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827-52-1 Usage

InChI:InChI=1/C12H16/c1-3-7-11(8-4-1)12-9-5-2-6-10-12/h1,3-4,7-8,12H,2,5-6,9-10H2

827-52-1 Well-known Company Product Price

Brand (Code)Product description CAS number Packaging Price Detail
Alfa Aesar (A16320)  Cyclohexylbenzene, 97+%    827-52-1 100g 446.0CNY Detail
Alfa Aesar (A16320)  Cyclohexylbenzene, 97+%    827-52-1 500g 1652.0CNY Detail
Aldrich (C104809)  Phenylcyclohexane  ≥97% 827-52-1 C104809-25G 340.47CNY Detail
Aldrich (C104809)  Phenylcyclohexane  ≥97% 827-52-1 C104809-100G 840.06CNY Detail
Aldrich (810002)  Phenylcyclohexane  ≥99%, acid < 200 ppm, H2O < 100 ppm 827-52-1 810002-25G 2,533.05CNY Detail

827-52-1SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 12, 2017

Revision Date: Aug 12, 2017

1.Identification

1.1 GHS Product identifier

Product name Cyclohexylbenzene

1.2 Other means of identification

Product number -
Other names 4-phenylcyclohexane

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only.
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:827-52-1 SDS

827-52-1Synthetic route

1-Phenylcyclohexene
771-98-2

1-Phenylcyclohexene

1-phenyl-1-cyclohexane
827-52-1

1-phenyl-1-cyclohexane

Conditions
ConditionsYield
With hydrogen; Pd-immobilized assembled capillaries In tetrahydrofuran at 20℃; for 0.283333h;100%
With hydrogen; micro-encapsulated PI palladium catalyst In tetrahydrofuran at 20℃; for 0.0833333h; Product distribution / selectivity;99%
Stage #1: 1-Phenylcyclohexene With lithium triethylborohydride; cobalt(II) bromide In tetrahydrofuran Inert atmosphere; Glovebox;
Stage #2: With hydrogen In tetrahydrofuran at 20℃; under 1500.15 Torr; for 3h;
99%
cyclohexene
110-83-8

cyclohexene

benzene
71-43-2

benzene

1-phenyl-1-cyclohexane
827-52-1

1-phenyl-1-cyclohexane

Conditions
ConditionsYield
With Y type molecular seives containing SiO2/Al2O3 at 150℃; under 22502.3 Torr; Temperature;99%
With Y-type molecular sieve at 150℃; under 22502.3 Torr; Flow reactor;99.1%
With scandium tris(trifluoromethanesulfonate) In 1,2-dichloro-ethane at 20℃; for 24h; Friedel-Crafts alkylation;98%
1-bromocyclohexane
108-85-0

1-bromocyclohexane

phenylmagnesium bromide

phenylmagnesium bromide

1-phenyl-1-cyclohexane
827-52-1

1-phenyl-1-cyclohexane

Conditions
ConditionsYield
With N,N,N,N,-tetramethylethylenediamine; iron(III) chloride In tetrahydrofuran at 0℃; for 0.5h;99%
Stage #1: phenylmagnesium bromide With dichloro(N,N,N’,N‘-tetramethylethylenediamine)zinc In tetrahydrofuran at 20℃; for 1h;
Stage #2: 1-bromocyclohexane With iron(III) chloride In tetrahydrofuran at 50℃; for 0.5h;
97%
With (1R,2R)-bis(dimethylamino)cyclohexane In tetrahydrofuran at 25℃; for 0.25h;95%
4-cyclohexylphenyl trifluoromethanesulfonate
474317-61-8

4-cyclohexylphenyl trifluoromethanesulfonate

1-phenyl-1-cyclohexane
827-52-1

1-phenyl-1-cyclohexane

Conditions
ConditionsYield
With methanol; magnesium; palladium on activated charcoal at 20℃; for 24h;99%
With ammonium acetate; magnesium; palladium on activated charcoal In methanol at 20℃; for 1h;94%
1-bromocyclohexane
108-85-0

1-bromocyclohexane

phenylmagnesium bromide
100-58-3

phenylmagnesium bromide

1-phenyl-1-cyclohexane
827-52-1

1-phenyl-1-cyclohexane

Conditions
ConditionsYield
With N,N,N,N,-tetramethylethylenediamine; iron(III) chloride In tetrahydrofuran at 0℃; Product distribution / selectivity;99%
With Fe4(μ-Ph)6(THF)4∘2THF In tetrahydrofuran at 20℃; for 0.166667h;95%
With bis(triphenylphosphoranediyl)ammonium tetrachloroferrate(III) at 20℃; for 1h; Reagent/catalyst; Schlenk technique; Inert atmosphere;94%
cyclohexa-1,4-diene
1165952-92-0

cyclohexa-1,4-diene

1-Phenylcyclohexene
771-98-2

1-Phenylcyclohexene

A

1-phenyl-1-cyclohexane
827-52-1

1-phenyl-1-cyclohexane

B

cyclohexene
110-83-8

cyclohexene

Conditions
ConditionsYield
With C24H72Ba2N4Si8 In (2)H8-toluene at 120℃; for 3h; Inert atmosphere; Schlenk technique; Sealed tube;A 99%
B n/a
1-iodocyclohexane
626-62-0

1-iodocyclohexane

phenylmagnesium bromide

phenylmagnesium bromide

1-phenyl-1-cyclohexane
827-52-1

1-phenyl-1-cyclohexane

Conditions
ConditionsYield
Stage #1: phenylmagnesium bromide With dichloro(N,N,N’,N‘-tetramethylethylenediamine)zinc In tetrahydrofuran at 20℃; for 1h;
Stage #2: Cyclohexyl iodide With iron(III) chloride In tetrahydrofuran at 50℃; for 0.5h;
98%
With (1R,2R)-bis(dimethylamino)cyclohexane In tetrahydrofuran at 25℃; for 0.25h;95%
With N,N,N,N,-tetramethylethylenediamine; iron(III) chloride In tetrahydrofuran at 0℃; for 0.5h;99 % Chromat.
1-iodocyclohexane
626-62-0

1-iodocyclohexane

diphenylzinc
1078-58-6

diphenylzinc

1-phenyl-1-cyclohexane
827-52-1

1-phenyl-1-cyclohexane

Conditions
ConditionsYield
With N,N,N,N,-tetramethylethylenediamine; iron(III) chloride In tetrahydrofuran at 50℃; for 0.5h; Product distribution / selectivity;98%
1-phenyl-4-cyclohexanone
4894-75-1

1-phenyl-4-cyclohexanone

1-phenyl-1-cyclohexane
827-52-1

1-phenyl-1-cyclohexane

Conditions
ConditionsYield
With sodium cyanoborohydride at 20℃; for 0.05h;98%
With ethoxyethoxyethanol; hydrazine hydrate; potassium hydroxide at 220℃; under 10343.2 Torr; Wolff-Kishner Reduction; Sonication;83%
With polymethylhydrosiloxane; iron(III) chloride hexahydrate In 1,2-dichloro-ethane at 120℃; for 1h; Microwave irradiation;64%
biphenyl
92-52-4

biphenyl

1-phenyl-1-cyclohexane
827-52-1

1-phenyl-1-cyclohexane

Conditions
ConditionsYield
With Raney nickel; isopropyl alcohol at 82℃; for 6h; Temperature; Inert atmosphere;97%
With nickel(II) oxide; monoaluminum phosphate; iron(II) phthalocyanine; hydrogen at 180℃; under 18751.9 Torr; Large scale;96%
With Raney Ni-Al In potassium hydroxide; water at 90℃; for 3h; Reduction;95%
1-bromocyclohexane
108-85-0

1-bromocyclohexane

diphenylzinc
1078-58-6

diphenylzinc

1-phenyl-1-cyclohexane
827-52-1

1-phenyl-1-cyclohexane

Conditions
ConditionsYield
With N,N,N,N,-tetramethylethylenediamine; iron(III) chloride In tetrahydrofuran at 50℃; for 0.5h; Product distribution / selectivity;97%
In benzene-d6 at 20℃; for 2h; Inert atmosphere; Glovebox;
With bis(triphenylphosphoranediyl)ammonium tetrachloroferrate(III) In tetrahydrofuran at 20℃; for 24h; Schlenk technique; Inert atmosphere;
(n-dodecylthio)benzene
56056-49-6

(n-dodecylthio)benzene

cyclohexylmagnesium bromide
931-50-0

cyclohexylmagnesium bromide

1-phenyl-1-cyclohexane
827-52-1

1-phenyl-1-cyclohexane

Conditions
ConditionsYield
With Nickel (II) acetylacetonate; (Z)-3,3-dimethyl-1,2-bis(diphenylphosphino)-1-butene In cyclopentyl methyl ether for 5h; Inert atmosphere; Reflux;97%
N-cyclohexyl-p-toluenesulfonamide
80-30-8

N-cyclohexyl-p-toluenesulfonamide

benzene
71-43-2

benzene

1-phenyl-1-cyclohexane
827-52-1

1-phenyl-1-cyclohexane

Conditions
ConditionsYield
With sulfuric acid for 3.5h; Heating;96%
methyl-phenyl-thioether
100-68-5

methyl-phenyl-thioether

cyclohexylmagnesium bromide
931-50-0

cyclohexylmagnesium bromide

1-phenyl-1-cyclohexane
827-52-1

1-phenyl-1-cyclohexane

Conditions
ConditionsYield
With Nickel (II) acetylacetonate; (Z)-3,3-dimethyl-1,2-bis(diphenylphosphino)-1-butene In cyclopentyl methyl ether for 5h; Inert atmosphere; Reflux;95%
3,5-dichlorobiphenyl
34883-41-5

3,5-dichlorobiphenyl

1-phenyl-1-cyclohexane
827-52-1

1-phenyl-1-cyclohexane

Conditions
ConditionsYield
With potassium hydroxide; Raney Ni-Al alloy In water at 90℃; for 3h;95%
2-chloro-1,1'-biphenyl
2051-60-7

2-chloro-1,1'-biphenyl

1-phenyl-1-cyclohexane
827-52-1

1-phenyl-1-cyclohexane

Conditions
ConditionsYield
With potassium hydroxide In water at 90℃; for 2h;94%
With potassium hydroxide; Raney Ni-Al alloy In water at 90℃; for 4h;91%
1-iodocyclohexane
626-62-0

1-iodocyclohexane

phenyltrifluorosilane
368-47-8

phenyltrifluorosilane

1-phenyl-1-cyclohexane
827-52-1

1-phenyl-1-cyclohexane

Conditions
ConditionsYield
With (1,2-dimethoxyethane)dichloronickel(II); (1S,2R)-(+)-norphedrine; lithium hexamethyldisilazane; water; cesium fluoride In N,N-dimethyl acetamide at 60℃; for 16h; Hiyama cross-coupling;94%
1-bromocyclohexane
108-85-0

1-bromocyclohexane

phenylmagnesium bromide

phenylmagnesium bromide

A

biphenyl
92-52-4

biphenyl

B

1-phenyl-1-cyclohexane
827-52-1

1-phenyl-1-cyclohexane

Conditions
ConditionsYield
Stage #1: 1-bromocyclohexane; [Fe(C2H4)4][Li(tmeda)]2 In tetrahydrofuran at -20℃;
Stage #2: phenylmagnesium bromide In tetrahydrofuran; diethyl ether at -20℃; Further stages.;
A n/a
B 94%
PCB 11
2050-67-1

PCB 11

1-phenyl-1-cyclohexane
827-52-1

1-phenyl-1-cyclohexane

Conditions
ConditionsYield
With potassium hydroxide; Raney Ni-Al alloy In water at 90℃; for 3h;94%
4,4'-dichlorobiphenyl
2050-68-2

4,4'-dichlorobiphenyl

1-phenyl-1-cyclohexane
827-52-1

1-phenyl-1-cyclohexane

Conditions
ConditionsYield
With Raney Ni-Al alloy; potassium carbonate In water at 90℃; for 5h;93%
2,5-dichlorobiphenyl
34883-39-1

2,5-dichlorobiphenyl

1-phenyl-1-cyclohexane
827-52-1

1-phenyl-1-cyclohexane

Conditions
ConditionsYield
With potassium hydroxide; Raney Ni-Al alloy In water at 90℃; for 3h;93%
cyclohexyl mesylate
16156-56-2

cyclohexyl mesylate

benzene
71-43-2

benzene

1-phenyl-1-cyclohexane
827-52-1

1-phenyl-1-cyclohexane

Conditions
ConditionsYield
With scandium tris(trifluoromethanesulfonate) at 80℃; for 4h;92%
scandium tris(trifluoromethanesulfonate) at 80℃; for 4h;92%
1-bromocyclohexane
108-85-0

1-bromocyclohexane

phenyllithium
591-51-5

phenyllithium

1-phenyl-1-cyclohexane
827-52-1

1-phenyl-1-cyclohexane

Conditions
ConditionsYield
[Li(tmeda)]2[Fe(C2H4)4] In tetrahydrofuran at -20℃;92%
With N,N,N,N,-tetramethylethylenediamine; iron(II) chloride In tetrahydrofuran; dibutyl ether at 20℃; for 1h;
1-phenyl-1-cyclohexane
827-52-1

1-phenyl-1-cyclohexane

Conditions
ConditionsYield
With Raney Ni-Al alloy; potassium carbonate In water at 90℃; for 3h;92%
4'-biphenyl chloride
2051-62-9

4'-biphenyl chloride

1-phenyl-1-cyclohexane
827-52-1

1-phenyl-1-cyclohexane

Conditions
ConditionsYield
With cesium hydroxide In water at 90℃; for 4h;91%
With cesium hydroxide; Raney Ni-Al alloy In water at 90℃; for 4h;91%
chlorobenzene
108-90-7

chlorobenzene

cyclohexylmagnesium bromide
931-50-0

cyclohexylmagnesium bromide

1-phenyl-1-cyclohexane
827-52-1

1-phenyl-1-cyclohexane

Conditions
ConditionsYield
Stage #1: cyclohexylmagnesium bromide With 1,3-bis[(2,6-diisopropyl)phenyl]imidazolinium chloride In tetrahydrofuran at 20℃; for 0.166667h; Kumada Cross-Coupling; Flow reactor; Inert atmosphere;
Stage #2: chlorobenzene With iron(III)-acetylacetonate In tetrahydrofuran at 25℃; for 0.0833333h; Kumada Cross-Coupling; Inert atmosphere; Flow reactor; Irradiation;
91%
biphenyl
92-52-4

biphenyl

A

cyclohexylcyclohexane
92-51-3

cyclohexylcyclohexane

B

1-phenyl-1-cyclohexane
827-52-1

1-phenyl-1-cyclohexane

Conditions
ConditionsYield
With MmNi3.5Co0.7Al0.8H4 at 160℃; under 3677.5 Torr; for 3h;A 4%
B 90%
With MmNi3.5Co0.7Al0.8H4 at 160℃; under 3677.5 Torr; for 3h; Product distribution; other biphenyls, var. temp., var. conc.;A 89%
B 7%
With hydrogen; [(norbornadiene)rhodium(I)chloride]2; phosphinated polydiacetylene In n-heptane at 30℃; under 60800 Torr; for 5.7h;A 78%
B 21%
m-chlorobiphenyl
2051-61-8

m-chlorobiphenyl

1-phenyl-1-cyclohexane
827-52-1

1-phenyl-1-cyclohexane

Conditions
ConditionsYield
With potassium hydroxide In water at 90℃; for 2h;90%
With Raney Ni-Al alloy; potassium carbonate In water at 90℃; for 5h;90%
3,4-dichlorobiphenyl
2974-92-7

3,4-dichlorobiphenyl

1-phenyl-1-cyclohexane
827-52-1

1-phenyl-1-cyclohexane

Conditions
ConditionsYield
With potassium hydroxide; Raney Ni-Al alloy In water at 90℃; for 3h;90%
dibenzothiophene
132-65-0

dibenzothiophene

A

biphenyl
92-52-4

biphenyl

B

1-phenyl-1-cyclohexane
827-52-1

1-phenyl-1-cyclohexane

Conditions
ConditionsYield
With hydrogen In n-heptane at 350℃; under 760.051 Torr; for 1h; Catalytic behavior; Reagent/catalyst; Temperature; Flow reactor;A 88.6%
B 4%
With hydrogen sulfide; hydrogen In Hexadecane at 300℃; under 54755.5 Torr; for 8h; Catalytic behavior; Reagent/catalyst; Inert atmosphere;A 80.6%
B 15.2%
With aluminum oxide; sodium hydroxide; hydrogen; dodecacarbonyl-triangulo-triruthenium In xylene at 300℃; under 38000 Torr; for 10h; Product distribution; on alumina-supported ruthenium acetylacetonate or ruthenium chloride catalyst systems;A 67%
B 4%
1-phenyl-1-cyclohexane
827-52-1

1-phenyl-1-cyclohexane

acetyl chloride
75-36-5

acetyl chloride

4-cyclohexylacetophenone
18594-05-3

4-cyclohexylacetophenone

Conditions
ConditionsYield
With aluminum (III) chloride In dichloromethane at 0℃; for 0.166667h;100%
With aluminium trichloride In dichloromethane for 24h; Ambient temperature;85%
With aluminium trichloride In dichloromethane at 0℃; for 0.5h;61%
1-phenyl-1-cyclohexane
827-52-1

1-phenyl-1-cyclohexane

cyclohexylcyclohexane
92-51-3

cyclohexylcyclohexane

Conditions
ConditionsYield
With hydrogen; platinum(IV) oxide In acetic acid at 250℃; under 1875.2 Torr; for 8h;100%
With hydrogen; [(η6-C6H6)(η6-C6Me6)Ru3(μ2-H)(μ2-OH)(μ3-O)]+ In water at 110℃; under 45003.6 Torr; for 1h;100.0 % Chromat.
carbon monoxide
201230-82-2

carbon monoxide

1-phenyl-1-cyclohexane
827-52-1

1-phenyl-1-cyclohexane

4-cyclohexylbenzaldehyde
27634-89-5

4-cyclohexylbenzaldehyde

Conditions
ConditionsYield
With hydrogen fluoride; boron trifluoride In n-heptane at -30℃; under 15001.5 Torr; for 1h; Autoclave;100%
With hydrogen fluoride; boron trifluoride In n-heptane at -30℃; under 15001.5 Torr; for 1h;
With hydrogen fluoride; boron trifluoride In n-heptane at -30℃; under 15001.5 Torr; for 1h; Autoclave;
With hydrogen fluoride; boron trifluoride In n-heptane at -30℃; under 15001.5 Torr; for 1h; Autoclave;
With hydrogen fluoride; boron trifluoride In n-heptane at -30℃; under 15001.5 Torr; for 1h; Autoclave;
1-phenyl-1-cyclohexane
827-52-1

1-phenyl-1-cyclohexane

α-chloromethylthio-γ-butyrolactone
106241-39-8

α-chloromethylthio-γ-butyrolactone

3-(4-Cyclohexyl-benzylsulfanyl)-dihydro-furan-2-one
106241-50-3

3-(4-Cyclohexyl-benzylsulfanyl)-dihydro-furan-2-one

Conditions
ConditionsYield
With tin(IV) chloride In dichloromethane for 1h; Ambient temperature;94%
1-phenyl-1-cyclohexane
827-52-1

1-phenyl-1-cyclohexane

Cyclohexanecarboxylic acid
98-89-5

Cyclohexanecarboxylic acid

Conditions
ConditionsYield
With sodium periodate; ruthenium trichloride In tetrachloromethane; water; acetonitrile for 24h; Ambient temperature;94%
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