenyl-ethyl)-{4-[6-piperidin-4-yl-3-(3-trifluoromethyl-phenyl)-pyridazin-4-yl]-pyrimidin-2-yl}-amine
271247-18-8

((S)-1-Phenyl-ethyl)-{4-[6-piperidin-4-yl-3-(3-trifluoromethyl-phenyl)-pyridazin-4-yl]-pyrimidin-2-yl}-amine

(R)-2-Hydroxy-1-{4-[5-[2-((S)-1-phenyl-ethylamino)-pyrimidin-4-yl]-6-(3-trifluoromethyl-phenyl)-pyridazin-3-yl]-piperidin-1-yl}-propan-1-one

(R)-2-Hydroxy-1-{4-[5-[2-((S)-1-phenyl-ethylamino)-pyrimidin-4-yl]-6-(3-trifluoromethyl-phenyl)-pyridazin-3-yl]-piperidin-1-yl}-propan-1-one

Conditions
ConditionsYield
With benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide93%
D-Lactic acid
10326-41-7

D-Lactic acid

9-anthryldiazomethane
10401-59-9

9-anthryldiazomethane

(R)-2-Hydroxy-propionic acid anthracen-9-ylmethyl ester

(R)-2-Hydroxy-propionic acid anthracen-9-ylmethyl ester

Conditions
ConditionsYield
In diethyl ether for 0.5h; Ambient temperature;90%
In diethyl ether for 0.5h; Ambient temperature;
In methanol at 20℃; for 0.5h;
D-Lactic acid
10326-41-7

D-Lactic acid

benzyl alcohol
100-51-6

benzyl alcohol

Conditions
ConditionsYield
Stage #1: benzyl alcohol With toluene-4-sulfonic acid In benzene for 0.5h; Reflux;
Stage #2: D-Lactic acid In benzene Reflux;
88%
With salicylaldehyde In toluene at 100℃; for 18h; Inert atmosphere; chemoselective reaction;85%
With hydrogenchloride for 18h;51.3%
D-Lactic acid
10326-41-7

D-Lactic acid

tert-butyldimethylsilyl chloride
18162-48-6

tert-butyldimethylsilyl chloride

(2S)-2-<(tert-Butyldimethylsilyl)oxy>lactic acid
129919-88-6

(2S)-2-<(tert-Butyldimethylsilyl)oxy>lactic acid

Conditions
ConditionsYield
With dmap; triethylamine87%
ethanol
64-17-5

ethanol

D-Lactic acid
10326-41-7

D-Lactic acid

(R)-Ethyl lactate
7699-00-5

(R)-Ethyl lactate

Conditions
ConditionsYield
With salicylaldehyde at 80℃; for 28h; Inert atmosphere; chemoselective reaction;85%
With sulfuric acid at 120℃; for 8h; Molecular sieve;25%
With hydrogenchloride
With sulfuric acid; benzene durch azeotrope Destillation;
D-Lactic acid
10326-41-7

D-Lactic acid

9-(6-methoxypyridin-3-yl)-3-methyl-1-(piperidin-4-yl)-3,4-dihydropyrimido[5,4-c][1,5]naphthyridin-2(1H)-one hydrochloride salt

9-(6-methoxypyridin-3-yl)-3-methyl-1-(piperidin-4-yl)-3,4-dihydropyrimido[5,4-c][1,5]naphthyridin-2(1H)-one hydrochloride salt

(R)-1-[1-(2-hydroxypropionyl)piperidine-4-yl]-9-(6-methoxypyridin-3-yl)-3-methyl-3,4-dihydropyrimido[5,4-c][1,5]naphthyridin-2(1H)-one

(R)-1-[1-(2-hydroxypropionyl)piperidine-4-yl]-9-(6-methoxypyridin-3-yl)-3-methyl-3,4-dihydropyrimido[5,4-c][1,5]naphthyridin-2(1H)-one

Conditions
ConditionsYield
Stage #1: 9-(6-methoxypyridin-3-yl)-3-methyl-1-(piperidin-4-yl)-3,4-dihydropyrimido[5,4-c][1,5]naphthyridin-2(1H)-one hydrochloride salt With triethylamine In dichloromethane at 20℃; for 0.5h;
Stage #2: D-Lactic acid With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 20℃; for 2h;
81.4%
Stage #1: 9-(6-methoxypyridin-3-yl)-3-methyl-1-(piperidin-4-yl)-3,4-dihydropyrimido[5,4-c][1,5]naphthyridin-2(1H)-one hydrochloride salt With triethylamine In dichloromethane at 20℃; for 0.5h;
Stage #2: D-Lactic acid With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 20℃; for 2h;
88mg
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine In dichloromethane; water at 20℃; for 2h;88 mg
D-Lactic acid
10326-41-7

D-Lactic acid

methyl 4-({4-[3-cyano-4-(piperidin-4-yloxy)phenyl]pyrimidin-2-yl}amino)benzoate
1292317-84-0

methyl 4-({4-[3-cyano-4-(piperidin-4-yloxy)phenyl]pyrimidin-2-yl}amino)benzoate

trifluoroacetic acid
76-05-1

trifluoroacetic acid

methyl 4-({4-[3-cyano-4-({1-[(2R)-2-hydroxypropanoyl]piperidin-4-yl}oxy)phenyl]pyrimidin-2-yl}amino)benzoate trifluoroacetate

methyl 4-({4-[3-cyano-4-({1-[(2R)-2-hydroxypropanoyl]piperidin-4-yl}oxy)phenyl]pyrimidin-2-yl}amino)benzoate trifluoroacetate

Conditions
ConditionsYield
Stage #1: D-Lactic acid; methyl 4-({4-[3-cyano-4-(piperidin-4-yloxy)phenyl]pyrimidin-2-yl}amino)benzoate With N-ethyl-N,N-diisopropylamine; HATU In N,N-dimethyl-formamide for 16h;
Stage #2: trifluoroacetic acid In water; acetonitrile
81%
1,10-Phenanthroline
66-71-7

1,10-Phenanthroline

malachite

malachite

D-Lactic acid
10326-41-7

D-Lactic acid

[copper(II)-di(lactato)-(1,10-phenanthroline)]*4H2O

[copper(II)-di(lactato)-(1,10-phenanthroline)]*4H2O

Conditions
ConditionsYield
In ethanol suspn. of Cu compd. and lactic acid in EtOH refluxed for 4 h at 75°C, 1,10-phenanthroline added, refluxed for 2 h, then stirred for several d; filtered, washed with EtOH, dried over CaCl2; elem. anal.;80%
D-Lactic acid
10326-41-7

D-Lactic acid

vanadia

vanadia

bis(triphenylphosphine)iminium chloride
21050-13-5

bis(triphenylphosphine)iminium chloride

[VO2(lac)]2(Ph3P=NPPh3)2

[VO2(lac)]2(Ph3P=NPPh3)2

Conditions
ConditionsYield
With tetraethylammonium hydroxide In water; acetonitrile V2O5 was added to aq. soln. Et4NOH and warmed to 60°C, soln. was filtered, lactic acid was added with stirring, pH was raised from 3.0 to6.3 by Et4NOH, soln. was concd. in air stream, soln. PPNCl in MeCN was added and left overnight; product was filtered, washed with MeCN, and dried in vacuo; elem. anal.;78%
D-Lactic acid
10326-41-7

D-Lactic acid

(rac)-4-bromo-5,6,7,8-tetrahydroisoquinolin-8-amine
1428651-87-9

(rac)-4-bromo-5,6,7,8-tetrahydroisoquinolin-8-amine

(R)-N-((R,S)-4-bromo-5,6,7,8-tetrahydro-isoquinolin-8-yl)-2-hydroxy-propionamide
1469979-88-1

(R)-N-((R,S)-4-bromo-5,6,7,8-tetrahydro-isoquinolin-8-yl)-2-hydroxy-propionamide

Conditions
ConditionsYield
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine In dichloromethane at 0 - 20℃; Inert atmosphere;77%
D-Lactic acid
10326-41-7

D-Lactic acid

5-{9-(cyclopropylmethyl)-8-[(3R)-3-methylpiperazin-1-yl]-6-morpholin-4-yl-9H-purin-2-yl}pyrimidin-2-amine
1222104-79-1

5-{9-(cyclopropylmethyl)-8-[(3R)-3-methylpiperazin-1-yl]-6-morpholin-4-yl-9H-purin-2-yl}pyrimidin-2-amine

(2R)-1-{(2R)-4-[2-(2-Aminopyrimidin-5-yl)-9-(cyclopropylmethyl)-6-morpholin-4-yl-9H-purin-8-yl]-2-methylpiperazin-1-yl}-1-oxopropan-2-ol
1222104-99-5

(2R)-1-{(2R)-4-[2-(2-Aminopyrimidin-5-yl)-9-(cyclopropylmethyl)-6-morpholin-4-yl-9H-purin-8-yl]-2-methylpiperazin-1-yl}-1-oxopropan-2-ol

Conditions
ConditionsYield
With benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide In dichloromethane; N,N-dimethyl-formamide at 20 - 40℃; for 40.5h;76%
D-Lactic acid
10326-41-7

D-Lactic acid

benzyl bromide
100-39-0

benzyl bromide

Conditions
ConditionsYield
Stage #1: D-Lactic acid With caesium carbonate In methanol; water pH=7;
Stage #2: benzyl bromide In methanol; water; N,N-dimethyl-formamide at 20℃; for 6h;
75%
With sodium hydrogencarbonate In N,N-dimethyl-formamide at 80 - 100℃; for 1h;68%
With potassium carbonate In N,N-dimethyl-formamide for 14h; Ambient temperature;
In N,N-dimethyl-formamide at 50℃; for 6h; Inert atmosphere; Glovebox; Sealed tube;
D-Lactic acid
10326-41-7

D-Lactic acid

(rac)-6-(8-amino-5,6,7,8-tetrahydroisoquinolin-4-yl)-1-methyl-3,4-dihydroquinolin-2(1H)-one
1428651-83-5

(rac)-6-(8-amino-5,6,7,8-tetrahydroisoquinolin-4-yl)-1-methyl-3,4-dihydroquinolin-2(1H)-one

(2R)-2-hydroxy-N-[(4R,S)-4-(1-methyl-2-oxo-1,2,3,4-tetrahydroquinolin-6-yl)-5,6,7,8-tetrahydroisoquinolin-8-yl]propanamide
1428652-31-6

(2R)-2-hydroxy-N-[(4R,S)-4-(1-methyl-2-oxo-1,2,3,4-tetrahydroquinolin-6-yl)-5,6,7,8-tetrahydroisoquinolin-8-yl]propanamide

Conditions
ConditionsYield
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; diisopropylamine In dichloromethane at 0 - 20℃; Inert atmosphere;75%
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine In dichloromethane at 0℃; Inert atmosphere;75%
D-Lactic acid
10326-41-7

D-Lactic acid

3-(((1R,2R)-2-((4-(6-fluorobenzo[d]isoxazole-3-yl)piperidin-1-yl)methyl)cyclohexyl)methyl)oxazolidine-2-one

3-(((1R,2R)-2-((4-(6-fluorobenzo[d]isoxazole-3-yl)piperidin-1-yl)methyl)cyclohexyl)methyl)oxazolidine-2-one

3-(((1R,2R)-2-((4-(6-fluorobenzo[d]isoxazole-3-yl)piperidin-1-yl)methyl)cyclohexyl)methyl)oxazolidine-2-one lactic acid salt

3-(((1R,2R)-2-((4-(6-fluorobenzo[d]isoxazole-3-yl)piperidin-1-yl)methyl)cyclohexyl)methyl)oxazolidine-2-one lactic acid salt

Conditions
ConditionsYield
In ethanol Reflux;74.1%
D-Lactic acid
10326-41-7

D-Lactic acid

(R)-3-iodo-1-(piperidin-3-yl)-1H-pyrazolo[3,4-d]pyrimidin-4-amine

(R)-3-iodo-1-(piperidin-3-yl)-1H-pyrazolo[3,4-d]pyrimidin-4-amine

(R)-1-((R)-3-(4-amino-3-iodo-1H-pyrazolo[3,4-d]pyrimidin-1-yl)piperidin-1-yl)-2-hydroxypropan-1-one

(R)-1-((R)-3-(4-amino-3-iodo-1H-pyrazolo[3,4-d]pyrimidin-1-yl)piperidin-1-yl)-2-hydroxypropan-1-one

Conditions
ConditionsYield
Stage #1: D-Lactic acid With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine In N,N-dimethyl-formamide at 20℃; for 0.5h;
Stage #2: (R)-3-iodo-1-(piperidin-3-yl)-1H-pyrazolo[3,4-d]pyrimidin-4-amine In N,N-dimethyl-formamide at 20℃; for 5h;
73.3%
D-Lactic acid
10326-41-7

D-Lactic acid

5-(9-isobutyl-6-morpholin-4-yl-8-piperazin-1-yl-9H-purin-2-yl)pyrimidin-2-amine
1222105-31-8

5-(9-isobutyl-6-morpholin-4-yl-8-piperazin-1-yl-9H-purin-2-yl)pyrimidin-2-amine

(2R)-1-{4-[2-(2-Aminopyrimidin-5-yl)-9-isobutyl-6-morpholin-4-yl-9H-purin-8-yl]piperazin-1-yl}-1-oxopropan-2-ol
1222104-78-0

(2R)-1-{4-[2-(2-Aminopyrimidin-5-yl)-9-isobutyl-6-morpholin-4-yl-9H-purin-8-yl]piperazin-1-yl}-1-oxopropan-2-ol

Conditions
ConditionsYield
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine In N,N-dimethyl-formamide at 20℃; for 96h;73%
D-Lactic acid
10326-41-7

D-Lactic acid

5-bromo-3-fluoro-N1-(propan-2-yl)benzene-1,2-diamine

5-bromo-3-fluoro-N1-(propan-2-yl)benzene-1,2-diamine

(1R)-1-[6-bromo-4-fluoro-1-(propan-2-yl)-1H-benzimidazol-2-yl]ethan-1-ol

(1R)-1-[6-bromo-4-fluoro-1-(propan-2-yl)-1H-benzimidazol-2-yl]ethan-1-ol

Conditions
ConditionsYield
for 44h; Time; Heating;71%
D-Lactic acid
10326-41-7

D-Lactic acid

5-amino-N-(4-(azepan-4-yloxy)pyrimidin-5-yl)-2-(2,6-difluorophenyl)thiazole-4-carboxamide
1422470-13-0

5-amino-N-(4-(azepan-4-yloxy)pyrimidin-5-yl)-2-(2,6-difluorophenyl)thiazole-4-carboxamide

C20H20F2N6O2S*C3H6O3

C20H20F2N6O2S*C3H6O3

Conditions
ConditionsYield
In methanol; dichloromethane at 20 - 30℃; for 0.5h;67.8%
D-Lactic acid
10326-41-7

D-Lactic acid

bis(trichloromethyl) carbonate
32315-10-9

bis(trichloromethyl) carbonate

L-lactic acid O-carboxyanhydride
91049-50-2

L-lactic acid O-carboxyanhydride

Conditions
ConditionsYield
With pyrographite In tetrahydrofuran at 0 - 20℃; for 8h;65%
D-Lactic acid
10326-41-7

D-Lactic acid

5-chloro-N-[3,5-dimethyl-1-(4-piperidinyl)-1H-pyrazol-4-yl]-4-(pyrazolo[1,5-a]pyridin-3-yl)-2-pyrimidinamine

5-chloro-N-[3,5-dimethyl-1-(4-piperidinyl)-1H-pyrazol-4-yl]-4-(pyrazolo[1,5-a]pyridin-3-yl)-2-pyrimidinamine

(2R)-1-[4-(4-{[5-chloro-4-(pyrazolo[1,5-a]pyridin-3-yl)-2-pyrimidinyl]amino}-3,5-dimethyl-1H-pyrazol-1-yl)-1-piperidinyl]-2-hydroxy-1-propanone

(2R)-1-[4-(4-{[5-chloro-4-(pyrazolo[1,5-a]pyridin-3-yl)-2-pyrimidinyl]amino}-3,5-dimethyl-1H-pyrazol-1-yl)-1-piperidinyl]-2-hydroxy-1-propanone

Conditions
ConditionsYield
With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate In N,N-dimethyl-formamide at 20℃; for 2h; Inert atmosphere;64%
D-Lactic acid
10326-41-7

D-Lactic acid

3-methyl-8-(6-(1-methyl-1H-pyrazol-4-yl)pyridin-(4-piperidin-3-yl)phenyl)-1H-imidazo[4,5-c]quinolin-2(3H)-one hydrochloride

3-methyl-8-(6-(1-methyl-1H-pyrazol-4-yl)pyridin-(4-piperidin-3-yl)phenyl)-1H-imidazo[4,5-c]quinolin-2(3H)-one hydrochloride

1-(4-(1-((R)-2-hydroxypropionyl)piperidin-3-yl)phenyl)3-methyl-8-(6-(1-methyl-1H-pyrazol-4-yl)pyridin-3-yl)-1H-imidazo[4,5-c]quinolin-2-(3H)-one

1-(4-(1-((R)-2-hydroxypropionyl)piperidin-3-yl)phenyl)3-methyl-8-(6-(1-methyl-1H-pyrazol-4-yl)pyridin-3-yl)-1H-imidazo[4,5-c]quinolin-2-(3H)-one

Conditions
ConditionsYield
With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine In dichloromethane at 20℃;63.4%
D-Lactic acid
10326-41-7

D-Lactic acid

tert-butyl 4-[(6-aminothieno[3,2-b]pyridin-7-yl)amino]-3-fluoropiperidine-1-carboxylate
1607590-13-5

tert-butyl 4-[(6-aminothieno[3,2-b]pyridin-7-yl)amino]-3-fluoropiperidine-1-carboxylate

tert-butyl 3-fluoro-4-[(6-{[(2R)-2-hydroxypropanoyl]amino}thieno[3,2-b]pyridin-7-yl)amino]piperidine-1-carboxylate
1607590-14-6

tert-butyl 3-fluoro-4-[(6-{[(2R)-2-hydroxypropanoyl]amino}thieno[3,2-b]pyridin-7-yl)amino]piperidine-1-carboxylate

Conditions
ConditionsYield
With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate In dichloromethane at 20℃;62%

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